Crack Propagation Behavior of Fused Silica during Cyclic Indentation under Incremental Loads
Source abstract
Abstract
Fused silica is an important optical material with important applications, where the surface must be precisely machined without subsurface damage. In this study, multi-cyclic indentations under incremental loads were performed on fused silica using two kinds of indenters to clarify the mechanisms of crack generation and propagation induced by precision grinding. It was found that incremental loading cyclic nanoindentation induced various patterns of subsurface cracking and surface spalling. Four kinds of surface spalling were identified at different locations around an indent, the temporal formation mechanisms of which were clarified by microscopic observation and topographical measurement. Load–displacement curve analysis demonstrated that incremental propagation of lateral cracks during early indentation cycles caused large-scale brittle fractures during later cycles. Compared with a Berkovich indenter, a cube-corner indenter caused more significant brittle fractures and surface spalling. The findings in this study will deepen the understanding of subsurface damaging mechanism of fused silica and other brittle solids caused by cyclic tool-workpiece interactions in grinding and other mechanical machining processes.
Source: crossref · Quality: baseline
Research context
OpenAlex topics: Advanced Surface Polishing Techniques · Advanced machining processes and optimization · Metal and Thin Film Mechanics
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
Department of Mechanical Engineering, Faculty of Science and Technology, Keio University, Hiyoshi 3-14-1, Kohoku-ku, Yokohama 223-8522, Japan
School of Mechanical Engineering, Shandong University of Technology, Zibo 255000, China
References (35)
Show source-provided references
1. Manufacturing and measurement of freeform optics10.1016/j.cirp.2013.05.003 ↗
2. Ultra-precision grinding of optical glass lenses with La-doped CeO2 slurry10.1016/j.cirp.2019.04.089 ↗
3. Relationship between subsurface damage and surface roughness of optical materials in grinding and lapping processes10.1016/j.jmatprotec.2007.11.118 ↗
4. Effect of rogue particles on the sub-surface damage of fused silica during grinding/polishing10.1016/j.jnoncrysol.2007.11.015 ↗
5. Evaluating subsurface damage in optical glasses
6. Direct Observation and Analysis of Indentation Cracking in Glasses and Ceramics10.1111/j.1151-2916.1990.tb05119.x ↗
7. 3D analysis of crack morphologies in silicate glass using FIB tomography10.1016/j.jeurceramsoc.2008.05.042 ↗
8. Morphology of Vickers Indent Flaws in Soda-Lime-Silica Glass10.1111/j.1151-2916.2001.tb01015.x ↗
9. A quantitative analysis of the indentation fracture of fused silica10.1111/jace.16645 ↗
10. Indentation cracking and deformation mechanism of sodium aluminoborosilicate glasses10.1111/jace.16894 ↗
11. In situ cube-corner indentation of soda-lime glass and fused silica10.1111/j.1551-2916.2004.01494.x ↗
12. Sub-surface mechanical damage distributions during grinding of fused silica10.1016/j.jnoncrysol.2006.09.012 ↗
13. Crack-free ductile mode grinding of fused silica under controllable dry grinding conditions10.1016/j.ijmachtools.2016.07.007 ↗
14. Effects of local strain rate and temperature on the workpiece subsurface damage in grinding of optical glass10.1016/j.ijmecsci.2020.105737 ↗
15. Effect of grinding wheel spindle vibration on surface roughness and subsurface damage in brittle material grinding10.1016/j.ijmachtools.2015.01.003 ↗
16. On the mechanism of secondary pop-out in cyclic nanoindentation of single-crystal silicon10.1557/jmr.2015.120 ↗
17. New insights into phase transformations in single crystal silicon by controlled cyclic nanoindentation10.1016/j.scriptamat.2015.02.008 ↗
18. Kosai, K., Huang, H., and Yan, J. (2017). Comparative Study of Phase Transformation in Single-Crystal Germanium during Single and Cyclic Nanoindentation. Crystals, 7.10.3390/cryst7110333 ↗
19. Direct observations of multi-cyclic nanoindentation-induced phase transformations in single-crystal Ge10.1088/2053-1591/ab1986 ↗
20. Crack initiation by indentation fatigue in lead alkali and soda-lime glass10.1111/j.1151-2916.1997.tb03183.x ↗
21. Cyclic fatigue of intrinsically brittle ceramics in contact with spheres10.1016/S1359-6454(99)00246-3 ↗
22. Cyclic loading behaviour of soda-lime silicate glass using indentation cracks10.1111/j.1460-2695.1997.tb00326.x ↗
23. Radial fracture during indentation by acute probes: I, description by an indentation wedging model10.1007/s10704-005-6034-9 ↗
24. Radial fracture during indentation by acute probes: II, experimental observations of cube-corner and vickers indentation10.1007/s10704-005-6033-x ↗
25. Sink-in/pile-up formation and crack nucleation mechanisms of high purity fused silica and soda-lime silica glass during nanoindentation experiments10.1016/j.ceramint.2020.06.260 ↗
26. Effect of phase transformations on the shape of the unloading curve in the nanoindentation of silicon10.1063/1.126300 ↗
27. Rate-dependent phase transformations in nanoindented germanium10.1063/1.3151967 ↗
28. Observation of fracture and plastic deformation during indentation and scratching inside the scanning electron microscope10.1016/j.tsf.2004.08.096 ↗
29. The effect of coating cracking on the indentation response of thin hard-coated systems10.1016/S0257-8972(97)00683-X ↗
30. Indentation fracture: Principles and applications10.1007/BF00823224 ↗
31. Elastic/Plastic Indentation Damage in Ceramics: The Lateral Crack System10.1111/j.1151-2916.1982.tb10782.x ↗
32. Mechanical behaviour of fully densified silica glass under Vickers indentation10.1016/j.actamat.2017.03.008 ↗
33. Prediction of subsurface damage depth of ground brittle materials by surface profiling
34. Effect of grinding parameters on surface roughness and subsurface damage and their evaluation in fused silica10.1364/OE.26.004638 ↗
35. Sun, R., Huang, Y., Zhang, X., Zhao, F., Zhang, Y., Liu, J., and Hu, J. (2022, January 27). Study on subsurface damage of fused quartz in grinding stage. Proceedings of the Eighth Symposium on Novel Photoelectronic Detection Technology and Applications, Kunming, China.10.1117/12.2619465 ↗