journal article·2021-06

In-Situ Investigation of Resin Shrinkage in the Composite Manufacturing Environment

Samarth Motagi, Sirish Namilae

Applied Composite Materials· Volume 28· Issue 3
Publisher page

Abstract

Cure shrinkage of the polymer matrix during the composite manufacturing process leads to residual stresses, which can adversely affect the structural integrity and dimensional stability of composite structures. In this paper, a novel approach is developed for measuring the resin shrinkage and strain evolution of an epoxy resin (EPON-862) in the composite manufacturing environment. The resin is cured in a custom designed autoclave with borosilicate viewports, while digital image correlation (DIC) is used to analyze the strain evolution throughout the cure cycle. These processing induced strains are correlated to the cure-state using differential scanning calorimetery (DSC). The different mechanisms involved in the polymer strain evolution during composite processing are discussed.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Epoxy Resin Curing Processes · Mechanical Behavior of Composites · Polymer crystallization and properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (12)

Show source-provided references
1. Dusek, K.: Network formation in curing of epoxy resins. Adv. Polym. Sci. 78, 1–59 (1986). https://doi.org/10.1007/bfb003535610.1007/bfb0035356 ↗
2. Wisnom, M.R., Gigliotti, M., Ersoy, N., Campbell, M., Potter, K.D.: Mechanisms generating residual stresses and distortion during manufacture of polymer-matrix composite structures. Compos. Part A Appl. Sci. Manuf. 37, 522–529 (2006). https://doi.org/10.1016/j.compositesa.2005.05.01910.1016/j.compositesa.2005.05.019 ↗
3. Snow, A.W., Armistead, J.P.: A simple dilatometer for thermoset cure shrinkage and thermal expansion measurements. J. Appl. Polym. Sci. 52, 401–411 (1994). https://doi.org/10.1002/app.1994.07052030510.1002/app.1994.070520305 ↗
4. Shah, D.U., Schubel, P.J.: Evaluation of cure shrinkage measurement techniques for thermosetting resins. Polym. Test. 29, 629–639 (2010). https://doi.org/10.1016/j.polymertesting.2010.05.00110.1016/j.polymertesting.2010.05.001 ↗
5. Kravchenko, O.G., Kravchenko, S.G., Casares, A., Pipes, R.B.: Digital image correlation measurement of resin chemical and thermal shrinkage after gelation. J. Mater. Sci. 50, 5244–5252 (2015). https://doi.org/10.1007/s10853-015-9072-310.1007/s10853-015-9072-3 ↗
6. EPON-862\Epikure W technical data sheet. https://www.miller-stephenson.com/wp-content/uploads/2016/08/W.pdf. Accessed 06 Jan 2021
7. Yoneyama, S., Murasawa, G.: Digital image correlation. Exp. Mech. (2009)
8. Correlated solutions, https://www.correlatedsolutions.com/vibration-fatigue-module. Accessed 06 Jan 2021
9. Hardis, R., Jessop, J.L.P., Peters, F.E., Kessler, M.R.: Cure kinetics characterization and monitoring of an epoxy resin using DSC, Raman spectroscopy, and DEA. Compos. Part A Appl. Sci. Manuf. 49, 100–108 (2013). https://doi.org/10.1016/j.compositesa.2013.01.02110.1016/j.compositesa.2013.01.021 ↗
10. Fu, Y., Michopoulos, J.G., Song, J.H.: On investigating the thermomechanical properties of cross-linked epoxy via molecular dynamics analysis. Nanoscale Microscale Thermophys. Eng. 21, 8–25 (2017). https://doi.org/10.1080/15567265.2016.126369610.1080/15567265.2016.1263696 ↗
11. Chava, S., Namilae, S.: In situ investigation of the kinematics of ply interfaces during composite manufacturing. J. Manuf. Sci. Eng. Trans. ASME. 143, 1–10 (2021). https://doi.org/10.1115/1.404774010.1115/1.4047740 ↗
12. Chava, S., Namilae, S.: Continuous Evolution of Processing Induced Residual Stresses in Composites: An In-situ Approach. In: Composites: Part A (In Print)