AFRL Additive Manufacturing Modeling Series: Challenge 4, In Situ Mechanical Test of an IN625 Sample with Concurrent High-Energy Diffraction Microscopy Characterization
Source abstract
Abstract
We describe 3D characterization of an additively manufactured Inconel 625 nickel-base superalloy specimen conducted during a uniaxial tension test using a suite of nondestructive x-ray techniques. High-energy diffraction microscopy in both near- and far-field modalities are employed in situ to track evolution of the material orientation and stress–strain fields at six points during the mechanical test, and these data streams are registered with micro-computed tomography reconstructions which probe the material density. This data volume was matched to a multi-modal serial sectioning characterization of the specimen taken after loading, described in this article’s companion. Twenty-eight grains which were monitored throughout the experiment were selected to form the basis for AFRL AM Modeling Series Challenge 4, Microscale Structure-to-Properties.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Additive Manufacturing Materials and Processes · High Temperature Alloys and Creep · Microstructure and mechanical properties
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References (35)
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1. Ludwig W, King A, Reischig P, Herbig M, Lauridsen EM, Schmidt S, Proudhon H, Forest S, Cloetens P, Rolland du Roscoat S, Buffière JY, Marrow TJ, Poulsen HF (2009) New opportunities for 3D materials science of polycrystalline materials at the micrometre lengthscale by combined use of X-ray diffraction and X-ray imaging. Mater Sci Eng, A 524(1–2):69–76. https://doi.org/10.1016/j.msea.2009.04.00910.1016/j.msea.2009.04.009 ↗
2. Lienert U, Li SF, Hefferan CM, Lind J, Suter RM, Bernier JV, Barton NR, Brandes MC, Mills MJ, Miller MP, Jakobsen B, Pantleon W (2011) High-energy diffraction microscopy at the advanced photon source. JOM 63(7):70–77. https://doi.org/10.1007/s11837-011-0116-010.1007/s11837-011-0116-0 ↗
3. Poulsen H (2012) An introduction to three-dimensional X-ray diffraction microscopy. J Appl Crystallogr 45:1084–1097. https://doi.org/10.1107/S002188981203914310.1107/S0021889812039143 ↗
4. Schuren JC, Shade PA, Bernier JV, Li SF, Blank B, Lind J, Kenesei P, Lienert U, Suter RM, Turner TJ, Dimiduk DM, Almer J (2015) New opportunities for quantitative tracking of polycrystal responses in three dimensions. Curr Opin Solid State Mater Sci 19(4):235–244. https://doi.org/10.1107/S002188981203914310.1107/S0021889812039143 ↗
5. Bernier JV, Suter RM, Rollett AD, Almer JD (2020) High-energy X-ray diffraction microscopy in materials science”. Annu Rev Mater Res 50(1):395–436. https://doi.org/10.1146/annurev-matsci-070616-12412510.1146/annurev-matsci-070616-124125 ↗
6. Pokharel R, Lind J, Li SF, Kenesei P, Lebensohn RA, Suter RM, Rollett AD (2015) In-situ observation of bulk 3D grain evolution during plastic deformation in polycrystalline Cu. Int J Plast 67:217–23410.1016/j.ijplas.2014.10.013 ↗
7. Shade PA, Musinski WD, Obstalecki M, Pagan DC, Beaudoin AJ, Bernier JV, Turner TJ (2019) Exploring new links between crystal plasticity models and high-energy X-ray diffraction microscopy. Curr Opin Solid State Mater Sci 23(5):100793. https://doi.org/10.1016/j.cossms.2019.07.00210.1016/j.cossms.2019.07.002 ↗
8. Miller MP, Pagan DC, Beaudoin AJ, Nygren KE, Shadle DJ (2020) Understanding micromechanical material behavior using synchrotron X-rays and in situ loading. Metall Mater Trans A 51:4360–4376. https://doi.org/10.1007/s11661-020-05888-w10.1007/s11661-020-05888-w ↗
9. Proudhon H, Pelerin M, King A, Ludwig W (2020) In situ 4D mechanical testing of structural materials: the data challenge. Curr Opin Solid State Mater Sci 24(4):100834. https://doi.org/10.1016/j.cossms.2020.10083410.1016/j.cossms.2020.100834 ↗
10. Groeber M (2018) A preview of the U.S. Air Force research laboratory additive manufacturing modeling challenge series. JOM 70(4):441–444. https://doi.org/10.1007/s11837-018-2806-310.1007/s11837-018-2806-3 ↗
11. Cox, M.E., Schwalbach, E.J., Blaiszik, B.J. et al. AFRL Additive Manufacturing Modeling Challenge Series: Overview. Integr Mater Manuf Innov (2021). https://doi.org/10.1007/s40192-021-00215-610.1007/s40192-021-00215-6 ↗
12. Pollock TM, Tin S (2006) Nickel-based superalloys for advanced turbine engines: chemistry, microstructure and properties. J Propul Power 22:361–37410.2514/1.18239 ↗
13. Chapman MG, Shah MN, Donegan SP, Scott JM, Shade PA, Menasche DB, Uchic MD (2021) AFRL Additive manufacturing modeling series: challenge 4, 3D reconstruction of an IN625 high-energy diffraction microscopy sample using multi-modal serial sectioning. Integr Mater Manuf Innov 17:1–20. https://doi.org/10.1007/s40192-021-00212-910.1007/s40192-021-00212-9 ↗
14. Shade PA, Musinski WD, Shah MN, Uchic MD, Donegan SP, Chapman MG, Park JS, Bernier JV, Kenesei P, Menasche DB, Obstalecki M, Schwalbach EJ, Miller JD, Groeber MA, Cox ME (2019) AFRL AM modeling challenge series challenge data package. Mater Data Facility. https://doi.org/10.18126/K5R2-32IU10.18126/K5R2-32IU ↗
15. Shade PA, Menasche DB, Bernier JV, Kenesei P, Park J-S, Suter RM, Schuren JC, Turner TJ (2016) Fiducial marker application method for position alignment of in situ multimodal X-ray experiments and reconstructions. J Appl Crystallogr 49:700–704. https://doi.org/10.1107/S160057671600198910.1107/S1600576716001989 ↗
16. Poulsen HF, Nielsen SF, Lauridsen EM, Schmidt S, Suter RM, Lienert U, Margulies L, Lorentzen T, Juul Jensen D (2001) Threedimensionalmaps of grain boundaries and the stress state ofindividual grains in polycrystals and powders. J. Appl. Cryst. 34:751–756. https://doi.org/10.1107/S002188980101427310.1107/S0021889801014273 ↗
17. Poulsen HF (2004) Three-dimensional X-ray diffraction microscopy: mapping polycrystals and their dynamics. Springer, Berlin10.1007/b97884 ↗
18. Ludwig W, King A, Herbig M, Reischig P, Marrow J, Babout L, Lauridsen EM, Paulson H, Buffire JY (2010) Characterization of polycrystalline materials using synchrotron X-ray imaging and diffraction techniques. JOM 62(12):22–2810.1007/s11837-010-0176-6 ↗
19. Suter RM, Hennessy D, Xiao C, Lienert U (2006) Forward modeling method for microstructure reconstruction using X-ray diffraction microscopy: single-crystal verification. Rev Sci Instrum 10(1063/1):2400017
20. Li SF, Suter RM (2013) Adaptive reconstruction method for three-dimensional orientation imaging. J Appl Crystallogr 46(2):512–524. https://doi.org/10.1107/S002188981300526810.1107/S0021889813005268 ↗
21. Oddershede J, Schmidt S, Poulsen HF, Sørensen HO, Wright J, Reimers W (2010) Determining grain resolved stresses in polycrystalline materials using three-dimensional X-ray diffraction. J Appl Phys 43:539–549. https://doi.org/10.1107/S002188981001296310.1107/S0021889810012963 ↗
22. Bernier JV, Barton NR, Lienert U, Miller MP (2011) Far-field high-energy diffraction microscopy: a tool for intergranular orientation and strain analysis. J Strain Anal Eng Design 46(7):527–547. https://doi.org/10.1177/2F030932471140576110.1177/2F0309324711405761 ↗
23. Shastri SD, Kenesei P, Mashayekhi A, Shade PA (2020) Focusing with saw-tooth refractive lenses at a high-energy X-ray beamline. J Synchrotron Radiat 27(3):590–598. https://doi.org/10.1107/S160057752000366510.1107/S1600577520003665 ↗
24. Lee JH, Almer J, Aydιner C, Bernier JV, Chapman K, Chupas P, Haeffner D, Kump K, Lee PL, Lienert U, Miceli A, Vera G (2007) Characterization and application of a GE amorphous silicon flat panel detector in a synchrotron light source. Nucl Instrum Methods Phys Res, Sect A 582(1):182–184. https://doi.org/10.1016/j.nima.2007.08.10310.1016/j.nima.2007.08.103 ↗
25. Shade PA, Blank B, Schuren JC, Turner TJ, Kenesei P, Goetze K, Suter RM, Bernier JV, Li SF, Lind J, Lienert U, Almer J (2015) A rotational and axial motion system load frame insert for in situ high energy X-ray studies. Rev Sci Instrum 86:093902. https://doi.org/10.1063/1.492785510.1063/1.4927855 ↗
26. https://github.com/joelvbernier/hexrd
27. Lind J, Rollett AD, Pokharel R, Hefferan CM, Li SF, Lienert U, Suter RM (2017) Image processing in experiments on, and simulations of plastic deformation of polycrystals. In: Proceedings of IEEE international conference on image processing. IEEE
28. Li SF. IceNine. https://github.com/FrankieLi/IceNine
29. Menasche DB, Shade PA, Suter RM (2020) Accuracy and precision of near-field high-energy diffraction microscopy forward-model-based microstructure reconstructions. J Appl Crystallogr 53(1):107–11610.1107/S1600576719016005 ↗
30. Wang Y, De Carlo F, Foster I, Insley J, Kesselman C, Lane P, von Laszewski G, Mancini DC, McNulty I, Su M, Tieman B (1999) Quasi-real-time X-ray microtomography system at the advanced photon source. SPIE Proceedings 3772:31810.1117/12.363735 ↗
31. De Carlo F, Albee PB, Chu YS, Mancini DC, Tieman B, Wang SY (2002) High-throughput real-time X-ray microtomography at the advanced photon source. In: SPIE proceedings, volume 450310.1117/12.452840 ↗
32. Menasche DB, Shade PA, Lind J, Li SF, Bernier JV, Kenesei P, Schuren JC, Suter RM (2016) Correlation of thermally induced pores with microstructural features using high energy X-rays. Metall Mater Trans A 47:5580–558810.1007/s11661-016-3712-3 ↗
33. Menasche DB, Lind J, Li SF, Kenesei P, Bingert JF, Lienert U, Suter RM (2016) Shock induced damage in copper: a before and after, three-dimensional study. J Appl Phy 119: https://doi.org/10.1063/1.494727010.1063/1.4947270 ↗
34. Naragani D, Sangid MD, Shade PA, Schuren JC, Sharma H, Park J-S, Kenesei P, Bernier JV, Todd TJ, Parr I (2017) Investigation of fatigue crack initiation from a non-metallic inclusion via high energy X-ray diffraction microscopy. Acta Mater 137:71–84. https://doi.org/10.1016/j.actamat.2017.07.02710.1016/j.actamat.2017.07.027 ↗
35. Cho JH, Rollett AD, Oh KH (2005) Determination of a mean orientation in electron backscatter diffraction measurements. Metall Mater Trans A 36:3427–3438. https://doi.org/10.1007/s11661-005-0016-410.1007/s11661-005-0016-4 ↗