journal article·2024-11-08Open access

Data Reconciliation for Assessing Compliance of Physicochemical Properties of Petroleum Products in Commercial Transactions

Rosana Medeiros Moreira, Ariadne Mayra Silva Rocha, Elcio Cruz de Oliveira

Applied Sciences· Volume 14· Issue 22

Abstract

The physicochemical properties of petroleum products in commercial transactions are crucial for quality control in the oil and gas industry. However, different laboratories often produce slightly different measurement results. These variations can be significant when approving or rejecting properties based on regulatory agency and environmental body specifications. A simple arithmetic average is typically used to determine the most probable value in disputes. This study proposed using a Data Reconciliation approach to address the disparity between the projected model and empirical data. An objective function was employed to optimize and evaluate parameters using maximum likelihood estimation, considering the experimental uncertainty values. This study found that the flash point of jet fuel, as determined by the Tag Closed Cup Tester, was within the specified range (maximum of 40 °C). The application of this tool resolved a dispute between a supplier and a customer, as the reconciled value with minimized uncertainty was determined to be 37.5 ± 2.0 °C. Additionally, the study utilized experimental results from 12 accredited laboratories to determine a single reconciled value for the final boiling point of gasoline. Despite the varying experimental uncertainties ranging from 6.0 °C to 13 °C, the reconciled uncertainty was minimized to 2.6 °C. The last case study identified that ASTM D4294 was incompatible with other test methods for evaluating the mass fraction in diesel oil. In this manner, Data Reconciliation enhanced the accuracy and effectively reduced measurement uncertainties, rendering it a potent tool for resolving legal disputes when evaluating the compliance of the physicochemical properties of petroleum products in commercial transactions.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Fault Detection and Control Systems · Scientific Measurement and Uncertainty Evaluation · Spectroscopy and Chemometric Analyses

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

National Institute of Technology, Rio de Janeiro 20081-312, Brazil

Brazilian Institute of Metrology, Quality and Technology (INMETRO), Duque de Caxias 25250-020, Brazil

Postgraduate Programme in Metrology, Pontifical Catholic University of Rio de Janeiro, Rio de Janeiro 22451-900, Brazil

Land Transportation and Storage, Measurement and Product Inventory Management, Logistics, Petrobras S.A., Rio de Janeiro 20231-030, Brazil

Funding

Brazilian agency CNPq · Coordenação de Aperfeiçoamento de Pessoal de Nível Superior—Brasil (CAPES)

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