journal article·2019-03

Microstructure, grain orientation, and properties of ITO ceramics sintered with various heating rates

Fangsheng Mei, Kai Qin, Fangchao Mei, Tiechui Yuan, Wende Liu, Ruidi Li, Lisan Chen

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Abstract

Abstract In this study, the microstructure, grain orientation, electrical resistivity, nanohardness, and fracture strength were systematically investigated in ITO ceramics sintered with different heating rates. It was found that ITO ceramics sintered at 1600°C consist of main phase (In 2 O 3 ) and secondary phase (In 2 SnO 5 ) and the distributions of coarse grains with high indium content and fine grains with high tin content are interval. The higher heating rate was found to refine the grain size and increase the {1000} textured secondary phase. The increase in electrical resistivity of ITO ceramics was due to the decrease in oxygen vacancies caused by the reducing oxide decomposition. Moreover, the nanohardness of fine grains was found to be higher than that of coarse grains due to the reinforcement effect of Sn element. Besides, the increase of heating rate is beneficial to enhance the fracture strength due to the higher resistance of grain boundary to fracture propagation and the predominantly intergranular fracture.
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Research context

OpenAlex topics: Advanced ceramic materials synthesis · ZnO doping and properties · Electronic Packaging and Soldering Technologies

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Science and Technology on High Strength Structural Materials Laboratory Central South University Changsha China

State Key Laboratory of Powder Metallurgy Central South University Changsha China

Zhuzhou Smelter Group Co. Ltd. Zhuzhou Hunan China

Shanghai Branch of China Southern Airlines Co. Ltd Shanghai China

Funding

Zhuzhou Smelter Group Co., Ltd

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