journal article·2021-02

BaZrO3 dopant interactions during MgB2 wire formation by modified internal magnesium diffusion process

A. Rosová, I. Maťko, E. Dobročka

Applied Physics A· Volume 127· Issue 2
Publisher page

Abstract

Undoped and BaZrO3 nanopowder-doped MgB2/Nb/Cu single filament wires were prepared by modified internal magnesium diffusion (IMD) process using 0, 2 and 5 wt% BaZrO3 addition in amorphous B powder. Superconducting MgB2 phase was formed during heat treatment at temperatures from 650 to 670 °C. The wire microstructure was analysed using XRD, SEM, TEM and EDS to study BaZrO3 dopant interaction with Mg and B precursors during the heat treatment and effect of dopant on MgB2 superconductor. The BaZrO3 nanopowder decomposed and its products reacted with Mg and B producing relatively large BaB6 grains and nanograins of ZrB2 and MgO phases which were not detected by conventional XRD measurements due to their low grain size. Measured MgB2 lattice parameters varied with the dopant addition and heat treatment temperature. Different possible origins of MgB2 lattice deformation were discussed, and it was shown that Zr substitution in MgB2 lattice could not cause this deformation.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Superconductivity in MgB2 and Alloys · Physics of Superconductivity and Magnetism · Boron and Carbon Nanomaterials Research

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (45)

Show source-provided references
1. I. Marino, A. Pujana, G. Sarmiento, S. Sanz, J.M. Merino, M. Tropeano, J. Sun, T. Canosa, Lightweight MgB2 superconducting 10 MW wind generator. Supercond. Sci. Technol. 29, 024005 (2016)10.1088/0953-2048/29/2/024005 ↗
2. D. Patel et al., Evaluation of a solid nitrogen impregnated MgB2 racetrack coil. Supercond. Sci. Technol. 31, 105010 (2018)10.1088/1361-6668/aad9e0 ↗
3. A. Ballarino, R. Flükiger, Status of MgB2 wire and cable applications in Europe. J. Phys. Conf. Ser. 871, 012098 (2017)10.1088/1742-6596/871/1/012098 ↗
4. D. Wang, Y. Ma, Ch. Yao, D. Xu, X. Zhang, S. Awaji, Transport properties of multifilament MgB2 long wires and coils prepared by internal Mg diffusion process. Supercond. Sci. Technol. 30, 064003 (2017)10.1088/1361-6668/aa6675 ↗
5. P. Kováč, L. Kopera, M. Hain, E. Martinez, J. Kováč, T. Melišek, D. Berek, I. Hušek, MgB2 cables made of thin wires manufactured by IMD process. Supercond. Sci. Technol. 33, 085004 (2020)10.1088/1361-6668/ab9520 ↗
6. L. Kopera, P. Kováč, J. Kováč, T. Melišek, I. Hušek, D. Berek, Small diameter wind and react coil made of anodised Al-sheathed MgB2 wire. Supercond. Sci. Technol. 32, 105003 (2019)10.1088/1361-6668/ab3301 ↗
7. D.Y. Wang, X.F. Pan, D. Xi, Q.Y. Wang, J.Q. Feng, G. Yan, Y. Zhao, Development and superconducting properties of practical 18- and 30-Filamentary MgB2 long wires with twisting by the in situ way. J. Spercond. Nov. Magn. 33, 2657 (2020)10.1007/s10948-020-05536-9 ↗
8. S. Sanz, T. Arlaban, R. Manzanas, M. Tropeano, R. Funke, P. Kováč, Y. Yang, H. Newmann, B. Mondsert, Superconducting light generator for large offshore wind turbines. J. Phys. Conf. Ser. 507, 032040 (2014)10.1088/1742-6596/507/3/032040 ↗
9. M. Avdeev, J.D. Jorgensen, R.A. Ribeiro, S.L. Budko, P.C. Canfield, Crystal chemistry of carbon-substituted MgB2. Physica C 387, 301 (2003)10.1016/S0921-4534(03)00722-6 ↗
10. S. Lee, T. Masui, A. Yamamoto, H. Uchiyama, S. Tajima, Crystal growth of C-doped MgB2 superconductors: accidental doping and inhomogeneity. Physica C 412–414, 31 (2004)10.1016/j.physc.2004.01.036 ↗
11. A. Wisniewski, R. Puzniak, J. Judek, C. Krutzler, M. Eisterer, H.W. Weber, J. Jun, S.M. Kazakov, J. Karpinski, Comparison of the influence of carbon substitution and neutron-induced defects on the upper critical field and flux pinning in MgB2 single crystals. Supercond. Sci. Technol. 20, 256 (2007)10.1088/0953-2048/20/3/025 ↗
12. K.S.B. De Silva, X. Xu, X.L. Wang, D. Wexler, D. Attard, F. Xiang, S.X. Dou, A significant improvement in the superconducting properties of MgB2 by co-doping with graphene and nano-SiC. Scripta Mater. 67, 802 (2012)10.1016/j.scriptamat.2012.07.014 ↗
13. A.G. Bhagurkar, A. Yamamoto, L. Wang, M. Xia, A.R. Dennis, J.H. Durrell, T.A. Aljohani, N.H. Babu, D.A. Cardwell, High trapped fields in C-doped MgB2 bulk superconductors fabricated by infiltration and growth process. Sci. Rep. 8, 13320 (2018)10.1038/s41598-018-31416-3 ↗
14. J. Karpinski, Synthesis, substitutions and properties of MgB2 single crystals, in MgB2 superconducting wires, ed.by R. Flükiger (World Scientific Publishing, 2016), p. 3310.1142/9789814725590_0002 ↗
15. J.Y. Xiang, D.N. Zheng, J.Q. Li, S.L. Li, H.H. Wen, Z.X. Zhao, Effect of Al doping on the superconducting and structural properties of MgB2. Physica C 386, 611 (2003)10.1016/S0921-4534(02)02175-5 ↗
16. A.J. Zambano, A.R. Moodenbaugh, L.D. Cooley, Effects of different reactions on composition homogeneity and superconducting properties of Al-doped MgB2. Supercond. Sci. Technol. 18, 1411 (2005)10.1088/0953-2048/18/11/001 ↗
17. H.L. Xu et al., Investigation on MgB2 superconductor doped by nano-Al powder. Physica C 449, 53 (2006)10.1016/j.physc.2006.06.050 ↗
18. Y.G. Zhao et al., Effect of Li doping on structure and superconducting transition temperature of Mg1-xLixB2. Physica C 361, 91 (2001)10.1016/S0921-4534(01)00907-8 ↗
19. S.M. Kazakov, M. Angst, J. Karpinski, I.M. Fita, R. Puzniak, Substitution effect of Zn and Cu in MgB2 on Tc and structure. Solid State Commun. 119, 1 (2001)10.1016/S0038-1098(01)00207-1 ↗
20. R.J. Cava, H.W. Zandbergen, K. Inumaru, The substitutional chemistry of MgB2. Physica C 385, 8 (2003)10.1016/S0921-4534(02)02327-4 ↗
21. C.H. Cheng et al., Chemical doping effect on the crystal structure and superconductivity of MgB2, Physica C 386, 588 (2003)10.1016/S0921-4534(02)02167-6 ↗
22. J.-C. Grivel, Influence of iridium doping in MgB2 superconducting wires. Physica C 547, 7 (2018)10.1016/j.physc.2018.01.002 ↗
23. Y. Feng, Y. Zhao, Y.P. Sun, F.C. Liu, B.Q. Fu, L. Zhou, C.H. Cheng. N. Koshizuka, M. Murakami, Improvement of critical current density in MgB2 superconductors by Zr doping at ambient pressure. Appl. Phys. Lett. 79, 3983 (2001)10.1063/1.1426264 ↗
24. M. Bhatia, M.D. Sumption, E.W. Collings, S. Dregia, Increases in the irreversibility field and the upper critical field of bulk MgB2 by ZrB2 addition. Appl. Phys. Lett. 87, 042505 (2005)10.1063/1.2001736 ↗
25. M.A. Susner, M.D. Sumption, A. Takase, E.W. Collings, Evidence for Zr site-substitution for Mg in PLD-deposited MgB2 thin films, Supercond. Sci. Technol. 27, 075009 (2014)10.1088/0953-2048/27/7/075009 ↗
26. B. Brunner, P. Kováč, A. Rosová, M. Reissner, E. Dobročka, Properties of MgB2 wires doped with BaZrO3 nanopowder made by a modified internal magnesium diffusion process. Supercond. Sci. Technol. 30, 115003 (2017)
27. T. Horide, T. Kitamura, A. Ichinose, K. Matsumoto, Elastic strain evolution in nonocomposite structure of YBa2Cu3O7 + BaZrO3 superconducting films. Jpn. J. Appl. Phys. 53, 083101 (2014)10.7567/JJAP.53.083101 ↗
28. J. Lee et al., High critical current density over 1 MAcm-2 at 13 T in BaZrO3 incorporated Ba(Fe,Co)2As2 thin film. Supercond. Sci. Technol. 30, 085006 (2017)10.1088/1361-6668/aa73f5 ↗
29. Sh. Chen et al., Generating mixed morphology BaZrO3 artificial pinning centers for strong and isotropic pinning in BaZrO3-Y2O3 double-doped YBCO thin films. Supercond. Sci. Technol. 30, 125011 (2017)10.1088/1361-6668/aa902f ↗
30. P. Kováč, I. Hušek, A. Rosová, M. Kulich, J. Kováč, T. Melišek, L. Kopera, M. Balog, P. Krížik, Ultra-lightweight superconducting wire based on Mg, B, Ti and Al. Sci. Rep. 8, 11229 (2018)10.1038/s41598-018-29354-1 ↗
31. A. Rosová, I. Hušek, M. Kulich,.T. Melišek, P. Kováč, E. Dobročka, L. Kopera, J. Scheiter, W. Häβler, Microstructure of undoped and C-doped MgB2 wiresprepared by an internal magnesium diffusion technique using different B powders. J. Alloys Comp. 764, 437 (2018)10.1016/j.jallcom.2018.06.108 ↗
32. A. Rosová, M. Kulich, P. Kováč, B. Brunner, J. Scheiter, W. Häßler, The effect of boron powder on the microstructure of MgB2 filaments prepared by the modified internal magnesium technique. Supercond. Sci. Technol. 30, 055001 (2017)10.1088/1361-6668/aa60f5 ↗
33. A. Rosová, I. Hušek, P. Kováč, E. Dobročka, T. Melišek, Microstructure of MgB2 superconducting wire prepared by internal magnesium diffusion process. J. Alloys Comp. 619, 726 (2015)10.1016/j.jallcom.2014.08.180 ↗
34. G. Giunchi, C. Orecchia, L. Malpezzi, N. Masciochci, Analysis of the minority crystalline phases in bulk superconducting MgB2 obtained by reactive liquid Mg infiltration. Physica C 433, 182 (2006)10.1016/j.physc.2005.10.015 ↗
35. J.L. Lábár, Electron diffraction based analysis of phase fractions and texture in nanocrystalline thin films, Part I. Microsc. Microanal. 14, 287 (2008)10.1017/S1431927608080380 ↗
36. J.L. Lábár, Electron diffraction based analysis of phase fractions and texture in nanocrystalline thin films, Part II. Microsc. Microanal. 15, 20 (2009)10.1017/S1431927609090023 ↗
37. A. Rosová, P. Kováč, I. Hušek, B. Brunner, E. Dobročka, Microstructure of MgB2 superconducting wire prepared by internal magnesium diffusion and in-situ powder-in-tube processes – Secondary phase intragrain nanolayers as an oxygen content indicator. Physica C 516, 1 (2015)10.1016/j.physc.2015.05.010 ↗
38. J.D. DeFouw, D.C. Dunand, Mechanisms and kinetics of MgB2 synthesis from boron fibers. Acta Mater. 56, 5751 (2008)10.1016/j.actamat.2008.07.049 ↗
39. P. Kováč, I. Hušek, T. Melišek, L. Kopera, M. Kulich. Fast creation of dense MgB2 phase in wires made by IMD process, Supercond. Sci. Technol. 29(10), 10LT01 (2016)10.1088/0953-2048/29/10/10LT01 ↗
40. K. Torkar, H. Krischen, E. Hitsch, Darstellung und Identifizierung von Bariumdiborid. Monath. Chem. 103, 744 (1972)10.1007/BF00905433 ↗
41. D.G. Hinks, J.D. Jorgensen, H. Zheng, S. Short, Synthesis and stoichiometry of MgB2. Physica C 382, 166 (2002)10.1016/S0921-4534(02)01842-7 ↗
42. N.D. Zhigadlo, S. Katrych, J. Karpinski, B. Batlogg, Influence of Mg deficiency on crystal structure and superconducting properties in MgB2 single crystals. Phys. Rev. B 81, 054520 (2010)10.1103/PhysRevB.81.054520 ↗
43. A. Serquis, Y.T. Zhu, E.J. Peterson, J.Y. Coulter, D.E. Peterson, F.M. Mueller, Effect of lattice strain and defects on superconductivity of MgB2. Appl. Phys. Lett. 79, 4399 (2001)10.1063/1.1428109 ↗
44. E.W. Collings, M.D. Sumption, M. Bhatia, M. Susuner, S.D. Bohnenstiehl, Prospects for improving the intrinsic and extrinsic properties of magnesium diboride superconducting strands. Supercond. Sci. Technol. 21, 103001 (2008)10.1088/0953-2048/21/10/103001 ↗
45. R. Zeng et al., Stress/strain induced flux pinning in highly dense MgB2 bulks. IEEE Trans. Appl. Supercond. 19, 2722 (2009)10.1109/TASC.2009.2019577 ↗