journal article·2021-04-27Open access

Density, hardness and strength properties of densified fir and aspen woods pretreated with water repellents

Hüseyin Pelit, Fatih Emiroglu

Holzforschung· Volume 75· Issue 4

Abstract

Abstract In this study, the effect of thermo-mechanical densification on the density, hardness, compression strength, bending strength (MOR), and modulus of elasticity (MOE) of fir and aspen wood pretreated with water repellents was analyzed. Wood specimens were impregnated with paraffin, linseed oil and styrene after pre-vacuum treatment. Then, the impregnated wood specimens were densified with compression ratios of 20 and 40%, and at 120, 150 and 180 °C. The results indicated that the density, hardness and strength properties of the all densified specimens (untreated and impregnated) increased depending on the compression ratio and temperature. For all tested properties, higher increases were obtained in the paraffin and styrene pretreated specimens compared to untreated samples. However, the increase rates in linseed oil pretreated specimens were generally lower than untreated specimens. Regarding water repellents the most successful results in all tested properties were determined in styrene pretreated specimens. The density, hardness and strength properties of all specimens increased with the increase in compression ratio. On the other hand, the increase in the compression temperature negatively affects the properties of untreated and linseed oil pretreated specimens, while having a generally positive effect on the properties of paraffin pretreated specimens. However, all tested properties of styrene pretreated specimens have increased significantly due to the increase in compression temperature. The increasing strength properties of wood as a result of densification have increased much more with paraffin and especially styrene pretreatment. These combinations can be considered as an important potential for applications that require more hardness and strength.
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Research context

OpenAlex topics: Wood Treatment and Properties · Natural Fiber Reinforced Composites · Tree Root and Stability Studies

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Wood Products Industrial Engineering , Faculty of Technology, Duzce University , 81620, Duzce , Turkey

Doğtaş Kelebek Furniture Industry and Trade Inc , 81620, Duzce , Turkey

Funding

Duzce University

References (49)

Show source-provided references
1. ASTM D 1413-76 (1976). Standard test method of testing wood preservatives by laboratory soilblock cultures. Annual Book of ASTM Standard.
2. Báder, M., Bak, M., Németh, R., Rousek, R., Horníček, S., Dömény, J., Klímek, P., Rademacher, P., Kudela, J., Sandberg, D., et al. (2018). Wood densification processing for newly engineered materials. In: 5th International conference on processing technologies for the forest and bio-based products industries (PTF BPI 2018), Freising/Münich, Germany, pp. 255–263.
3. Bekhta, P., Proszyk, S., Lis, B., and Krystofiak, T. (2014). Gloss of thermally densified alder (Alnus glutinosa Goertn.), beech (Fagus sylvatica L.), birch (Betula verrucosa Ehrh.), and pine (Pinus sylvestris L.) wood veneers. Eur. J. Wood Wood Prod. 72: 799–808. https://doi.org/10.1007/s00107-014-0843-3.10.1007/s00107-014-0843-3 ↗
4. Bekhta, P., Salca, E.A., and Lunguleasa, A. (2020). Some properties of plywood panels manufactured from combinations of thermally densified and non-densified veneers of different thicknesses in one structure. J. Build. Eng. 101116. https://doi.org/10.1016/j.jobe.2019.101116.10.1016/j.jobe.2019.101116 ↗
5. Blomberg, J., Persson, B., and Blomberg, A. (2005). Effects of semi-isostatic densification of wood on the variation in strength properties with density. Wood. Sci. Technol. 39: 339–350. https://doi.org/10.1007/s00226-005-0290-8.10.1007/s00226-005-0290-8 ↗
6. Boonstra, M.J. and Blomberg, J. (2007). Semi-isostatic densification of heat-treated radiata pine. Wood. Sci. Technol. 41: 607–617. https://doi.org/10.1007/s00226-007-0140-y.10.1007/s00226-007-0140-y ↗
7. Büyüksari, Ü. (2013). Surface characteristics and hardness of MDF panels laminated with thermally compressed veneer. Compos. B Eng. 44: 675–678.10.1016/j.compositesb.2012.01.087 ↗
8. Candan, Z., Hiziroglu, S., and Mcdonald, A.G. (2010). Surface quality of thermally compressed Douglas fir veneer. Mater. Des. 31: 3574–3577. https://doi.org/10.1016/j.matdes.2010.02.003.10.1016/j.matdes.2010.02.003 ↗
9. Che, W., Xiao, Z., Wang, Z., Nguyen, T.T., and Xie, Y. (2019). Enhanced weathering resistance of radiata pine wood by treatment with an aqueous styrene/acrylic acid copolymer dispersion. J. Wood Chem. Technol. 39: 421–435. https://doi.org/10.1080/02773813.2019.1636824.10.1080/02773813.2019.1636824 ↗
10. Diouf, P.N., Stevanovic, T., Cloutier, A., Fang, C.H., Blanchet, P., Koubaa, A., and Mariotti, N. (2011). Effects of thermo-hygro-mechanical densification on the surface characteristics of trembling aspen and hybrid poplar wood veneers. Appl. Surf. Sci. 257: 3558–3564. https://doi.org/10.1016/j.apsusc.2010.11.074.10.1016/j.apsusc.2010.11.074 ↗
11. Dubey, M.K., Pang, S., Chauhan, S., and Walker, J. (2016). Dimensional stability, fungal resistance and mechanical properties of radiata pine after combined thermo-mechanical compression and oil heat-treatment. Holzforschung 70: 793–800. https://doi.org/10.1515/hf-2015-0174.10.1515/hf-2015-0174 ↗
12. Dwianto, W., Inoue, M., and Norimoto, M. (1997). Fixation of compressive deformation of wood by heat treatment. Mokuzai Gakkaishi 43: 303–309.
13. Fang, C.H., Cloutier, A., Blanchet, P., Koubaa, A., and Mariotti, N. (2011). Densification of wood veneers combined with oil-heat treatment. Part 1: dimensional stability. BioResources 6: 373–385.10.15376/biores.6.1.373-385 ↗
14. Gabrielli, C.P., and Kamke, F.A. (2010). Phenol–formaldehyde impregnation of densified wood for improved dimensional stability. Wood. Sci. Technol. 44: 95–104. https://doi.org/10.1007/s00226-009-0253-6.10.1007/s00226-009-0253-6 ↗
15. Inoue, M., Norimoto, M., Tanahashi, M., and Rowell, R.M. (1993a). Steam or heat fixation of compressed wood. Wood Fiber Sci. 25: 224–235.
16. Inoue, M., Ogata, S., Kawai, S., Rowell, R.M., and Norimoto, M. (1993b). Fixation of compressed wood using melamine-formaldehyde resin. Wood Fiber Sci. 25: 404–410.
17. ISO 13061-2 (2014). Physical and mechanical properties of wood – Test methods for small clear wood specimens – Part 2: Determination of density for physical and mechanical tests. The International Organization for Standardization.
18. ISO 13061-3 (2014). Physical and mechanical properties of wood – Test methods for small clear wood specimens – Part 3: Determination of ultimate strength in static bending. The International Organization for Standardization.
19. ISO 13061-12 (2017). Physical and mechanical properties of wood – Test methods for small clear wood specimens – Part 12: Determination of static hardness. The International Organization for Standardization.
20. ISO 13061-17 (2017). Physical and mechanical properties of wood – Test methods for small clear wood specimens – Part 17: Determination of ultimate stress in compression parallel to grain. The International Organization for Standardization.
21. İmirzi, H.Ö., Ülker, O., and Burdurlu, E. (2014). Effect of densification temperature and some surfacing techniques on the surface roughness of densified Scots pine (Pinus sylvestris L.). BioResources 9: 191–209.10.15376/biores.9.1.191-209 ↗
22. Kamke, F.A., and Sizemore, H. (2008). Viscoelastic thermal compression of wood. US Patent No. US7404422B2.
23. Kariz, M., Kuzman, M.K., Sernek, M., Hughes, M., Rautkari, L., Kamke, F.A., and Kutnar, A. (2017). Influence of temperature of thermal treatment on surface densification of spruce. Eur. J. Wood Wood Prod. 75: 113–123. https://doi.org/10.1007/s00107-016-1052-z.10.1007/s00107-016-1052-z ↗
24. Kollmann, F.F.P., Kuenzi, E.W., and Stamm, A.J. (1975). Principles of wood science and technology. In: Wood based materials, Vol. II. Berlin: Springer-Verlag, pp. 139–149.10.1007/978-3-642-87931-9 ↗
25. Kutnar, A. and Kamke, F.A. (2012). Influence of temperature and steam environment on set recovery of compressive deformation of wood. Wood. Sci. Technol. 46: 953–964. https://doi.org/10.1007/s00226-011-0456-5.10.1007/s00226-011-0456-5 ↗
26. Kutnar, A., Kamke, F.A., and Sernek, M. (2008). The mechanical properties of densified VTC wood relevant for structural composites. Holz Roh Werkst 66: 439–446. https://doi.org/10.1007/s00107-008-0259-z.10.1007/s00107-008-0259-z ↗
27. Laine, K., Rautkari, L., Hughes, M., and Kutnar, A. (2013). Reducing the set-recovery of surface densified solid Scots pine wood by hydrothermal post-treatment. Eur. J. Wood Wood Prod. 71: 17–23. https://doi.org/10.1007/s00107-012-0647-2.10.1007/s00107-012-0647-2 ↗
28. Laine, K., Segerholm, K., Wålinder, M., Rautkari, L., Hughes, M., and Lankveld, C. (2016). Surface densification of acetylated wood. Eur. J. Wood Wood Prod. 74: 829–835. https://doi.org/10.1007/s00107-016-1077-3.10.1007/s00107-016-1077-3 ↗
29. Laskowska, A. (2020). The influence of ultraviolet radiation on the colour of thermo-mechanically modified beech and oak wood. Maderas Cienc. Tecnol. 22: 55–68.10.4067/S0718-221X2020005000106 ↗
30. Morsing, N. (2000). Densification of wood – The influence of hygrothermal treatment on compression of beech perpendicular to the grain, Ph.D. Thesis, Technical University of Denmark, Department of Structural Engineering and Materials.
31. Navi, P. and Girardet, F. (2000). Effects of thermo-hydro-mechanical treatment on the structure and properties of wood. Holzforschung 54: 287–293. https://doi.org/10.1515/hf.2000.048.10.1515/HF.2000.048 ↗
32. Navi, P. and Heger, F. (2004). Combined densification and thermo–hydro-mechanical processing of wood. MRS Bull. 29: 332–336. https://doi.org/10.1557/mrs2004.100.10.1557/mrs2004.100 ↗
33. Neyses, B., Karlsson, O., and Sandberg, D. (2020). The effect of ionic liquid and superbase pre-treatment on the spring-back, set-recovery and Brinell hardness of surface-densified Scots pine. Holzforschung 74: 303–312. https://doi.org/10.1515/hf-2019-0158.10.1515/hf-2019-0158 ↗
34. Pelit, H. and Emiroglu, F. (2020). Effect of water repellents on the hygroscopicity and dimensional stability of densified fir and aspen woods. Drvna Ind 71: 29–40. https://doi.org/10.5552/drvind.2020.1901.10.5552/drvind.2020.1901 ↗
35. Pelit, H., and Yorulmaz, R. (2019). Influence of densification on mechanical properties of thermally pretreated spruce and poplar wood. BioResources 14: 9739–9754.
36. Pelit, H., Budakçı, M., and Sönmez, A. (2018). Density and some mechanical properties of densified and heat post-treated Uludağ fir, linden and black poplar woods. Eur. J. Wood Wood Prod. 76: 79–87. https://doi.org/10.1007/s00107-017-1182-y.10.1007/s00107-017-1182-y ↗
37. Pelit, H., Sönmez, A., and Budakçı, M. (2014). Effects of ThermoWood® process combined with thermo-mechanical densification on some physical properties of Scots pine (Pinus sylvestris L.). BioResources 9: 4552–4567. https://doi.org/10.15376/biores.9.3.4552-4567.10.15376/biores.9.3.4552-4567 ↗
38. Rassam, G., Ghofrani, M., Taghiyari, H.R., Jamnani, B., and Khajeh, M.A. (2012). Mechanical performance and dimensional stability of nano-silver impregnated densified spruce wood. Eur. J. Wood Wood Prod. 70: 595–600. https://doi.org/10.1007/s00107-011-0590-7.10.1007/s00107-011-0590-7 ↗
39. Rautkari, L. (2012). Surface modification of solid wood using different techniques, Ph. D. Thesis, Finland: Aalto University, School of Chemical Technology.
40. Rautkari, L., Properzi, M., Pichelin, F., and Hughes, M. (2009). Surface modification of wood using friction. Wood Sci. Technol. 43: 291–299. https://doi.org/10.1007/s00226-008-0227-0.10.1007/s00226-008-0227-0 ↗
41. Rowell, R.M. (Ed.) (2012). Handbook of wood chemistry and wood composites. Boca Raton: CRC Press.10.1201/b12487 ↗
42. Sandberg, D., Haller, P., and Navi, P. (2013). Thermo-hydro and thermo-hydro-mechanical wood processing: an opportunity for future environmentally friendly wood products. Wood Mater. Sci. Eng. 8: 64–88. https://doi.org/10.1080/17480272.2012.751935.10.1080/17480272.2012.751935 ↗
43. Sandberg, D., Kutnar, A., and Mantanis, G. (2017). Wood modification technologies-a review. Iforest 10: 895–908. https://doi.org/10.3832/ifor2380-010.10.3832/ifor2380-010 ↗
44. Seborg, R.M., Tarkow, H., and Stamm, A.J. (1962). Modified woods. Madison: Forest Products Laboratory, Report No: 2192 (revised).
45. Song, J., Chen, C., Zhu, S., Zhu, M., Dai, J., Ray, U., Li, Y., Kuang, Y., Li, Y., Quispe, N., et al. (2018). Processing bulk natural wood into a high-performance structural material. Nature 554: 224–228. https://doi.org/10.1038/nature25476.10.1038/nature25476 ↗
46. Tabarsa, T. and Chui, Y.H. (1997). Effects of hot-pressing on properties of white spruce. Forest Prod. J. 47: 71–76.
47. Ünsal, Ö., Candan, Z., Büyüksarı, Ü., Korkut, S., Chang, Y.S., and Yeo, H. (2011). Effect of thermal compression treatment on the surface hardness, vertical density propile and thickness swelling of eucalyptus wood boards by hot-pressing. Mokchae Konghak 39: 1–8. https://doi.org/10.5658/wood.2011.39.2.148.10.5658/WOOD.2011.39.2.148 ↗
48. Wang, B.J., Ellis, S., and Dai, C. (2006). Veneer surface roughness and compressibility pertaining to plywood/LVL manufacturing. Part II. Optimum panel densification. Wood Fiber Sci. 38: 727–735.
49. Welzbacher, C.R., Wehsener, J., Rapp, A.O., and Haller, P. (2008). Thermo-mechanical densification combined with thermal modification of Norway spruce (Picea abies Karst) in industrial scale—dimensional stability and durability aspects. Holz Roh Werkst 66: 39–49. https://doi.org/10.1007/s00107-007-0198-0.10.1007/s00107-007-0198-0 ↗