journal article·2021-10Open access

Densification of glass powder studied by master sintering curve and master kinetic curve methods

Ali Talimian, Lothar Wondraczek, Dušan Galusek

Abstract

Abstract The master sintering curve method was applied to analyze the sintering and crystallization behavior of 15Na 2 O.10CaO.75SiO 2 (SLS) and 17Na 2 O.33CaO.50SiO 2 (NC 2 S 3 ) glasses, in mol %. The densification of samples was successfully analyzed using the master sintering curve (MSC) method; it gives activation energy Q = 310–340 kJ.mol −1, which is in good agreement with the expected activation energy of the viscous flow. While the obtained activation energy enables predicting the sintering behavior of SLS glass, the actual results are different from the estimated data for NC 2 S 3 . The activation energy of crystallization of NC 2 S 3 , determined by constructing Master Kinetic Curves (MKC) was lower than the sintering activation energy: this impairs the prediction ability of MSC for NC 2 S 3 glass.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Glass properties and applications · Thermal and Kinetic Analysis · Advanced ceramic materials synthesis

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Centre for Functional and Surface Functionalised Glass Alexander Dubcek University of Trencin Trencin Slovakia

Otto Schott Institute of Materials Research University of Jena Jena Germany

Joint Glass Centre of the IIC SAS, TnUAD and FChPT STU Trencin Slovakia

Funding

H2020 Spreading Excellence and Widening Participation · Vedecká Grantová Agentúra MŠVVaŠ SR a SAV

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