journal article·2021-11-29Open access

Experimental Quantification of the Variability of Mechanical Properties in 3D Printed Continuous Fiber Composites

Clarissa Becker, Hannes Oberlercher, Rosmarie Brigitte Heim, Günter Wuzella, Lisa-Marie Faller, Franz Oswald Riemelmoser, Pascal Nicolay, Frédéric Druesne

Applied Sciences· Volume 11· Issue 23

Abstract

The material properties of 3D printed continuous fiber composites have been studied many times in the last years. However, only a minimal number of samples were used to determine the properties in each of the reported studies. Moreover, reported results can hardly be compared due to different sample geometries. Consequently, the variability of the mechanical properties (from one sample to the other) is a crucial parameter that has not been well quantified yet. In the present work, the flexural properties of 3D printed continuous carbon fiber/nylon composite specimens were experimentally quantified, using batches of 15 test specimens. In order to account for the possible influence of the quality of the prepreg filaments on the observed variability, three different filament rolls were used to manufacture the different batches. Also, two configurations were tested, with a fiber direction parallel (longitudinal) or perpendicular (transverse) to the main axis of the specimens. The results show moderate to high variabilities of the flexural modulus, flexural strength and maximum strain. The coefficient of variation was more than twice as high in the transverse case as in the longitudinal case.
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Research context

OpenAlex topics: Additive Manufacturing and 3D Printing Technologies · Additive Manufacturing Materials and Processes · Innovations in Concrete and Construction Materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

ADMiRE Lab-Additive Manufacturing, Intelligent Robotics, Sensors and Engineering, School of Engineering and IT, Carinthia University of Applied Sciences, Europastrasse 4, 9524 Villach, Austria

Université de Technologie de Compiègne, CNRS, Roberval (Mécanique, Énergie et Électricité), Centre de Recherche Royallieu, CS 60 319, CEDEX, 60 203 Compiègne, France

Competence Center for Wood Composites & Wood Chemistry, Altenberger Straße 69, 4040 Linz, Austria

Carinthia Institute for Smart Materials (CiSMAT), Carinthia University of Applied Sciences, Europastrasse 4, 9524 Villach, Austria

Funding

Interreg program Si-At · Ministère de l’Enseignement Supérieur et de la Recherche

References (63)

Show source-provided references
1. 3D printing of polymer matrix composites: A review and prospective10.1016/j.compositesb.2016.11.034 ↗
2. Fused filament fabrication of fiber-reinforced polymers: A review
3. Additively manufactured carbon fiber-reinforced composites: State of the art and perspective
4. A critical review on 3D printed continuous fiber-reinforced composites: History, mechanism, materials and properties10.1016/j.compstruct.2019.111476 ↗
5. Recent Progress in Additive Manufacturing of Fiber Reinforced Polymer Composite10.1002/admt.201800271 ↗
6. An investigation to study the combined effect of different infill pattern and infill density on the impact strength of 3D printed polylactic acid parts10.1016/j.coco.2020.100605 ↗
7. Three-dimensional printing of continuous-fiber composites by in-nozzle impregnation10.1038/srep23058 ↗
8. Zhang, D., Rudolph, N., and Woytowitz, P. (2019). Reliable Optimized Structures with High Performance Continuous Fiber Thermoplastic Composites From Additive Manufacturing (AM), SAMPE.10.33599/nasampe/s.19.1396 ↗
9. Fabrication of continuous carbon, glass and Kevlar fibre reinforced polymer composites using additive manufacturing
10. Yao, Y., Li, M., Lackner, M., and Herfried, L. (2020). A Continuous Fiber-Reinforced Additive Manufacturing Processing Based on PET Fiber and PLA. Materials, 13.10.3390/ma13143044 ↗
11. Effect of 3D printing process parameters on the impact strength of onyx—Glass fiber reinforced composites
12. Abdullah, F., Okuyama, K.i., Morimitsu, A., and Yamagata, N. (2020). Effects of Thermal Cycle and Ultraviolet Radiation on 3D Printed Carbon Fiber/Polyether Ether Ketone Ablator. Aerospace, 7.10.3390/aerospace7070095 ↗
13. Low-pressure additive manufacturing of continuous fiber-reinforced polymer composites10.1002/pc.25294 ↗
14. Additive manufacturing of continuous fibre reinforced thermoplastic composites using fused deposition modelling: Effect of process parameters on mechanical properties10.1016/j.compscitech.2019.107688 ↗
15. Interface and performance of 3D printed continuous carbon fiber reinforced PLA composites10.1016/j.compositesa.2016.05.032 ↗
16. Optimization of printing parameters of 3D-printed continuous glass fiber reinforced polylactic acid composites10.1016/j.tws.2021.107717 ↗
17. 3D printing of continuous fiber reinforced diamond cellular structural composites and tensile properties10.1016/j.compstruct.2020.112610 ↗
18. 3D printed continuous fibre reinforced composite corrugated structure10.1016/j.compstruct.2017.10.080 ↗
19. 3D printing of composite sandwich structures using continuous carbon fiber and fiber tension10.1016/j.compositesa.2018.07.029 ↗
20. Composite additive manufacturing of morphing aerospace structures10.1016/j.mfglet.2019.12.004 ↗
21. Continuous lattice fabrication of ultra-lightweight composite structures
22. A novel free-hanging 3D printing method for continuous carbon fiber reinforced thermoplastic lattice truss core structures10.1016/j.matdes.2017.10.007 ↗
23. Robotic additive manufacturing system for dynamic build orientations10.1108/RPJ-09-2019-0243 ↗
24. Method for load-capable path planning in multi-axis fused deposition modeling10.1016/j.procir.2019.04.188 ↗
25. FrameFab: Robotic fabrication of frame shapes
26. Development of a Low-Cost Parallel Kinematic Machine for Multidirectional Additive Manufacturing10.1115/1.4028897 ↗
27. Iridescence Print: Robotically Printed Lightweight Mesh Structures10.1089/3dp.2015.0018 ↗
28. Development of a hybrid rapid prototyping system using low-cost fused deposition modeling and five-axis machining10.1016/j.jmatprotec.2014.05.004 ↗
29. Support-free volume printing by multi-axis motion10.1145/3197517.3201342 ↗
30. Process planning for five-axis support free additive manufacturing
31. Investigation of mechanical anisotropy of the fused filament fabrication process via customized tool path generation
32. Zolfagharian, A., Khosravani, M.R., and Kaynak, A. (2020). Fracture Resistance Analysis of 3D-Printed Polymers. Polymers, 12.10.3390/polym12020302 ↗
33. Yerazunis, W.S., Barnwell, J.C., and Nikovski, D.N. (2016, January 8–10). Strengthening ABS, Nylon, and Polyester 3D Printed Parts by Stress Tensor Aligned Deposition Paths and Five-Axis Printing. Proceedings of the Solid Freeform Fabrication 2016: 27th Annual International Solid Freeform Fabrication Symposium, Austin, TX, USA.
34. 3D printing of optimized composites with variable fiber volume fraction and stiffness using continuous fiber10.1016/j.compscitech.2019.107905 ↗
35. Optimization design and 3D printing of curvilinear fiber reinforced variable stiffness composites10.1016/j.compscitech.2020.108502 ↗
36. Performance-driven 3D printing of continuous curved carbon fibre reinforced polymer composites: A preliminary numerical study10.1016/j.compositesb.2018.06.017 ↗
37. Path-designed 3D printing for topological optimized continuous carbon fibre reinforced composite structures10.1016/j.compositesb.2019.107612 ↗
38. Load-dependent path planning method for 3D printing of continuous fiber reinforced plastics10.1016/j.compositesa.2020.106181 ↗
39. Stiffness-based optimization framework for the topology and fiber paths of continuous fiber composites10.1016/j.compositesb.2019.107681 ↗
40. 3D topology optimization of continuous fiber-reinforced structures via natural evolution method10.1016/j.compstruct.2019.02.063 ↗
41. An investigation into 3D printing of fibre reinforced thermoplastic composites
42. Characterization of mechanical properties and fracture mode of additively manufactured carbon fiber and glass fiber reinforced thermoplastics10.1016/j.matdes.2017.10.021 ↗
43. 3D compaction printing of a continuous carbon fiber reinforced thermoplastic10.1016/j.compositesa.2020.105985 ↗
44. Evaluation of compressive and flexural properties of continuous fiber fabrication additive manufacturing technology
45. 3D printed continuous CF/PA6 composites: Effect of microscopic voids on mechanical performance10.1016/j.compscitech.2020.108077 ↗
46. McDowell, D.L., Panchal, J.H., Choi, H.J., Seepersad, C.C., Allen, J.K., and Mistree, F. (2010). Robust Design of Materials—Design Under Uncertainty. Integrated Design of Multiscale, Multifunctional Materials and Products, Elsevier.10.1016/B978-1-85617-662-0.00006-5 ↗
47. Sindinger, S.L., Marschall, D., Kralovec, C., and Schagerl, M. (2021). Structural Response Prediction of Thin-Walled Additively Manufactured Parts Considering Orthotropy, Thickness Dependency and Scatter. Materials, 14.10.3390/ma14092463 ↗
48. International Organization for Standardization (2012). ISO 527-1:2012, Plastics— Determination of Tensile Properties—Part 1: General Principles, ISO.
49. International Organization for Standardization (2009). ISO 527-5:2009, Plastics—Determination of Tensile Properties—Part 5: Test Conditions for Unidirectional Fibre-Reinforced Plastic Composites, ISO.
50. Markforged (2020). Product Specifiactions Mark Two, Markforged.
51. Markforged (2021). Material Datasheet Composites, Markforged.
52. International Organization for Standardization (1998). ISO 14125:1998, Fibre-Reinforced Plastic Composites—Determination of Flexural Properties, ISO.
53. Markforged (2021). Eiger Slicing Software, Markforged.
54. Heim, R.B. (2020). Mikrostrukturelle Analyse Eines Additiv Gefertigten Endlosfaserverbundwerkstoffes. [Bachelor’s Thesis, Carinthia University of Applied Sciences].
55. ZwickRoell GmbH & Co (2020). KG. Product Information—Materials Testing Machines AllroundLine Z005 to Z100, ZwickRoell GmbH & Co.KG.
56. International Organization for Standardization (2018). ISO 7500-1:2018, Metallic Materials—Calibration and Verification of Static Uniaxial Testing Machines—Part 1: Tension/Compression Testing Machines—Calibration and Verification of the Force-Measuring System, ISO.
57. ZwickRoell GmbH & Co.KG (2018). Testing Software testXpert® II. Intelligent and Reliable, ZwickRoell GmbH & Co.KG.
58. Schürmann, H. (2007). Konstruieren mit Faser-Kunststoff-Verbunden: Mit 39 Tabellen, Springer.10.1007/978-3-540-72190-1 ↗
59. Zeiss (2017). Axio Lab.A1-Materials Brochure, Zeiss.
60. dhs Dietermann & Heuser Solution GmbH (2010). Article Description Pixel-Fox (V4), dhs Dietermann & Heuser Solution GmbH.
61. Struers (2016). VersoCit-2-Instructions, Struers.
62. Mark3D (2021). Markforged Desktop Series, Mark3D.
63. ASTM International (2007). ASTM D7264/D7264M-07, Standard Test Method for Flexural Properties of Polymer Matrix Composite Materials, ASTM International.