journal article·2023-07-03Open access

Effect of magnesium oxide in multiphase additive on the formation process and morphology of β-Si3N4 whisker

Ziyue Wang, Qianqian Wu, Lujie Wang, Qian Qi, Ning Cui, Tongyang Li, Yuan Yu, Huaguo Tang, Zhuhui Qiao

Abstract

β-Si3N4 whiskers were synthesized by using a moderately low-temperature heat-treatment process, with the aid of a low weight fraction of multiple aids (Y2O3-MgO). The synthesis conditions and aspect ratio of the whiskers were adjusted by changing the MgO content in the composite additive system, heat treatment temperature and holding time. The phase composition and morphology of the whiskers were analyzed by XRD and SEM, respectively. The phase transformation could be completed at 1700°C by introducing only 0.5 wt% MgO. The heat-treated temperature was successfully further reduced to 1650°C by extending the holding time to 5 h. The introduction of MgO can make the whiskers form rapidly at a lower temperature. By introducing a small amount of MgO and appropriately extending the holding time at a lower treatment temperature has been proved to be an effective method to obtain β-Si3N4 whiskers with higher aspect ratio under mild conditions.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · MXene and MAX Phase Materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

School of Mechanical and Automotive Engineering, Qingdao University of Technology, Qingdao, 266520, China

State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, China

School of Materials Science and Engineering, Shandong University of Science and Technology, Qingdao, Shandong, 266590, China

Shandong Laboratory of Yantai Advanced Materials and Green Manufacturing, Yantai, Shandong, 264006, China

Qingdao Center of Resource Chemistry & New Materials, Qingdao, 266000, China

Funding

National Natural Science Foundation of China · Natural Science Foundation of Shandong Province · State Key Laboratory of High Performance Ceramics and Superfine Microstructure

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