journal article·2025-12-07Open access

Atmospheric Pressure Plasma Surface Treatment for Structural Adhesive Bonding in Automotive Body Manufacturing: A Parametric Study

Ertugrul Ilhan, Kadir Cavdar

Applied Sciences· Volume 15· Issue 24

Abstract

This study investigates the optimization of structural adhesives used in automotive body manufacturing processes via Thermal Atmospheric Pressure Plasma (TAPP) and Cold Atmospheric Plasma (CAP) surface treatments. Surface preparation of sheet metal parts using plasma before the adhesive joining process represents an innovative approach not yet utilized in automotive body production, and this work seeks to fill a gap in the existing literature. Test samples were prepared to compare the effects of curing temperature and time, as well as of TAPP versus CAP surface preparation, on bond strength. Using a Taguchi experimental design, we systematically varied five parameters: adhesive curing time, curing temperature, plasma type (TAPP or CAP), plasma-sample distance, and number of plasma passes. Tensile tests on the resulting specimens quantified bond strength, and regression analysis of those results identified the optimal processing conditions. The findings offer valuable insights into how TAPP and CAP treatments affect the adhesive joining of automotive sheet metals and establish the optimum parameters for each method.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Surface Modification and Superhydrophobicity · Mechanical Behavior of Composites · Fiber-reinforced polymer composites

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Mechanical Engineering, Faculty of Engineering, Bursa Uludag University, 16059 Bursa, Türkiye

References (26)

Show source-provided references
1. Experimental analysis of steel joints bonded with automotive grade hot setting structural adhesives
2. Structural bonding in automotive body shop10.1007/s35784-017-0006-0 ↗
3. Experimental methods to capture curing induced effects in adhesive bonded joints10.1016/j.ijadhadh.2020.102735 ↗
4. On the Development of Structural Adhesive Technology for the Automotive Body in Japan10.1016/0389-4304(96)00008-2 ↗
5. Optimization of inductive fast-curing of epoxy adhesive by model-based kinetics10.1016/j.ijadhadh.2023.103392 ↗
6. Analysis of the effect of selected factors on the strength of adhesive joints10.1088/1757-899X/393/1/012041 ↗
7. iSens: A fiber-based, highly permeable and imperceptible sensor design10.1002/adma.202102736 ↗
8. Vassilopoulos, A.S. (2009). Effect of Surface Preparation on the Behaviour of Double Strap Adhesive Joints with Thick Steel Adherents. Durability of Composites for Civil and Military Applications, CRC Press.
9. Experimental investigation of the effects of adhesive thickness on the fracture behavior of structural acrylic adhesive joints under various loading rates10.1016/j.ijadhadh.2020.102782 ↗
10. Atlas Copco (2023, June 12). Dispensing System for Body Shops. Available online: https://www.atlascopco.com/en-uk/itba/products/joining-solutions/industrial-dispensing-systems/sca-body-shop-dispensing-systems.
11. ISRA Vision (2024, August 14). Inspection Solutions for the Body Shop. Available online: https://www.isravision.com/en-en/industries/automotive/body-shop#bead-&-seam-inspection.
12. Adhesively bonded joints–a review on design, manufacturing, experiments, modeling and challenges10.1016/j.compositesb.2024.111225 ↗
13. Significant slowdown of plasma-optimized surface energy deactivation by vacuum sealing for efficient adhesive bonding10.1016/j.compositesb.2022.110001 ↗
14. Kovács, P., Körömi, B., Weltsch, Z., and Berczeli, M. (2023). Investigation of the Tensile Strength of Adhesive-Bonded Steels Using Surface Treatments. Materials, 16.10.3390/ma16247663 ↗
15. Kim, D.H., Kim, H.S., Jung, Y., Hong, J.-Y., Jeon, Y.-P., and Lee, J.U. (2025). Plasma Treatment of Metal Surfaces for Enhanced Bonding Strength of Metal–Polymer Hybrid Structures. Polymers, 17.10.3390/polym17020165 ↗
16. Wen, L., Dong, Z., and Wang, R. (2025). The Effect of Low-Temperature Plasma Treatment on the Adhesive Bonding Performance of CF/PEKK Surfaces. Surfaces, 8.10.3390/surfaces8030041 ↗
17. Károly, Z., Kalácska, G., Zsidai, L., Mohai, M., and Klébert, S. (2018). Improvement of Adhesion Properties of Polyamide 6 and Polyoxymethylene-Copolymer by Atmospheric Cold Plasma Treatment. Polymers, 10.10.3390/polym10121380 ↗
18. Surface analysis of 316 stainless steel treated with cold atmospheric plasma10.1016/j.apsusc.2017.01.150 ↗
19. Ohkubo, Y., Okazaki, Y., Shibahara, M., Nishino, M., Seto, Y., Endo, K., and Yamamura, K. (2021). Effects of He and Ar Heat-Assisted Plasma Treatments on the Adhesion Properties of Polytetrafluoroethylene (PTFE). Polymers, 13.10.3390/polym13234266 ↗
20. Optimization of high-pressure laminate manufacturing process by Taguchi method
21. Dehnad, K. (2012). Quality Control, Robust Design, and the Taguchi Method, Springer.
22. Using Taguchi method to optimize the performance of flexible manufacturing systems: An empirical model10.4028/www.scientific.net/AMM.799-800.1410 ↗
23. A review of adhesive steel-to-steel connections for use in heavy construction10.1016/j.jcsr.2023.108405 ↗
24. Ereğli Demir ve Çelik Fabrikaları T.A.Ş. (2023, December 10). Yassı Ürünler Kataloğu. Available online: https://www.erdemir.com.tr/storage/uploads/2023/09/114532c6a680955c24e52da88e4fb2a6.pdf.
25. Henkel AG & Co. KGaA (2023, June 22). Technisches Datenblatt: TEROSON EP 4552 GB (Revision 1). Available online: https://www.sks-gmbh.com/jdownloads/Henkel%20Datenbltter/Teroson/TEROSON%20EP%204552%20GB-DE.pdf.
26. (2022). Adhesives—Designation of Main Failure Patterns of Bonded Joints (Standard No. ISO 10365:2022).