journal article·2021-07-01Open access

Rapid subsurface damage detection of SiC using inductivity coupled plasma

Yi Zhang, Linfeng Zhang, Keyu Chen, Dianzi Liu, Dong Lu, Hui Deng

Abstract

Abstract This paper proposes a method for the rapid detection of subsurface damage (SSD) of SiC using atmospheric inductivity coupled plasma. As a plasma etching method operated at ambient pressure with no bias voltage, this method does not introduce any new SSD to the substrate. Plasma diagnosis and simulation are used to optimize the detection operation. Assisted by an SiC cover, a taper can be etched on the substrate with a high material removal rate. Confocal laser scanning microscopy and scanning electron microscope are used to analyze the etching results, and scanning transmission electron microscope (STEM) is adopted to confirm the accuracy of this method. The STEM result also indicates that etching does not introduce any SSD, and the thoroughly etched surface is a perfectly single crystal. A rapid SSD screening ability is also demonstrated, showing that this method is a promising approach for the rapid detection of SSD.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Plasma Diagnostics and Applications · Semiconductor materials and devices · Silicon Carbide Semiconductor Technologies

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (42)

Show source-provided references
1. Silicon carbide—a high-transparency nonlinear material for THz applications10.1364/OE.24.002590 ↗
2. Ultrahigh-quality silicon carbide single crystals10.1038/nature02810 ↗
3. Fabrication of liquid phase sintered SiC materials and their characterization10.1016/j.fusengdes.2005.09.025 ↗
4. Mechanical behavior of single crystalline and polycrystalline silicon carbides evaluated by Vickers indentation10.2109/jcersj.109.1271_602 ↗
5. Study on tool wear characteristics in diamond turning of reaction-bonded silicon carbide10.1007/s00170-011-3289-3 ↗
6. High fluence laser damage precursors and their mitigation in fused silica10.1364/OE.22.005839 ↗
7. Mechanical properties and elastic constants due to damage accumulation and amorphization in SiC10.1103/PhysRevB.69.224108 ↗
8. Effects of mechanical damage on the electrical properties of zirconia ceramics10.1016/0955-2219(92)90074-N ↗
9. Effects of process parameter variations on the removal rate in chemical mechanical polishing of 4H-SiC10.1007/s11664-001-0111-2 ↗
10. Investigation on the material removal and surface generation of a single crystal SiC wafer by ultrasonic chemical mechanical polishing combined with ultrasonic lapping10.3390/ma11102022 ↗
11. Recent development of chemical mechanical polishing
12. Physical, chemical, and in vitro toxicological characterization of nanoparticles in chemical mechanical planarization suspensions used in the semiconductor industry: towards environmental health and safety assessments10.1039/C5EN00046G ↗
13. Methods for detection of subsurface damage: a review10.1186/s10033-018-0229-2 ↗
14. Evaluating subsurface damage in optical glasses10.2971/jeos.2011.11001 ↗
15. Sub-surface mechanical damage distributions during grinding of fused silica10.1016/j.jnoncrysol.2006.09.012 ↗
16. Subsurface damage measurement of ground fused silica parts by HF etching techniques10.1364/OE.17.020448 ↗
17. Surface and subsurface damage in Zerodur® glass ceramic during ultrasonic assisted grinding10.1007/s00170-016-9551-y ↗
18. Wet etching of GaN, AlN, and SiC: a review10.1016/j.mser.2004.11.002 ↗
19. Research of polishing process to control the iron contamination on the magnetorheological finished KDP crystal surface10.1364/AO.54.001478 ↗
20. Magnetorheological finishing of SiC aspheric mirrors10.1081/AMP-200060417 ↗
21. Subsurface Damage (SSD) Assessment in Ground Silicon Carbide (SiC)10.1364/OFT.2017.OM3B.5 ↗
22. Plasma etching: principles, mechanisms, application to micro- and nano-technologies10.1016/S0169-4332(00)00328-7 ↗
23. Plasma processes at atmospheric and low pressures10.1016/j.vacuum.2008.04.063 ↗
24. A new reactive atom plasma technology (RAPT) for precision machining: the etching of ULE® surfaces10.1002/adem.200600028 ↗
25. The morphology and chemistry evolution of fused silica surface after Ar/CF4 atmospheric pressure plasma processing10.1016/j.apsusc.2013.09.100 ↗
26. Investigation of grinding and lapping surface damage evolution of fused silica by inductively coupled plasma etching10.1007/s12541-019-00142-9 ↗
27. 3D optical microscopes: a basic technology comparison for metrology applications: learn more about 3D techniques such as white light interferometry and confocal microscopy
28. Indiscriminate revelation of dislocations in single crystal SiC by inductively coupled plasma etching10.1016/j.jeurceramsoc.2019.03.026 ↗
29. Etching characteristics of quartz crystal wafers using argon-based atmospheric pressure CF4 plasma stabilized by ethanol addition10.1007/s41871-019-00044-4 ↗
30. A review of SiC reactive ion etching in fluorinated plasmas10.1002/1521-3951(199707)202:1<605::AID-PSSB605>3.0.CO;2-Y ↗
31. Influence of carbon monoxide gas on silicon dioxide dry etching10.1016/0039-6028(95)01313-X ↗
32. Microsecond pulse driven Ar/CF4 plasma jet for polymethylmethacrylate surface modification at atmospheric pressure10.1016/j.apsusc.2014.12.076 ↗
33. Molecular emission of CF4 gas in low-pressure inductively coupled plasma10.5012/bkcs.2006.27.3.373 ↗
34. Analysis of the impact of different additives during etch processes of dense and porous low-k with OES and QMS10.1016/j.mee.2009.08.004 ↗
35. Reactive oxygen species in plasma against E. coli cells survival rate10.1088/1674-1056/24/8/085201 ↗
36. Continuous and modulated deposition of fluorocarbon films from c‐C4F8 plasmas10.1002/ppap.200400021 ↗
37. On the periodicity of fixed-abrasive planetary lapping based on a generic model10.1016/j.jmapro.2019.05.036 ↗
38. Differential etching of ion-implanted garnet10.1063/1.1662031 ↗
39. MRF applications: measurement of process-dependent subsurface damage in optical materials using the MRF wedge technique10.1117/12.638839 ↗
40. Laser annealing of P and Al implanted 4H-SiC epitaxial layers10.3390/ma12203362 ↗
41. Moissanite (SiC) with metal-silicide and silicon inclusions from tuff of Israel: Raman spectroscopy and electron microscope studies10.1016/j.lithos.2017.04.001 ↗
42. Rapid detection of subsurface damage of optical materials in lapping process and its influence regularity10.3321/j.issn:1004-924X.2008.01.004 ↗