journal article·2019-06

Benchmark Study of Thermal Behavior, Surface Topography, and Dendritic Microstructure in Selective Laser Melting of Inconel 625

Zhengtao Gan, Yanping Lian, Stephen E. Lin, Kevontrez K. Jones, Wing Kam Liu, Gregory J. Wagner

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Abstract

In the NIST additive manufacturing benchmark (AM-Bench) experiments, melt pool geometry, cooling rates, surface topography, and dendritic microstructure in laser melted Inconel 625 were used to challenge and validate computational models of the melting and solidification process. To this end, three thermal models incorporating different physics are compared with the experimental data. It is identified that the heat convection enhanced by the thermocapillary flow inside the melt pool and heat loss caused by vaporization play pivotal roles to guarantee the accuracy of the predictions, and thus should be considered in the thermal model. Neglecting fluid flow and vaporization leads to nearly 100% difference in cooling rate during solidification, and 20% difference in cooling rate after solidification from the results. With the most accurate thermal model, surface topographies of the melt tracks are predicted and quantitatively analyzed. Using the Kurz-Fisher model, the primary dendrite arm spacing is predicted based on the thermal gradient and solidification rate predictions, while elemental segregation is predicted using the Scheil-Gulliver model and a non-equilibrium solidification model. Additionally, it is shown that increasing scan speed inhibits elemental microsegregation.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · Additive Manufacturing and 3D Printing Technologies · High Entropy Alloys Studies

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References (60)

Show source-provided references
1. DebRoy T, Wei H, Zuback J, Mukherjee T, Elmer J, Milewski J, Beese A, Wilson-Heid A, De A, Zhang W (2017) Additive manufacturing of metallic components – process, structure and properties. Prog Mater Sci 92:112–22410.1016/j.pmatsci.2017.10.001 ↗
2. Keller T, Lindwall G, Ghosh S, Ma L, Lane BM, Zhang F, Kattner UR, Lass EA, Heigel JC, Idell Y et al (2017) Application of finite element, phase-field, and CALPHAD-based methods to additive manufacturing of Ni-based superalloys. Acta Mater 139:244– 25310.1016/j.actamat.2017.05.003 ↗
3. Gan Z, Yu G, Li S, He X, Chen R, Zheng C, Ning W (2016) A novel intelligent adaptive control of laser-based ground thermal test. Chin J Aeronaut 29:1018–102610.1016/j.cja.2016.06.015 ↗
4. King WE, Barth HD, Castillo VM, Gallegos GF, Gibbs JW, Hahn DE, Kamath C, Rubenchik AM (2014) Observation of keyhole-mode laser melting in laser powder-bed fusion additive manufacturing. J Mater Process Technol 214:2915–292510.1016/j.jmatprotec.2014.06.005 ↗
5. Pyka G, Burakowski A, Kerckhofs G, Moesen M, Van Bael S, Schrooten J, Wevers M (2012) Surface modification of ti6al4v open porous structures produced by additive manufacturing. Adv Eng Mater 14:363–37010.1002/adem.201100344 ↗
6. AlMangour B, Yang J-M (2016) Improving the surface quality and mechanical properties by shot-peening of 17-4 stainless steel fabricated by additive manufacturing. Mater Des 110:914–92410.1016/j.matdes.2016.08.037 ↗
7. Chen Y, Zhang K, Huang J, Hosseini SRE, Li Z (2016) Characterization of heat affected zone liquation cracking in laser additive manufacturing of Inconel 718. Mater Des 90:586– 59410.1016/j.matdes.2015.10.155 ↗
8. Formenti A, Eliasson A, Mitchell A, Fredriksson H (2005) Solidification sequence and carbide precipitation in Ni-base superalloys in718, in625 and in939. High Temp Mater Process 24:239–25810.1515/HTMP.2005.24.4.239 ↗
9. Smith J, Xiong W, Yan W, Lin S, Cheng P, Kafka OL, Wagner GJ, Cao J, Liu WK (2016) Linking process, structure, property, and performance for metal-based additive manufacturing: computational approaches with experimental support. Comput Mech 57:583–61010.1007/s00466-015-1240-4 ↗
10. Emamian A, Alimardani M, Khajepour A (2012) Correlation between temperature distribution and in situ formed microstructure of Fe–tic deposited on carbon steel using laser cladding. Appl Surf Sci 258:9025–903110.1016/j.apsusc.2012.05.143 ↗
11. Gao W, Zhao S, Wang Y, Zhang Z, Liu F, Lin X (2016) Numerical simulation of thermal field and Fe-based coating doped Ti. Int J Heat Mass Transf 92:83–9010.1016/j.ijheatmasstransfer.2015.08.082 ↗
12. Smith J, Xiong W, Cao J, Liu WK (2016) Thermodynamically consistent microstructure prediction of additively manufactured materials. Comput Mech 57:359–37010.1007/s00466-015-1243-1 ↗
13. Mukherjee T, Wei H, De A, DebRoy T (2018) Heat and fluid flow in additive manufacturing—Part I: modeling of powder bed fusion. Comput Mater Sci 150:304–31310.1016/j.commatsci.2018.04.022 ↗
14. Mukherjee T, Wei H, De A, DebRoy T (2018) Heat and fluid flow in additive manufacturing—Part II: powder bed fusion of stainless steel, and titanium, nickel and aluminum base alloys. Comput Mater Sci 150:369–38010.1016/j.commatsci.2018.04.027 ↗
15. Knapp G, Mukherjee T, Zuback J, Wei H, Palmer T, De A, DebRoy T (2017) Building blocks for a digital twin of additive manufacturing. Acta Mater 135:390–39910.1016/j.actamat.2017.06.039 ↗
16. Qi H, Mazumder J, Ki H (2006) Numerical simulation of heat transfer and fluid flow in coaxial laser cladding process for direct metal deposition. J Appl Phys 100:02490310.1063/1.2209807 ↗
17. Wen S, Shin YC (2011) Modeling of the off-axis high power diode laser cladding process. J Heat Trans 133:03100710.1115/1.4002447 ↗
18. King WE, Anderson AT, Ferencz R, Hodge N, Kamath C, Khairallah SA, Rubenchik AM (2015) Laser powder bed fusion additive manufacturing of metals; physics, computational, and materials challenges. Appl Phys Rev 2:04130410.1063/1.4937809 ↗
19. Panwisawas C, Qiu C, Anderson MJ, Sovani Y, Turner RP, Attallah MM, Brooks JW, Basoalto HC (2017) Mesoscale modelling of selective laser melting: thermal fluid dynamics and microstructural evolution. Comput Mater Sci 126:479–49010.1016/j.commatsci.2016.10.011 ↗
20. Khairallah SA, Anderson AT, Rubenchik A, King WE (2016) Laser powder-bed fusion additive manufacturing: physics of complex melt flow and formation mechanisms of pores, spatter, and denudation zones. Acta Mater 108:36–4510.1016/j.actamat.2016.02.014 ↗
21. Yan W, Ge W, Qian Y, Lin S, Zhou B, Liu WK, Lin F, Wagner GJ (2017) Multi-physics modeling of single/multiple-track defect mechanisms in electron beam selective melting. Acta Mater 134:324–33310.1016/j.actamat.2017.05.061 ↗
22. Lian Y, Lin S, Yan W, Liu WK, Wagner GJ (2018) A parallelized three-dimensional cellular automaton model for grain growth during additive manufacturing. Comput Mech 61:543–55810.1007/s00466-017-1535-8 ↗
23. Rodgers TM, Madison JD, Tikare V (2017) Simulation of metal additive manufacturing microstructures using kinetic monte carlo. Comput Mater Sci 135:78–8910.1016/j.commatsci.2017.03.053 ↗
24. Kundin J, Mushongera L, Emmerich H (2015) Phase-field modeling of microstructure formation during rapid solidification in inconel 718 superalloy. Acta Mater 95:343–35610.1016/j.actamat.2015.05.052 ↗
25. Dantzig JA, Rappaz M (2009) Solidification. EPFL Press10.1201/9781439808030 ↗
26. Liang Y-J, Cheng X, Wang H-M (2016) A new microsegregation model for rapid solidification multicomponent alloys and its application to single-crystal nickel-base superalloys of laser rapid directional solidification. Acta Mater 118:17–2710.1016/j.actamat.2016.07.008 ↗
27. Gan Z, Yu G, He X, Li S (2017) Numerical simulation of thermal behavior and multicomponent mass transfer in direct laser deposition of Co-base alloy on steel. Int J Heat Mass Transf 104:28–3810.1016/j.ijheatmasstransfer.2016.08.049 ↗
28. Parimi LL, Ravi G, Clark D, Attallah MM (2014) Microstructural and texture development in direct laser fabricated in718. Mater Charact 89:102–11110.1016/j.matchar.2013.12.012 ↗
29. Murr LE, Gaytan S, Ceylan A, Martinez E, Martinez J, Hernandez D, Machado B, Ramirez D, Medina F, Collins S et al (2010) Characterization of titanium aluminide alloy components fabricated by additive manufacturing using electron beam melting. Acta Mater 58:1887–189410.1016/j.actamat.2009.11.032 ↗
30. Heigel JC, Lane BM (2018) Measurement of the melt pool length during single scan tracks in a commercial laser powder bed fusion process. J Manuf Sci Eng 140:05101210.1115/1.4037571 ↗
31. Ghosh S, Ma L, Levine LE, Ricker RE, Stoudt MR, Heigel JC, Guyer JE (2018) Single-track melt-pool measurements and microstructures in inconel 625. JOM, 1–610.1007/s11837-018-2771-x ↗
32. Escano LI, Parab ND, Xiong L, Guo Q, Zhao C, Fezzaa K, Everhart W, Sun T, Chen L (2018) Revealing particle-scale powder spreading dynamics in powder-bed-based additive manufacturing process by high-speed x-ray imaging. Sci Rep 8:1507910.1038/s41598-018-33376-0 ↗
33. Zhao C, Fezzaa K, Cunningham RW, Wen H, Carlo F, Chen L, Rollett AD, Sun T (2017) Real-time monitoring of laser powder bed fusion process using high-speed x-ray imaging and diffraction. Sci Rep 7:360210.1038/s41598-017-03761-2 ↗
34. Lyle BL, Levine E (2018) AM-Bench 2018. https://www.nist.gov/ambench/
35. Lyle BL, Levine E (2018) Ambench2018-description. https://www.nist.gov/ambench/amb2018-02-description/
36. Kurz W, Fisher DJ (1986) Fundamentals of solidification, vol 1. trans tech publications Aedermannsdorf, Switzerland
37. Gulliver G (1922) Metal and alloys
38. Gan Z, Liu H, Li S, He X, Yu G (2017) Modeling of thermal behavior and mass transport in multi-layer laser additive manufacturing of ni-based alloy on cast iron. Int J Heat Mass Transfer 111:709–72210.1016/j.ijheatmasstransfer.2017.04.055 ↗
39. Gan Z, Yu G, He X, Li S (2017) Surface-active element transport and its effect on liquid metal flow in laser-assisted additive manufacturing. Int Commun Heat Mass Transfer 86:206–21410.1016/j.icheatmasstransfer.2017.06.007 ↗
40. Bennon W, Incropera F (1987) A continuum model for momentum, heat and species transport in binary solid-liquid phase change systems—I. Model formulation. Int J Heat Mass Transf 30:2161–217010.1016/0017-9310(87)90094-9 ↗
41. He X, DebRoy T, Fuerschbach P (2003) Alloying element vaporization during laser spot welding of stainless steel. J Phys D Appl Phys 36:307910.1088/0022-3727/36/23/033 ↗
42. Cho W-I, Na S-J, Cho M-H, Lee J-S (2010) Numerical study of alloying element distribution in CO2 laser–GMA hybrid welding. Comput Mater Sci 49:792–80010.1016/j.commatsci.2010.06.025 ↗
43. Capriccioli A, Frosi P (2009) Multipurpose ANSYS Fe procedure for welding processes simulation. Fusion Eng Des 84:546–55310.1016/j.fusengdes.2009.01.039 ↗
44. Pawel R, Williams R (1985) Survey of physical property data for several alloys, Technical Report, Oak Ridge National Lab.
45. Kurz W, Fisher D (1981) Dendrite growth at the limit of stability: tip radius and spacing. Acta Metall 29:11–2010.1016/0001-6160(81)90082-1 ↗
46. Lippold J, Sowards J, Murray G, Alexandrov B, Ramirez A (2008) Weld solidification cracking in solid-solution strengthened Ni-base filler metals. In: Hot cracking phenomena in welds II. Springer, pp 147–17010.1007/978-3-540-78628-3_9 ↗
47. Pudar M, Zamberger S, Spiradek-Hahn K, Radis R, Kozeschnik E (2010) Computational analysis of precipitation during continuous casting of microalloyed steel. Steel Res Int 81:372–38010.1002/srin.201000021 ↗
48. Tian Y, McAllister D, Colijn H, Mills M, Farson D, Nordin M, Babu S (2014) Rationalization of microstructure heterogeneity in inconel 718 builds made by the direct laser additive manufacturing process. Metall and Mater Trans A 45:4470–448310.1007/s11661-014-2370-6 ↗
49. Ghosh S, Ma L, Ofori-Opoku N, Guyer JE (2017) On the primary spacing and microsegregation of cellular dendrites in laser deposited Ni–Nb alloys. Modell Simul Mater Sci Eng 25:06500210.1088/1361-651X/aa7369 ↗
50. Hu Y, Lin X, Yu X, Xu J, Lei M, Huang W (2017) Effect of Ti addition on cracking and microhardness of Inconel 625 during the laser solid forming processing. J Alloys Compd 711:267–27710.1016/j.jallcom.2017.03.355 ↗
51. Patankar S (1980) Numerical heat transfer and fluid flow. CRC Press
52. Shepherd J (2002) Overcoming the CFL time-step limitation: a stable iterative implicit numerical scheme for slowly evolving advection-diffusion systems. Ocean Model 4:17–28
53. Tuković ž, Jasak H (2012) A moving mesh finite volume interface tracking method for surface tension dominated interfacial fluid flow. Comput Fluids 55:70–8410.1016/j.compfluid.2011.11.003 ↗
54. Lyle BL, Levine E (2018) AM-Bench 2018-test-data. https://www.nist.gov/ambench/benchmark-test-data/
55. Zhao D, Chaudhury P, Frank R, Jackman L (1994) Flow behavior of three 625-type alloys during high temperature deformation. In: Superalloys 718,625,706 and Various Derivatives. The Minerals, Metals & Materials Society, pp 625–70610.7449/1994/Superalloys_1994_315_329 ↗
56. Heigel JC, Lane BM (2017) The effect of powder on cooling rate and melt pool length measurements using in situ thermographic techniques. In: Solid freeform fabrication 2017
57. Tan Q-M (2011) Dimensional analysis: with case studies in mechanics. Springer Science & Business Media
58. Zhang W, Kim C-H, DebRoy T (2004) Heat and fluid flow in complex joints during gas metal arc welding—Part I: Numerical model of fillet welding. J Appl Phys 95:5210–521910.1063/1.1699485 ↗
59. Kou S (2003) Welding metallurgy. New Jersey, pp 431–446
60. Abbaschian L, Lima MSFd (2003) Cracking susceptibility of aluminum alloys during laser welding. Mater Res 6:273–27810.1590/S1516-14392003000200024 ↗