journal article·2025-04-29Open access

Microwave hybrid process-based fabrication of super duplex stainless steel joints using nickel and stainless steel filler materials

Parminder Singh, Deoraj Prajapati, Shankar Sehgal

Abstract

Abstract This study introduces a joining procedure applicable to super duplex stainless steel (SAF2507) alloys through the microwave hybrid heating (MHH)-based process using nickel (Ni) and stainless steel (SS304) filler powders. Mechanical test results of the Ni-filler joints revealed an average value of microhardness of 432 HV and an ultimate tensile strength value of 442 MPa. Similarly, SS304 filler joints showed an average value of microhardness of 461 HV and an ultimate tensile strength of 534 MPa. The hardness of SS304 filler joints was 6.71% more than that of Ni-filler joints. Increased hardness leads to better ear properties, which are required in many engineering applications. Furthermore, the tensile strength of SS304 filler joints was 20.81% better than that of Ni-filler joints. Better tensile strength of joints is a major requirement from a design safety point of view. Energy-dispersive spectroscopy results revealed the presence of iron, chromium, molybdenum, nickel, manganese, and carbon elements in the weld zone. Furthermore, the microstructural analysis performed using scanning electron microscopy showed a robust metallurgical bonding among the two interface surfaces, leading to the formation of good quality joints with no interfacial cracking.
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Research context

OpenAlex topics: Microwave-Assisted Synthesis and Applications · Advanced Welding Techniques Analysis · Aluminum Alloys Composites Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Mechanical Engineering Department, PEC (Deemed to be University) , Chandigarh , 160012 , India

University Centre for Research and Development, Chandigarh University , Mohali , Punjab, 140413 , India

Mechanical Engineering, UIET, Panjab University , Chandigarh , 160014 , India

References (47)

Show source-provided references
1. Das, S., A. Bansal, and A. K. Sharma. Theory of welding of metallic parts in microwave cavity applicator. Fundamental Journal of Modern Physics, Vol. 3, No. 2, 2012, pp. 125–155.
2. Yahaya, B., S. Izman, M. Konneh, and N. Redzuan. Microwave hybrid heating of materials using susceptors -A brief review. Advances in Materials Research, Vol. 845, 2014, pp. 426–430.10.4028/www.scientific.net/AMR.845.426 ↗
3. Bhoi, N. K., H. Singh, and S. Pratap. A study on microwave susceptor material for hybrid heating. Journal of Physics: Conference Series, Vol. 1240, No. 1, 2019, id. 012097.10.1088/1742-6596/1240/1/012097 ↗
4. Singh, S., D. Gupta, and V. Jain. Recent applications of microwaves in materials joining and surface coatings. Journal of Engineering Manufacture, Vol. 230, No. 4, 2015, pp. 1–15.10.1177/0954405414560778 ↗
5. Kumar, A., A. Kumar, B. Sumit, and S. Morsi. Multi-physics simulation study on casting T-section of copper powder using microwave energy. Arabian Journal for Science and Engineering, 2025.10.1007/s13369-024-09903-9 ↗
6. Singh, P., D. R. Prajapati, and S. Sehgal. Microwave joining of SAF 2507 and optimization of elemental constitution using design of experiments. E3S Web of Conferences, Vol. 552, 2024, id. 01032.10.1051/e3sconf/202455201032 ↗
7. Singh, P., D. R. Prajapati, and S. Sehgal. Filler powder free joining of SAF 2507 using selective microwave hybrid heating technique. Indian Journal of Engineering & Materials Sciences, Vol. 29, 2022, pp. 307–311.10.56042/ijems.v29i3.65752 ↗
8. Sato, Y. S., T. W. Nelson, C. J. Sterling, R. J. Steel, and C. O. Pettersson. Microstructure and mechanical properties of friction stir welded SAF 2507 super duplex stainless steel. Materials Science & Engineering, A: Structural Materials: Properties, Microstructure and Processing, Vol. 397, No. 1–2, 2005, pp. 376–384.10.1016/j.msea.2005.02.054 ↗
9. Saeid, T., A. Abdollah-zadeh, H. Assadi, and F. Malek Ghaini. Effect of friction stir welding speed on the microstructure and mechanical properties of a duplex stainless steel. Materials Science & Engineering, A: Structural Materials: Properties, Microstructure and Processing, Vol. 496, No. 1–2, 2008, pp. 262–268.10.1016/j.msea.2008.05.025 ↗
10. Davison, R. M. and J. D. Redmond. A guide to using duplex stainless steels. Materials & Design, Vol. 12, No. 4, 1991, pp. 187–192.10.1016/0261-3069(91)90162-W ↗
11. Tavares, S. S. M., J. M. Pardal, L. D. Lima, I. N. Bastos, A. M. Nascimento, and J. A. de Souza. Characterization of microstructure, chemical composition, corrosion resistance and toughness of a multipass weld joint of superduplex stainless steel UNS S32750. Materials Characterization, Vol. 58, No. 7, 2007, pp. 610–616.10.1016/j.matchar.2006.07.006 ↗
12. Cui, Z., L. Wang, H. Ni, W. Hao, C. Man, S. Chen, et al. Influence of temperature on the electrochemical and passivation behavior of 2507 super duplex stainless steel in simulated desulfurized flue gas condensates. Corrosion Science, Vol. 118, 2017, pp. 31–48.10.1016/j.corsci.2017.01.016 ↗
13. Silverstein, R. and D. Eliezer. Mechanisms of hydrogen trapping in austenitic, duplex, and super martensitic stainless steels. Journal of Alloys and Compounds, Vol. 720, 2017, pp. 451–459.10.1016/j.jallcom.2017.05.286 ↗
14. Zhang, Z., H. Zhao, H. Zhang, J. Hu, and J. Jin. Microstructure evolution and pitting corrosion behavior of UNS S32750 super duplex stainless steel welds after short-time heat treatment. Corrosion Science, Vol. 121, 2017, pp. 22–31.10.1016/j.corsci.2017.02.006 ↗
15. Ye, F., H. Fujii, T. Tsumura, and K. Nakata. Friction stir welding of Inconel alloy 600. Journal of Materials Science, Vol. 41, No. 16, 2006, pp. 5376–5379.10.1007/s10853-006-0169-6 ↗
16. Mohammed, G. R., M. Ishak, S. N. A. S. Ahmad, and H. A. Abdulhadi. Fiber laser welding of dissimilar 2205/304 stainless steel plates. Metals (Basel), Vol. 7, No. 12, 2017, pp. 1–19.10.3390/met7120546 ↗
17. Bhattacharya, A. and R. Kumar. Dissimilar joining between austenitic and duplex stainless steel in double-shielded GMAW: A comparative study. Materials and Manufacturing Processes, Vol. 31, No. 3, 2016, pp. 300–310.10.1080/10426914.2015.1070414 ↗
18. Mithilesh, P., D. Varun, A. R. G. Reddy, K. D. Ramkumar, N. Arivazhagan, and S. Narayanan. Investigations on dissimilar weldments of inconel 625 and AISI 304. Procedia Engineering, Vol. 75, 2014, pp. 66–70.10.1016/j.proeng.2013.11.013 ↗
19. Ramkumar, T., M. Selvakumar, P. Narayanasamy, A. A. Begam, P. Mathavan, and A. A. Raj. Studies on the structural property, mechanical relationships and corrosion behaviour of Inconel 718 and SS 316L dissimilar joints by TIG welding without using activated flux. Journal of Manufacturing Processes, Vol. 30, 2017, pp. 290–298.10.1016/j.jmapro.2017.09.028 ↗
20. Singh, S., V. Kumar, S. Kumar, and A. Kumar. Variant of MIG welding of similar and dissimilar metals: A review. Materials Today: Proceedings, Vol. 56, 2022, pp. 3550–3555.10.1016/j.matpr.2021.11.287 ↗
21. Hong, X., B. Huang, T. Li, X. Wang, Y. Wu, and J. Zheng. Optimization of plasma arc welding process parameters of SAF 2507/316L dissimilar steel based on response surface method. Welding in the World, Vol. 67, No. 11, 2023, pp. 2493–2509.10.1007/s40194-023-01584-6 ↗
22. Li, T., K. Wang, and Y. Lei. A review ofwelding process for UNS S32750 super duplex stainless steel. Materials (Basel), Vol. 17, No. 5215, 2024, pp. 1–16.10.3390/ma17215215 ↗
23. Hong, X., B. Huang, T. Li, J. Zheng, and Y. Zhu. Effects of welding speed and welding current on the residual stress and deformation of SAF 2507/316L dissimilar plasma arc welding. Materialwissenschaft und Werkstofftechnik, Vol. 55, No. 2, 2024, pp. 179–193.10.1002/mawe.202300128 ↗
24. Mabuwa, S., V. Msomi, H. Mehdi, and T. Ngonda. A study on the metallurgical characterisation of the longitudinally sampled friction stir processed TIG welded dissimilar aluminum joints. Proceedings of the Institution of Mechanical Engineers, Part E: Journal of Process Mechanical Engineering, 2023.10.1177/09544089231169589 ↗
25. Lawal, S. L. and S. A. Afolalu. Innovations in TIG and MIG welding technologies: Recent developments and future trends. International Conference on Science, Engineering and Business for Driving Sustainable Development Goals, SEB4SDG 2024, 2024, pp. 1–6.10.1109/SEB4SDG60871.2024.10630400 ↗
26. Dagur, H., R. Kumar, V. Singh, S. Chauhan, A. Deep, and D. Patel. Effect of TIG and activated flux TIG welding processes on weld bead geometry, microstructure, and hardness of SAF 2507 grade super duplex stainless steel joints. Engineering Research Express, Vol. 5, No. 3, 2023, id. 035010.10.1088/2631-8695/ace2af ↗
27. Song, S., Z. Han, Y. Hu, D. Wang, Z. Ren, J. Zhou, et al. Investigations on mechanical and surface properties of friction stir welded dissimilar joints of 2507 SDSS and 317L ASS. Tribology International, Vol. 201, 2025, id. 110226.10.1016/j.triboint.2024.110226 ↗
28. Qi, K., R. Li, G. Wang, G. Li, B. Liu, and M. Wu. Microstructure and corrosion properties of laser-welded SAF 2507 super duplex stainless steel joints. Journal of Materials Engineering and Performance, Vol. 28, No. 1, 2019, pp. 287–295.10.1007/s11665-018-3833-5 ↗
29. Köse, C. Effect of heat input and post weld heat treatment on the texture, microstructure and mechanical properties of laser beam welded AISI 317L austenitic stainless steel. Materials Science & Engineering, A: Structural Materials: Properties, Microstructure and Processing, Vol. 855, No. September 2021, 2022, pp. 861–894.10.1016/j.msea.2022.143966 ↗
30. Šimeková, B., M. Dománková, I. Kovaříková, P. Kovačócy, M. Martinkovič, M. Šimek, et al. Microstructural and mechanical characterization of the laser beam welded SAF 2507 super-duplex stainless steel. Metals (Basel), Vol. 14, No. 10, 2024, id. 1184.10.3390/met14101184 ↗
31. Wang, Q., G. Gu, C. Jia, K. Li, and C. Wu. Investigation of microstructure evolution, mechanical and corrosion properties of SAF 2507 super duplex stainless steel joints by keyhole plasma arc welding. Journal of Materials Research and Technology, Vol. 22, 2023, pp. 355–374.10.1016/j.jmrt.2022.11.107 ↗
32. Cao, F., T. Jiang, W. Hou, G. Huang, Y. Shen, Y. Ding, et al. Effect of inhomogeneous fiber structure on the mechanical properties of friction stir welded SAF 2507 super duplex stainless steel. Materials Chemistry and Physics, Vol. 283, 2022, pp. 611–623.10.1016/j.jmapro.2021.11.043 ↗
33. Singh, P., D. R. Prajapati, and S. Sehgal. A review on different types of material joints fabricated by microwave hybrid heating method. Materials Today: Proceedings, Vol. 50, 2021, pp. 904–910.10.1016/j.matpr.2021.06.253 ↗
34. Kamble, D. L., R. K. Sahu, and S. Narendranath. Characterization of Inconel 625-SS 304 weldments developed by selective microwave hybrid joining technique for promising applications. Journal of Materials Engineering and Performance, Vol. 33, 2023, pp. 6693–6705.10.1007/s11665-023-08390-7 ↗
35. Handa, V., P. Goyal, and S. Sehgal. Application of graphite rods in producing Inconel 625 (UNS N06625) joints through the use of microwave radiation energy. Indian Journal of Engineering & Materials Sciences, Vol. 29, No. 3, 2022, pp. 378–384.10.56042/ijems.v29i3.65756 ↗
36. Sahota, D. S., A. Bansal, and V. Kumar. Microwave butt joining of stainless steel (SS-316L) with an SS-316L powder. Transactions of the Indian Institute of Metals, Vol. 76, No. 12, 2023, pp. 3303–3312.10.1007/s12666-023-03009-w ↗
37. Thakur, A., R. Bedi, A. K. Bagha, and P. S. Rao. Microstructural and mechanical properties of mild steel pipes joined using selective microwave hybrid heating. Journal of Manufacturing Processes, Vol. 82, 2022, pp. 848–859.10.1016/j.jmapro.2022.08.024 ↗
38. Gamit, D., R. R. Mishra, and A. K. Sharma. Joining of mild steel pipes using microwave hybrid heating at 2.45 GHz and joint characterization. Journal of Manufacturing Processes, Vol. 27, 2017, pp. 158–168.10.1016/j.jmapro.2017.04.028 ↗
39. Kumar, V., S. Sehgal, A. Rathan, M. K. Agrawal, and S. S. Abdullaev. Parametric investigation into the mechanical characteristics of dissimilar steel joints produced using SMHH-based joining technology. Journal of Adhesion Science and Technology, 2023, pp. 1–19.10.1080/01694243.2023.2267273 ↗
40. Kumar, V. and S. Sehgal. Metallurgical and mechanical assessment of SS2205/SS304 joints fabricated using modified selective microwave hybrid heating-based joining. Journal of Materials Engineering and Performance, Vol. 33, 2023, pp. 9732–9744.10.1007/s11665-023-08605-x ↗
41. Singh, T. and S. Sehgal. Computational modeling and simulation of the microwave hybrid heating process: A state of the art review. Archives of Computational Methods in Engineering, Vol. 31, No. 2, 2024, pp. 1153–1200.10.1007/s11831-023-10012-3 ↗
42. Singh, T. and S. Sehgal. A systematic review on the microwave joining of metallic material through hybrid heating technique. Proceedings of the Institution of Mechanical Engineers, Part E: Journal of Process Mechanical Engineering, 2024.10.1177/09544089241296595 ↗
43. Singh, T. and S. Sehgal. Thermal modeling and simulation applied to novel microwave hybrid heating process. Physica Scripta, Vol. 99, No. 9, 2024, id. 95536.10.1088/1402-4896/ad6d06 ↗
44. Kumar, V. and S. Sehgal. Comparative experimental investigations on novel joining technology based on microwave energy to produce SS2205-SS2205 joints. Indian Journal of Engineering & Materials Sciences, Vol. 30, No. 1, 2023, pp. 147–153.10.56042/ijems.v1i1.66679 ↗
45. Bagha, L., S. Sehgal, A. Thakur, H. Kumar, and D. Goyal. Low cost joining of SS304-SS304 through microwave hybrid heating without filler-powder. Engineering Research Express, Vol. 1, No. 2, 2019, id. 025035.10.1088/2631-8695/ab551d ↗
46. Pal, M., V. Kumar, S. Sehgal, H. Kumar, K. Kuldeep, and A. K. Bagha. Microwave hybrid heating based optimized joining of SS304/SS316. Materials and Manufacturing Processes, 2020, pp. 1–7.10.1080/10426914.2020.1854469 ↗
47. Bagha, L., S. Sehgal, A. Thakur, and H. Kumar. Effects of powder size of interface material on selective hybrid carbon microwave joining of SS304–SS304. Journal of Manufacturing Processes, Vol. 25, 2017, pp. 290–295.10.1016/j.jmapro.2016.12.013 ↗