journal article·2022-03-01Open access

Localized electrodeposition micro additive manufacturing of pure copper microstructures

Wanfei Ren, Jinkai Xu, Zhongxu Lian, Xiaoqing Sun, Zhenming Xu, Huadong Yu

Abstract

Abstract The fabrication of pure copper microstructures with submicron resolution has found a host of applications, such as 5G communications and highly sensitive detection. The tiny and complex features of these structures can enhance device performance during high-frequency operation. However, manufacturing pure copper microstructures remain challenging. In this paper, we present localized electrochemical deposition micro additive manufacturing (LECD-μAM). This method combines localized electrochemical deposition (LECD) and closed-loop control of atomic force servo technology, which can effectively print helical springs and hollow tubes. We further demonstrate an overall model based on pulsed microfluidics from a hollow cantilever LECD process and closed-loop control of an atomic force servo. The printing state of the micro-helical springs can be assessed by simultaneously detecting the Z-axis displacement and the deflection of the atomic force probe cantilever. The results showed that it took 361 s to print a helical spring with a wire length of 320.11 μm at a deposition rate of 0.887 μm s−1, which can be changed on the fly by simply tuning the extrusion pressure and the applied voltage. Moreover, the in situ nanoindenter was used to measure the compressive mechanical properties of the helical spring. The shear modulus of the helical spring material was about 60.8 GPa, much higher than that of bulk copper (∼44.2 GPa). Additionally, the microscopic morphology and chemical composition of the spring were characterized. These results delineate a new way of fabricating terahertz transmitter components and micro-helical antennas with LECD-μAM technology.
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Research context

OpenAlex topics: Nanowire Synthesis and Applications · 3D IC and TSV technologies · Advancements in Semiconductor Devices and Circuit Design

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (39)

Show source-provided references
1. Printable nanoscopic metamaterial absorbers and images with diffraction-limited resolution10.1021/acsami.6b01585 ↗
2. Experimental study of localized electrochemical deposition of Ni-Cu alloy using a moving anode10.1016/j.procir.2017.12.053 ↗
3. Three-dimensional printing of freeform helical microstructures: a review10.1039/C4NR02041C ↗
4. Direct-write fabrication of freestanding nanocomposite strain sensors10.1088/0957-4484/23/8/085502 ↗
5. Omnidirectional printing of flexible, stretchable, and spanning silver microelectrodes10.1126/science.1168375 ↗
6. Laser-assisted direct ink writing of planar and 3D metal architectures10.1073/pnas.1525131113 ↗
7. Printing of complex free-standing microstructures via laser-induced forward transfer (LIFT) of pure metal thin films10.1016/j.addma.2018.09.028 ↗
8. Crystallinity of inorganic films grown by atomic layer deposition: overview and general trends10.1063/1.4757907 ↗
9. Atomic layer deposition: an overview10.1021/cr900056b ↗
10. Plasmonic helical nanoantenna as a converter between longitudinal fields and circularly polarized waves10.1021/acs.nanolett.0c04948 ↗
11. Three-dimensional microfabrication by localized electrochemical deposition10.1109/84.485212 ↗
12. Theoretical modeling and fabrication of two-dimensional microstructures by using micro-anode-guided electroplating with real-time image processing10.4028/www.scientific.net/KEM.656-657.604 ↗
13. Localized electrochemical deposition of micrometer copper columns by pulse plating10.1016/j.electacta.2009.11.002 ↗
14. A novel electrochemical micro additive manufacturing method of overhanging metal parts without reliance on support structures10.1016/j.promfg.2016.08.081 ↗
15. A review: development of the maskless localized electrochemical deposition technology10.1007/s00170-020-05799-5 ↗
16. Fabrication of metal microfluidic chip mold with coplanar auxiliary cathode in the electroforming process10.1088/1361-6439/aaf605 ↗
17. A study on the effect of interelectrode gap in the electrochemical additive manufacturing process10.1080/10910344.2018.1486419 ↗
18. Fabrication of micro-sized copper columns using localized electrochemical deposition with a 20 μm diameter micro anode10.1149/2.0111903jss ↗
19. A mathematical model of the deposition rate and layer height during electrochemical additive manufacturing10.1007/s00170-019-03292-2 ↗
20. Microscale 3D printing of nanotwinned copper10.1002/adma.201705107 ↗
21. Parallel process 3D metal microprinting10.1002/admt.201800393 ↗
22. Fabrication of 3D microstructure by localized electrochemical deposition with image feedback distance control and five-axis motion platform10.1149/2.0191607jss ↗
23. Meniscus-confined three-dimensional electrodeposition for direct writing of wire bonds10.1126/science.1190496 ↗
24. Local polymer replacement for neuron patterning and in situ neurite guidance10.1021/la5012692 ↗
25. FluidFM: combining atomic force microscopy and nanofluidics in a universal liquid delivery system for single cell applications and beyond10.1021/nl901384x ↗
26. Nanoscale dispensing in liquid environment of streptavidin on a biotin-functionalized surface using hollow atomic force microscopy probes10.1016/j.mee.2008.10.025 ↗
27. Template-free 3D microprinting of metals using a force-controlled nanopipette for layer-by-layer electrodeposition10.1002/adma.201504967 ↗
28. Local surface modification via confined electrochemical deposition with FluidFM10.1039/C5RA07239E ↗
29. Three-dimensional nanoprinting via scanning probe lithography-delivered layer-by-layer deposition10.1021/acsnano.6b01145 ↗
30. Geerlings · Appl. Phys. Lett. · 2015 · 10710.1063/1.4931354 ↗
31. Simultaneous scanning ion conductance microscopy and atomic force microscopy with microchanneled cantilevers10.1103/PhysRevLett.115.238103 ↗
32. Simultaneous scanning ion conductance and atomic force microscopy with a nanopore: effect of the aperture edge on the ion current images10.1063/1.5053879 ↗
33. Dynamic “scanning-mode” meniscus confined electrodepositing and micropatterning of individually addressable ultraconductive copper line arrays10.1021/acs.jpclett.8b00636 ↗
34. Effects of rotor electrode in the fabrication of high aspect ratio microstructures by localized electrochemical deposition10.1088/0960-1317/11/5/301 ↗
35. Electrodeposition-based 3D printing of metallic microarchitectures with controlled internal structures10.1002/smll.201500177 ↗
36. Ultralow flexural properties of copper microhelices fabricated via electrodeposition-based three-dimensional direct-writing technology10.1039/C7NR03803H ↗
37. Vertical, capacitive microelectromechanical switches produced via direct writing of copper wires10.1038/micronano.2016.10 ↗
38. Atomic force microscope-based meniscus-confined three-dimensional electrodeposition10.1002/admt.201900827 ↗
39. Localized pulsed electrodeposition process for three-dimensional printing of nanotwinned metallic nanostructures10.1021/acs.nanolett.7b03930 ↗