journal article·2022-07-18Open access

Additive Manufacturing Potentials of High Performance Ferritic (HiperFer) Steels

Torsten Fischer, Bernd Kuhn, Xiuru Fan, Markus Benjamin Wilms

Applied Sciences· Volume 12· Issue 14

Abstract

In the present study, the first tailored steel based on HiperFer (high-performance ferrite) was developed specifically for the additive manufacturing process. This steel demonstrates its full performance potential when produced via additive manufacturing, e.g., through a high cooling rate, an in-build heat treatment, a tailored microstructure and counteracts potential process-induced defects (e.g. pores and cavities) via “active” crack-inhibiting mechanisms, such as thermomechanically induced precipitation of intermetallic (Fe,Cr,Si)2(W,Nb) Laves phase particles. Two governing mechanisms can be used to accomplish this: (I) “in-build heat treatment” by utilizing the “temper bead effect” during additive manufacturing and (II) “dynamic strengthening” under cyclic, plastic deformation at high temperature. To achieve this, the first HiperFerAM (additive manufacturing) model alloy with high precipitation kinetics was developed. Initial mechanical tests indicated great potential in terms of the tensile strength, elongation at rupture and minimum creep rate. During the thermomechanical loading, global sub-grain formation occurred in the HiperFerAM, which refined the grain structure and allowed for higher plastic deformation, and consequently, increased the elongation at rupture. The additive manufacturing process also enabled the reduction of grain size to a region, which has not been accessible by conventional processing routes (casting, rolling, heat treatment) so far.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · High Temperature Alloys and Creep · High Entropy Alloys Studies

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Institute of Energy and Climate Research (IEK), Microstructure and Properties of Materials (IEK-2), Forschungszentrum Jülich GmbH, 52425 Julich, Germany

Central Iron & Steel Research Institute (CISRI) Group, Material Digital R&D Centre, Beijing 100081, China

Materials Science and Additive Manufacturing, School of Mechanical Engineering and Safety Engineering, University of Wuppertal, 42119 Wuppertal, Germany

Fraunhofer-Institute for Laser Technology (ILT), 52074 Aachen, Germany

Funding

German Helmholtz Society framework programme “Energy Efficiency, Materials and Resources”

References (57)

Show source-provided references
1. The effect of absorption ratio on meltpool features in laser-based powder bed fusion of IN71810.1016/j.optlastec.2022.108263 ↗
2. Thermal properties of powder beds in energy absorption and heat transfer during additive manufacturing with electron beam10.1016/j.powtec.2020.11.082 ↗
3. Evolution of temperature and residual stress behavior in selective laser melting of 316L stainless steel across a cooling channel10.1108/RPJ-09-2021-0237 ↗
4. Investigation of temperature distribution and solidification morphology in multilayered directed energy deposition of Al-0.5Sc-0.5Si alloy10.1016/j.ijheatmasstransfer.2021.122492 ↗
5. Study of anisotropy through microscopy, internal friction and electrical resistivity measurements of Ti-6Al-4V samples fabricated by selective laser melting10.1108/RPJ-06-2021-0151 ↗
6. Control of thermally stable core-shell nano-precipitates in additively manufactured Al-Sc-Zr alloys
7. High-strength Damascus steel by additive manufacturing10.1038/s41586-020-2409-3 ↗
8. Massive nanoprecipitation in an Fe-19Ni-xAl maraging steel triggered by the intrinsic heat treatment during laser metal deposition10.1016/j.actamat.2017.02.069 ↗
9. Fischer, T., Kuhn, B., Rieck, D., Schulz, A., Trieglaff, R., and Wilms, M.B. (2020). Fatigue Cracking of Additively Manufactured Materials—Process and Material Perspectives. Appl. Sci., 10.10.3390/app10165556 ↗
10. Mapping the geometry of Ti-6Al-4V: From martensite decomposition to localized spheroidization during selective laser melting10.1016/j.scriptamat.2020.02.043 ↗
11. Rittinghaus, S.-K., Amr, A., and Hecht, U. (2022). Intrinsic heat treatment of an additively manufactured medium entropy AlCrFe2Ni2-alloy. Met. Mater. Int.10.1007/s12540-022-01246-0 ↗
12. Influence of thermal properties on residual stresses in SLM of aerospace alloys10.1108/RPJ-03-2019-0065 ↗
13. Mishrunova, T., Artzt, K., Haubrich, J., Requena, G., and Bruno, G. (2019). Exploring the correlation between subsurface residual stresses and manufacturing parameters in laser powder bed fused Ti-6Al-4V. Metals, 9.10.3390/met9020261 ↗
14. Influence of high-productivity process parameters on the surface quality and residual stress state of AISI 316L components produced by directed energy deposition10.1007/s11665-021-05954-3 ↗
15. Proposal of design rules for improving the accuracy of selective laser melting (SLM) manufacturing using benchmarks parts10.1108/RPJ-06-2021-0130 ↗
16. Defect formation and prevention in directed energy deposition of high-manganese steels and the effect on mechanical properties10.1016/j.msea.2019.138688 ↗
17. Ikeda, T., Yonehara, M., Ikeshoji, T.-T., Nobuki, T., Hatate, M., Kuwabara, K., Otsubo, Y., and Kyogoku, H. (2021). Influences of process parameters on the microstructure and mechanical properties of CoCrFeNiTi based high-entropy alloy in a laser powder bed fusion process. Crystals, 11.10.3390/cryst11050549 ↗
18. Fatigue life optimization for 17-4Ph steel produced by selective laser melting10.1108/RPJ-03-2021-0062 ↗
19. Steels in additive manufacturing: A review of their microstructure and properties10.1016/j.msea.2019.138633 ↗
20. Anisotropic properties of directed energy deposition (DED)-processed Ti–6Al–4V10.1016/j.jmapro.2016.06.020 ↗
21. Davies, C.M., Thomlinson, H., and Hooper, P.A. (2017, January 26). Fatigue Crack Initiation and Growth Behaviour of 316L Stainless Steel Manufactured Through Selective Laser Melting. Proceedings of the ASME 2017 Pressure Vessels and Piping Conference, Volume 6A: Materials and Fabrication, Waikoloa, HI, USA.10.1115/PVP2017-65410 ↗
22. Effects of building orientation and heat treatment on fatigue behavior of selective laser melted 17-4 PH stainless steel10.1016/j.ijfatigue.2016.03.014 ↗
23. High cycle fatigue and ratcheting interaction of laser powder bed fusion stainless steel 316L: Fracture behaviour and stress-based modelling10.1016/j.ijfatigue.2018.12.016 ↗
24. Blinn, B., Klein, M., Gläßner, C., Smaga, M., Aurich, J.C., and Beck, T. (2018). An investigation of the microstructure and fatigue behavior of additively manufactured AISI 316L stainless steel with regard to the influence of heat treatment. Metals, 8.10.3390/met8040220 ↗
25. HiperFer—High Performance Ferritic Steels
26. Development of High Chromium Ferritic Steels Strengthened by Intermetallic Phases10.1016/j.msea.2013.11.048 ↗
27. Kuhn, B., Lopez Barrilao, J., and Fischer, T. (2019, January 21–24). “Reactive” microstructure, the key to cost-effective, fatigue-resistant high temperature structural materials. Proceedings of the Joint EPRI-123HiMAT International Conference on Advances in High Temperature Materials, Nagasaki, Japan.10.31399/asm.cp.am-epri-2019p0001 ↗
28. The Influence of Deformation on the Precipitation Behavior of a Ferritic Stainless Steel
29. Pöpperlová, J., Fan, X., Kuhn, B., Bleck, W., and Krupp, U. (2020). Impact of Tungsten on Thermomechanically Induced Precipitation of Laves Phase in High Performance Ferritic (HiperFer) Stainless Steels. Appl. Sci., 10.10.3390/app10134472 ↗
30. Fan, X., Kuhn, B., Pöpperlová, J., Bleck, W., and Krupp, U. (2020). Thermomechanically Induced Precipitation in High Performance Ferritic (HiperFer) Stainless Steels. Appl. Sci., 10.10.3390/app10165713 ↗
31. Fan, X., Kuhn, B., Pöpperlová, J., Bleck, W., and Krupp, U. (2020). Compositional Optimization of High-Performance Ferritic (HiperFer) Steels—Effect of Niobium and Tungsten Content. Metals, 10.10.3390/met10101300 ↗
32. Kuhn, B., Talik, M., Fischer, T., Fan, X., Yamamoto, Y., and Lopez Barrilao, J. (2020). Science and technology of high performance ferritic (HiperFer) Stainless Steels. Metals, 10.10.20944/preprints202003.0120.v1 ↗
33. Kuhn, B., Barrilao, J.L., and Fischer, T. (2020). Impact of Thermomechanical Fatigue on Microstructure Evolution of a Ferritic-Martensitic 9 Cr and a Ferritic, Stainless 22 Cr Steel. Appl. Sci., 10.10.3390/app10186338 ↗
34. Blinn, B., Görzen, D., Fischer, T., Kuhn, B., and Beck, T. (2020). Analysis of the Thermomechanical Fatigue Behavior of Fully Ferritic High Chromium Steel Crofer®22 H with Cyclic Indentation Testing. Appl. Sci., 10.10.3390/app10186461 ↗
35. Development of high strength ferritic steel for interconnect application in SOFCs10.1016/j.jpowsour.2007.12.028 ↗
36. National Board Inspection Code (NBIC) (2011). Part-3 National Board Inspection Code, ASME Press.
37. ASME BPV Code (2019). Section III, Division 1: Rules for Construction of Nuclear Facility Components, ASME Press.
38. Welding Technology Institute of Australis (2006). (WTIA) publication, TGN-PE-02, Temper Bead Welding, Rev0,1, Welding Technology Institute of Australia.
39. ASME BPVC (2015). Section IX-Welding, Brazing, and Fusing Qualifications, ASME Press.
40. Talik, M., and Kuhn, B. (2015, January 15–17). High Temperature Mechanical Properties of a 17wt%Cr High Performance Ferritic (HiperFer) Steel Strengthened by Intermetallic Laves Phase Particles. Proceedings of the 9th International Charles Parsons Turbine and Generator Conference, Loughborough, UK.
41. (1991). Zugversuch, Prüfverfahren bei erhöhter Temperatur, DIN Deutsches Institut für Normung e. V. (Standard No. DIN EN 10002-5:1992-02).
42. (2011). Metallische Werkstoffe-Zugversuch-Teil 2: Prüfverfahren bei erhöhter Temperatur, DIN Deutsches Institut für Normung e. V. (Standard No. DIN EN ISO 6892-2:2011-05).
43. (2018). Metallic Materials-Vickers Hardness Test-Part 1: Test method (ISO 6507-1:2018) (Standard No. DIN EN ISO 6507-1:2018).
44. Identification, size classification and evolution of Laves phase precipitates in high chromium, fully ferritic steels10.1016/j.micron.2017.07.010 ↗
45. Effect of Nb precipitate coarsening on the high temperature strength in Nb containing ferritic stainless steels10.1016/j.msea.2005.01.030 ↗
46. Precipitation behavior of Laves phase and its effect on toughness of 9Cr-2Mo Ferritic-martensitic steel10.1016/S0022-3115(86)80083-6 ↗
47. Formation of Laves Phase in Sanicro 25 Austenitic Steel during Creep-Rupture Test at 700 °C10.1007/s13632-019-00529-0 ↗
48. On the formation and growth of Mo-rich Laves phase particles during long-term creep of a 12% chromium tempered martensite ferritic steel10.1016/j.scriptamat.2009.08.031 ↗
49. Guo, J.T., and Zhou, L.Z. (1996, January 22–26). The Effect of Phosphorus, Sulphur and Silicon on Segregation, Solidification and Mechanical Properties of Cast Alloy 718. Proceedings of the 8th International Symposium on Superalloys, Seven Springs Mountain Resort, Champion, PA, USA.10.7449/1996/Superalloys_1996_451_455 ↗
50. Effect of Si on Precipitation Behavior of Nb-Laves Phase and Amount of Nb in Solid Solution at Elevated Temperature in High Purity 17%Cr-0.5%Nb Steels10.2320/matertrans.M2010112 ↗
51. Temperature Dependence of Laves Phase Composition in Nb, W and Si-Alloyed High Chromium Ferritic Steels for SOFC Interconnect Applications10.1007/s11669-015-0403-5 ↗
52. Creep properties and microstructure of a precipitation-strengthened ferritic Fe–Al–Ni–Cr alloy10.1016/j.actamat.2014.02.020 ↗
53. Fan, X. (2020). Optimization of Laves Phase Strengthened High Performance Ferritic Stainless Steels. [Ph.D. Thesis, RWTH Aachen]. Available online: https://publications.rwth-aachen.de/record/792517/files/792517.pdf.
54. Kuhn, B., Fischer, T., Fan, X., Talik, M., Aarab, F., and Yamamoto, Y. (2020, January 27). HiperFer-Weiterentwicklungs-Und Anwendungspotenziale. Proceedings of the 43th FVWHT Vortragsveranstaltung Langzeitverhalten Warmfester Stähle und Hochtemperaturwerkstoffe, Online.
55. Kuhn, B., Talik, M., Lopez Barrilao, J., and Singheiser, L. (July, January 29). Microstructure stability of ferritic-martensitic, austenitic and fully ferritic steels under fluctuating loading conditions. Proceedings of the 1st 123rd HiMat Conference, Sapporo, Japan.
56. Training high-strength aluminum alloys to withstand fatigue10.1038/s41467-020-19071-7 ↗
57. Lesuer, D.R., Syn, C.K., and Sherby, O.D. (1999). An Evaluation of Power Law Breakdown in Metals, Alloys, Dispersion Hardened Materials and Compounds, Lawrence Livermore National Lab.(LLNL).