journal article·2022-09-09Open access

Microstructure, Flexural Strength, and Fracture Toughness Comparison between CAD/CAM Milled and 3D-Printed Zirconia Ceramics

Min-Su Kim, Min-Ho Hong, Bong-Ki Min, Young-Kyung Kim, Hyun-Jun Shin, Tae-Yub Kwon

Applied Sciences· Volume 12· Issue 18

Abstract

The present study comprehensively compared the microstructure, flexural strength, and fracture toughness of zirconia ceramics prepared via two different methods, subtractive milling (SM) and stereolithography (SLA). Disc- or rectangular-shaped zirconia specimens (Prettau (SM) and 3DMix Zirconia (SLA)) were prepared following each manufacturer’s instructions and polished. The microstructures of the two different zirconia specimens were studied by scanning electron microscopy, X-ray diffractometry, energy-dispersive X-ray spectroscopy, and electron backscattered diffractometry. The flexural strength and fracture toughness based on the indentation fracture method were measured for the two different zirconia ceramics. A greater number of small pores and smaller grains were found in the SLA specimen than in the SM specimen. The crystal structure and microstructure analysis revealed that both ceramics had a similar phase composition to each other. No significant differences in flexural strength (p = 0.242) or fracture toughness (p = 0.101) were detected between the two ceramics. The mean flexural strength of the SLA-fabricated zirconia as well as the SM zirconia satisfied the class 5 criteria (>800 MPa) in the ISO 6872 standard.
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Research context

OpenAlex topics: Additive Manufacturing and 3D Printing Technologies · Dental materials and restorations · Injection Molding Process and Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Dental Science, Graduate School, Kyungpook National University, 2177 Dalgubeol-daero, Jung-gu, Daegu 41940, Korea

Department of Dental Laboratory Science, College of Health Sciences, Catholic University of Pusan, 57 Oryundae-ro, Geumjeong-gu, Busan 46252, Korea

Center for Research Facilities, Yeungnam University, 280 Daehak-ro, Gyeongsan 38541, Korea

Department of Conservative Dentistry, School of Dentistry, Kyungpook National University, 2177 Dalgubeol-daero, Jung-gu, Daegu 41940, Korea

Division of Mechanical Engineering Technology, Yeungnam University College, 170 Hyeonchung-ro, Nam-gu, Daegu 42415, Korea

Department of Dental Biomaterials, School of Dentistry and Institute for Biomaterials Research & Development, Kyungpook National University, 2177 Dalgubeol-daero, Jung-gu, Daegu 41940, Korea

Funding

National Research Foundation of Korea (NRF)

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