journal article·2024-10-21Open access

One-Step Magneton Sputtering of Crystalline Cu-Doped TiO2 Coatings: Characterization and Antibacterial Activity

Maria P. Nikolova, Sadegh Yousefi, Yordan Handzhiyski, Margarita D. Apostolova

Applied Sciences· Volume 14· Issue 20

Abstract

Early biofilm formation could be inhibited by applying a thin biocompatible copper coating to reduce periprosthetic infections. In this study, we deposited crystalline Cu-doped TiO2 films using one-step DC magnetron sputtering in an oxygen atmosphere on a biased Ti6Al4V alloy without external heating. The bias voltage varied from −25 V to −100 V, and the resultant substrate temperature was measured. The deposited coatings were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), microhardness, scratch and hydrophilicity tests, potentiodynamic polarization measurements, and antibacterial assays against S. aureus and E. coli. The findings demonstrated that when a higher negative bias is applied, the substrate temperature drops, and the anatase to rutile transformation is initiated without indicating obvious Cu-containing phases. The SEM images of the films showed spherical agglomerates with homogeneously distributed Cu with decreasing Cu content as the bias value increased. Higher bias results in the grain refinement of the thinning coatings with more lattice microstrain and more defects, together with an increase in water contact angles and hardness values. Samples biased at −75 V exhibited the highest adhesive strength between coatings and substrate, whereas the specimen biased at −50 V demonstrated higher corrosion resistance. Cu-containing TiO2 coatings with pure anatase phase composition and Cu concentrations of 2.62 wt.% demonstrated excellent bactericidal activity against both S. aureus and E. coli. The layers containing 2.34 wt.% Cu exhibited very good antibacterial properties against S. aureus, only. According to these findings, the produced copper-doped TiO2 coatings have high bactericidal qualities in vitro and may be used to prepare orthopaedic and dental implants in the future.
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Research context

OpenAlex topics: Nanoparticles: synthesis and applications · ZnO doping and properties · Polymer Nanocomposite Synthesis and Irradiation

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Material Science and Technology, University of Ruse “Angel Kanchev”, 8 Studentska Str., 7017 Ruse, Bulgaria

Ferdows Department of Education (Ministry of Education), Experimental Sciences Teacher, Ferdows 9771853113, Iran

Department of Metallurgy and Materials Science, Semnan University, Semnan 3513119111, Iran

Roumen Tsanev Institute of Molecular Biology, Bulgarian Academy of Sciences, Acad. Georgi Bonchev Str., Bl. 21, 1113 Sofia, Bulgaria

Funding

European Union-Next Generation EU, through the National Recovery and Resilience Plan of the Republic of Bulgaria

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