journal article·2007Open access

Parallel-plate Rheometer Calibration Using Oil and Computer Simulation

Chiara F. Ferraris, Mette Geiker, Nicos S. Martys, Nicholas Muzzatti

Abstract

Fluid flow patterns in traditional rotational rheometers are generally well known and rheological parameters such as viscosity can be easily calculated from experimental data of single phase fluids and analytical solutions of the patterns. However, when the fluid is a suspension, where some of the particles are as large as 2 mm in diameter, these rheometers need to be modified. The distance between the shearing planes needs to be increased, which necessitates additional physical confinement of the fluid. This causes the flow pattern to be not analytically soluble leading to an inability to correctly compute the viscosity. This paper presents a modified parallel plate rheometer, and proposes means of calibration using standard oils and numerical simulation of the flow. A lattice Boltzmann method was used to simulate the flow in the modified rheometer, thus using an accurate numerical solution in place of the intractable analytical solution. The simulations reproduced experimental results by taking into account the actual rheometer geometry. The numerical simulations showed that small changes in the rheometer design can have a significant impact on how the rheological data should be extracted from the experimental results.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Lattice Boltzmann Simulation Studies · Rheology and Fluid Dynamics Studies · Fluid Dynamics and Vibration Analysis

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

National Institute of Standard and Technology (NIST), Gaithersburg, USA.

Technical University of Denmark, Lyngby, Denmark.

References (20)

Show source-provided references
1. Banfill, P. F. G. (1990). “Use of the ViscoCorder to study the rheology of fresh concrete.” Mag. of Concrete Research, 42 (153), 213-221.10.1680/macr.1990.42.153.213 ↗
2. Davies, G. A. and Stokes, J. R. (2005). “On the gap error in parallel plate rheometry that arises from the presence of air when zeroing the gap.” J. of Rheology, 49(4), 919-922.10.1122/1.1942501 ↗
3. De Larrard, F., Sedran, T., Hu, C., Sitzkar, J. C., Joly, M. and Derkx, F. (1996). “Evolution of the workability of superplasticized concretes: Assessment with BTRHEOM rheometer.” in P. J. M. Bartos, D. L. Marrs and D. J. Cleland (Eds.), Proceedings of the International RILEM Conference on Production Methods and Workability of Concrete, RILEM, Paisley, 377-388.
4. Ferraris, C. and Gaidis, J. M. (1992). “The Connection between the rheology of concrete and the rheology of cement paste.” ACI Materials Journal, 88(4), 388-393.
5. Ferraris, C. F. (1999). “Measurement of the rheological properties of cement paste: a new approach.” Int. RILEM Conf. “The role of admixtures in high performance concrete.” ed. by J. G. Cabrera and R. Rivera-Villareal, Monterrey (Mexico) 333-342.
6. Ferraris, C. and Brower, L. (Eds.). (2001). “Comparison of concrete rheometers: International tests at LCPC (Nantes, France) in October 2000.” NISTIR 6819.
7. Ferraris, C. and Martys, N. (2001b). “De la pâte de ciment au béton: modélisation et mesures expérimentales des propriétés rhéologiques.” Proc. Rhéologie Génie Civil et Environment, 36 ème Colloque du Groupe Français de Rhéologie, Marne-la-Vallée (France) 226-230.
8. Ferraris, C. F. and Martys, N. S. (2003). “Relating fresh concrete viscosity measurements from different rheometers.” J. of Res. Natl. Inst. of Stand. and Technol., http://www.nist.gov/jres 108 (3) 229 -234.
9. Ferraris, C. and Brower, L. (Eds.). (2004). “Comparison of concrete rheometers: International tests at MB (Cleveland OH, USA) in May 2003.” NISTIR 7154.
10. Hsieh, G., Mason, T. O., Garboczi, E. J. and Pederson, L. R. (1997). “Experimental limitations in impedance spectroscopy: Part III--Effect of reference electrode position.” Solid State Ionics 96, 153-172.10.1016/S0167-2738(97)00073-8 ↗
11. Hu, C. “Rhéologie des bétons fluides.” (1995). “Etudes et recherches des Laboratoires des Ponts et Chaussées.” OA 16, 203 p., Paris, France.
12. Martys, N. S. and Hagedorn, J. G. (2002). “Multiscale modeling of fluid transport in heterogeneous materials using discrete Boltzmann methods.” Materials and Structures, 35, 650-659.10.1007/BF02480358 ↗
13. Martys, N. S., Ferraris, C. F., Gupta, V., Cheung J. H., Hagedorn, J. G., Peskin, A. P. and Garboczi, E. J. (2007). “Computational model predictions of suspension rheology: Comparison to experiment.” 12th Int. Congress of the Chemistry of Cement, Montreal (Canada) paper # W6-06.3.
14. Nachbaur, L., Mutin, J. C., Nonat, A. and Choplin, L. (2001). “Dynamic mode rheology of cement and tricalcium silicate pastes from mixing to setting.” Cement and Concrete Research, 31, 183-192.10.1016/S0008-8846(00)00464-6 ↗
15. Sanchez-Perez, J. and Archer, L. A. (2003). “Interfacial slip violations in polymer solutions: Role of microscale surface roughness.” Langmuir, 3304-3312.10.1021/la0265326 ↗
16. Struble, L. J. and Sun, G.-K. (1997). “Rheological changes associated with cement setting.” Proceedings of the 2nd RILEM Workshop on Hydration and Setting, Dijon.
17. Swindells, J. F., Hardy, R. C. and Cottington, R. L. (1954). “Precise measurements with Bingham viscometers and cannon master viscometers.” J. of Research of the Nat. Bureau of Standards, 52(3), 105-115.10.6028/jres.052.016 ↗
18. Tattersal, G. H. and Banfill, P. F. G. (1983). “The rheology of fresh concrete.” Pitman Advanced Publishing Program.
19. Wallevik, O. (1990). “Den ferske betongens reologi of anvendelse pa betong med og uten tilsetningt av silikastov.” PhD. Thesis, University of Trondheim, NTH.
20. Yang, M. and Jennings, H. M. (1995). “Influences of mixing methods on the microstructure and rheological behavior of cement paste.” Advn. Cem. Bas. Mat., 2, 70-78.10.1016/1065-7355(95)90027-6 ↗