journal article·2018-07

Synthesis of highly dispersed silicon carbide powders by a solvothermal-assisted sol–gel process

Hongmei Chen, Jinming Jiang, Huayu Zhao

Applied Physics A· Volume 124· Issue 7
Publisher page

Abstract

Highly dispersed silicon carbide powders were prepared by a solvothermal-assisted sol–gel process with tetraethyl orthosilicate and phenolic resin as starting materials and carbothermal reduction reactions at a relatively low temperature (1400–1600 °C). Investigated by X-ray diffraction, transmission electron microscopy, scanning electron microscope and the nitrogen adsorption–desorption isotherm measurements, the obtained SiC powders had an average crystallite size of 200 nm and high specific surfaces areas of 149 m2/g. Besides, mechanism for preparation of highly dispersed SiC powders was proposed.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · Diamond and Carbon-based Materials Research

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (25)

Show source-provided references
1. K. Suzuki, M. Sasaki, Microstructure and mechanical properties of liquid-phase-sintered SiC with AlN and Y2O3 additions. Ceram. Int. 31, 749–755 (2005)10.1016/j.ceramint.2004.08.014 ↗
2. J. David, G. Trolliard, A. MaÎtre, Transmission electron microscopy study of the reaction mechanisms involved in the carbothermal reduction of anatase. Acta. Mater. 61, 5414–5428 (2013)10.1016/j.actamat.2013.05.030 ↗
3. K. Yamada, N. Kamiya, S. Wada, Abrasive wear of Al2O3–SiC composites. J. Ceram. Soc. Jpn. Int. Ed. 99, 797–800 (1991)
4. Y. Xiang, W. Li, S. Wang, Z.H. Chen, Oxidation behavior of oxidation protective coatings for PIP-C/SiC composites at 1500 °C. Ceram. Int. 38, 9–13 (2012)10.1016/j.ceramint.2011.06.063 ↗
5. W. Li, Y. Xiang, S. Wang, Y. Ma, Z.H. Chen, Ablation behavior of three-dimensional braided C/SiC composites by oxyacetylene torch under different environments. Ceram. Int. 39, 463–468 (2013)10.1016/j.ceramint.2012.06.049 ↗
6. N. Ekinaga, Characteristics of SiC whisker and their applications, in Proceedings of the 1st Japan International SAME Symposium, pp. 883–888, (1989)
7. S. Ogihara, K. Maeda, Y. Takeda, K. Nakamura, Effect of impurity and carrier concentrations on electrical resistivity and thermal conductivity of SiC ceramics containing BeO. J. Am. Ceram. Soc. 68, 16–18 (1985)10.1111/j.1151-2916.1985.tb15257.x ↗
8. A. Najafi, F. Golestani-Fard, H.R. Rezaie, N. Ehsani, A study on sol–gel synthesis and characterization of SiC nanopowders. J. Sol–Gel Sci. Techn. 59, 205–214 (2011)10.1007/s10971-011-2482-z ↗
9. H.P. Martin, R. Ecke, E. Müller, Synthesis of nanocrystalline silicon carbide powder by carbothermal reduction. J. Eur. Ceram. Soc. 18, l737-l742 (1998)
10. A. Najafi, F. Golestani-Fard, H.R. Rezaie, N. Ehsani, Synthesis and characterization of SiC nano powder with low residual carbon processed by sol–gel method. Powder Technol. 219, 202–210 (2012)10.1016/j.powtec.2011.12.045 ↗
11. B. Li, Y.C. Song, C.R. Zhang, J.S. Yu. Synthesis and characterization of nanostructured silicon carbide crystal whiskers by sol–gel process and carbothermal reduction. Ceram. Int. 40, 12613–12616 (2014)10.1016/j.ceramint.2014.04.099 ↗
12. F. Lusquinos, J. Pou, F. Quintero, M. Perez-Amor, Laser cladding of SiC/Si composite coating om Si–SiC ceramic substrates. Surf. Coat. Techol. 202, 1588–1593 (2008)10.1016/j.surfcoat.2007.07.011 ↗
13. X.H. Wang, A. Yamamoto, K. Eguchi et al., Thermoelectric properties of SiC thick films deposited by thermal plasma physical vapor deposition. Sci. Technol. Adv. Mater. 4, 167–172 (2003)10.1016/S1468-6996(03)00015-9 ↗
14. H.R. Orthner, R. Tomasi, W.J. Botta, Reaction sintering of titanium carbide and titanium silicide prepared by high-energy milling. Mater. Sci. Eng. A. 336, 202–208 (2002)10.1016/S0921-5093(01)01963-3 ↗
15. Y. Xiang, Y. Li, F. Cao, The degradation behavior of SiC coated PIP–C/SiC composites in thermal cycling environment. Compos. B 79, 204–208 (2015)10.1016/j.compositesb.2015.04.028 ↗
16. L. Zhao, X.F. Chen, X.C. Wang, Y.J. Zhang, W. Wei, Y.H. Sun et al., One-step solvothermal synthesis of a carbon@TiO2 Dyade structure effectively promoting visible-light photocatalysis. Adv. Mater. 22, 3317–3321 (2010)10.1002/adma.201000660 ↗
17. S.K. Liu, Z. Chen, K. Xie, Y. Li, J. Xu, C. Zheng, A facile one-step hydrothermal synthesis of a-Fe2O3 nanoplates imbedded in graphene networks with high-rate lithium storage and long cycle life. J. Mater. Chem. A. 2, 13942–13948 (2014)10.1039/C4TA03152K ↗
18. X.F. Ma, X. Huang, Z. Kang, G.J. Zhang, H.J. Luo. One-pot syntheses and characterization of zirconium carbide microspheres by carbon microencapsulation. Ceram. Int. 41, 6740–6746 (2015)10.1016/j.ceramint.2015.01.118 ↗
19. M.J. Mayo, Processing of nanocrystalline ceramics from ultrafine particles. Int. Mater. Rev. 41, (85–115 (1996)10.1179/imr.1996.41.3.85 ↗
20. W.W. Alan, J.N. Kevin, A.C. Gene, P.R. Raymoud, Kinetics of carbothermal reduction synthesis of beta silicon carbide. AICHE. J. 39, 493–503 (1993)10.1002/aic.690390311 ↗
21. W.S. Seo, K. Koumoto, Stacking faults in β-SiC formed during carbothermal reduction of SiO2. J. Am. Ceram. Soc. 79, (1777–1782 (1996)10.1111/j.1151-2916.1996.tb07995.x ↗
22. J.M. Jiang, S. Wang, W. Li., Z.H. Chen, Low-temperature synthesis of tantalum carbide by facile one-pot reaction. Ceram. Int. 42, 7118–7124 (2016)10.1016/j.ceramint.2016.01.100 ↗
23. L. Sun, M.J. Annen, F. Lorenzano-Porras, P.W. Carr, A.V. Mccormick, Synthesis of porous zirconia spheres for HPLC by polymerization-induced colloid aggregation (PICA). Acta Sedimentologica Sinica. 163, (464–473) (2004)
24. W.T. Xu, Y.F. Zhou, D.C. Huang, M.X. Yang, C. Yu, K. W, et al. Synthesis and pyrolysis evolution of glucose-derived hydrothermal precursor for nanosized zirconium carbide. Ceram. Int. 42, 10655–10663 (2016)10.1016/j.ceramint.2016.03.171 ↗
25. F.F. Wang, D.P. Xiang, Y.W. Wang, J.B. Li, Rapid synthesis of SiC powders by spark plasma-assisted carbothermal reduction reaction. Ceram. Int. 43, 4970–4975 (2017)10.1016/j.ceramint.2017.01.003 ↗