journal article·2006-08

Mechanochemical synthesis of the low-temperature (B20) phase of FeGe

I. A. Sviridov, L. M. Kubalova, O. Ya. Vasil’eva, V. I. Fadeeva

Inorganic Materials· Volume 42· Issue 8
Publisher page

Abstract

We have investigated solid-state reactions in an equiatomic mixture of Fe and Ge powders during ball milling in a water-cooled high-energy mill under an argon atmosphere. The mechanical alloying products have been characterized by x-ray diffraction, Mössbauer spectroscopy, and calorimetry. The observed sequence of phase formation correlates with the thermodynamic properties of the iron germanides involved. The alloy prepared by ball milling for 2 h consists entirely of nanocrystallites (≃15 nm) of the low-temperature, stable, cubic ( B 20) phase of FeGe.
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Research context

OpenAlex topics: Advanced Materials Characterization Techniques · Semiconductor materials and interfaces · Microstructure and mechanical properties

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