journal article·2023-05

Atmospheric-Pressure Synthesis of Titanium Carbide in an Arc Plasma Reactor

A. A. Gumovskaya, V. V. Shekhovtsov, A. Ya. Pak, R. D. Gerasimov, O. G. Volokitin, G. Ya. Mamontov

Inorganic Materials· Volume 59· Issue 5
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Abstract

Abstract— This paper reports on titanium carbide synthesis in an atmospheric-pressure arc plasma reactor by exposing a stoichiometric starting mixture (Ti : C ~ 1 : 1.05) to a plasma jet. The phase composition of the synthesized TiC powder has been determined as a function of the time during which the starting mixture was exposed to a thermal plasma flow and the current (40–120 A) through the electric arc plasma source. The powders obtained under optimal conditions consist of the cubic titanium carbide phase and have a broad particle size distribution, with distinct agglomerates on the order of 50–100 μm in size. It is worth noting that the surface of the agglomerates has the form of a densified perforated crust (with a pore diameter no greater that 2 μm).
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OpenAlex topics: MXene and MAX Phase Materials · Advanced materials and composites · Metal and Thin Film Mechanics

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