journal article·2014-12

Microstructural Characterisation of Jute/Epoxy Quasi-Unidirectional Composites

Amandeep Singh Virk, Wayne Hall, John Summerscales

Applied Composite Materials· Volume 21· Issue 6
Publisher page

Abstract

The elastic properties of a composite can be predicted by micromechanical models based on the properties of the individual constituent materials of the composite and their geometrical characteristics. This paper presents a novel methodology using image analysis to determine (a) the fibre volume fraction and (b) the fibre orientation distribution factor of quasi-unidirectional jute fibre reinforced epoxy resin composites. For fibre volume fraction, digital micrographs were smoothed to reduce noise in the image, an intensity histogram informed selection of the threshold intensity for conversion to a binary image, the image was morphologically closed and opened to remove internal voids and small features respectively and the fibre volume fraction was calculated as the ratio of the detected fibre area to the total image area. For fibre orientation, the image was sharpened with Contrast-Limited Adaptive Histogram Equalisation, a threshold was set for conversion to binary and then a masking image was rotated at a number of seed points over the image to find the angles with the minimum sum of intensity at each point. The data generated was then used to validate new rules-of-mixture equations for natural fibre composites.
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Research context

OpenAlex topics: Natural Fiber Reinforced Composites · Mechanical Behavior of Composites · Mechanical Engineering and Vibrations Research

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (58)

Show source-provided references
1. Summerscales, J., Dissanayake, N., Virk, A., Hall, W.: A review of bast fibres and their composites. Part 1—Fibres as reinforcements. Compos A Appl Sci Manuf 41(10), 1329–1335 (2010)10.1016/j.compositesa.2010.06.001 ↗
2. Summerscales, J., Dissanayake, N., Virk, A., Hall, W.: A review of bast fibres and their composites. Part 2—Composites. Compos A Appl Sci Manuf 41(10), 1336–1344 (2010)10.1016/j.compositesa.2010.05.020 ↗
3. Summerscales, J., Virk, A.S., Hall, W.: A review of bast fibres and their composites. Part 3: modelling. Compos A Appl Sci Manuf 44(1), 132–139 (2010)
4. Summerscales, J., Grove. S.: Manufacturing methods for natural fibre composites. In: Hodzic, A., Shanks, R. (eds.): Handbook of natural fibre composites: properties, processes, failure and applications, Woodhead Publishing, Cambridge, 2014. doi: 10.1533/9780857099228.2.17610.1533/9780857099228.2.176 ↗
5. Dissanayake, N.P.J., Summerscales, J.: Life cycle assessment for natural fibre composites. In: Thakur, V.K. (ed.) Green composites from natural resources. Taylor and Francis Group LLC, USA (2013). ISBN 978-1-4665-7069-6 doi: 10.1201/b16076-910.1201/b16076-9 ↗
6. Garkhail, S.K., Heijenrath, R.W.H., Peijs, T.: Mechanical properties of natural-fibre-mat-reinforced thermoplastics based on flax fibres and polypropylene. Appl Compos Mater 7, 351–372 (2000)10.1023/A:1026590124038 ↗
7. Facca, A.G., Kortschot, M.T., Yan, N.: Predicting the elastic modulus of natural fibre reinforced thermoplastics. Compos A Appl Sci Manuf 37(10), 1660–1671 (2006)10.1016/j.compositesa.2005.10.006 ↗
8. Summerscales, J., Hall, W., Virk, A.S.: A fibre diameter distribution factor (FDDF) for natural fibre composites. J Mater Sci 46(17), 5876–5880 (2011)10.1007/s10853-011-5569-6 ↗
9. Virk, A.S., Hall, W., Summerscales, J.: Modulus and strength prediction for natural fibre composites. Mater Sci Technol 28(7), 864–871 (2012)10.1179/1743284712Y.0000000022 ↗
10. Summerscales, J. (ed.) Microstructural characterisation of fibre-reinforced composites, Cambridge: Woodhead Publishing (1998)10.1201/9781439823828 ↗
11. Summerscales, J., Pearce, N.R.L., Russell, P., Guild, F.J.: Voronoi cells, fractal dimensions and fibre composites. J Microsc 201(2), 153–162 (2001)10.1046/j.1365-2818.2001.00841.x ↗
12. Guild, F.J., Summerscales, J.: Microstructural image analysis applied to fibre composite materials: a review. Composites 24(5), 383–394 (1993)10.1016/0010-4361(93)90246-5 ↗
13. Yurgartis, S.W.: Measurement of small angle fiber misalignments in continuous fiber composites. Compos Sci Technol 30(4), 279–293 (1987)10.1016/0266-3538(87)90016-9 ↗
14. Clarke, A.R., Archenhold, G., Davidson, N.C.: A novel technique for determining 3D spatial distribution of glass fibres in polymer composites. Compos Sci Technol 55, 75–91 (1995)10.1016/0266-3538(95)00087-9 ↗
15. Clarke, A.R., Archenhold, G., Davidson, N.C., Fleck, N.A.: Determining the power spectral density of the waviness of unidirectional glass fibres in polymer composites. Appl Compos Mater 2, 233–243 (1995)10.1007/BF00567194 ↗
16. Clarke, A.R., Archenhold, G., Davidson, N.C.: 3D confocal microscopy of glass fibre-reinforced composites, Chapter 3 in [8]
17. Creighton, C.J., Sutcliffe, M.P.F., Clyne, T.W.: A multiple field image analysis procedure for characterisation of fibre alignment in composites. Compos A Appl Sci Manuf 32, 221–229 (2001)10.1016/S1359-835X(00)00115-9 ↗
18. Kratmann, K.K., Sutcliffe, M.P.F., Lilleheden, L.T., Pyrz, R., Thomsen, O.T.: A novel image analysis procedure for measuring fibre misalignment in unidirectional fibre composites. Compos Sci Technol 69(2), 228–238 (2009)10.1016/j.compscitech.2008.10.020 ↗
19. Virk, A.S., Hall, W., Summerscales, J.: Physical characterisation of jute technical fibres: fibre dimensions. J Natur Fibres 7(3), 216–228 (2010)10.1080/15440478.2010.504389 ↗
20. Virk, A.S., Hall, W., Summerscales, J.: Tensile properties of jute fibres. Mater Sci Technol 25(10), 1289–1295 (2009)10.1179/174328408X385818 ↗
21. Virk, A.S., Hall, W., Summerscales, J.: Multiple Data Set (MDS) weak-link scaling analysis of jute fibres. Compos A Appl Sci Manuf 40(11), 1764–1771 (2009)10.1016/j.compositesa.2009.08.022 ↗
22. Virk, A.S., Hall, W., Summerscales, J.: Modelling tensile properties of jute fibres. Mater Sci Technol 27(1), 458–460 (2011)10.1179/026708309X12578491814636 ↗
23. Rowell, R.M., Stout, H.P., Jute and Kenaf. In: Lewin, M., Pearce, E. M., (eds.) Handbook of Fiber Chemistry, Marcel Dekker Inc. Chapter 7, ISBN 0824794710 (1998)
24. Chattopadhyay, S.N., Pan, N.C., Day, A.: Reuse of reactive dyes for dyeing of jute fabric. Bioresour Technol 97(1), 77–83 (2006)10.1016/j.biortech.2005.02.033 ↗
25. Milner, A. The Ashford Book of Dyeing, Unicorn, ISBN 0908704887 (1998)
26. Sicomin SR 8100 Epoxy system for injection and infusion—product data sheet, http://www.mcmc-uk.com/prod-data-sheet/sr-8100-infusion-uk.pdf , accessed 25 June 2013 (2003)
27. West System® 501 White Pigment materials safety data sheet, http://www.westsystem.com/ss/assets/MSDS/MSDS501.pdf accessed 25 June 2013 (2011)
28. Caldwell, B., Cooper, M., Reid, L.G., Vanderheiden, G.: Web Content Accessibility Guidelines (WCAG) 2.0: Contrast Ratio, http://www.w3.org/TR/2008/REC-WCAG20-20081211/#contrast-ratiodef , accessed 25 June 2013 (2008)
29. Grafil: Test reference 101.13: Filament tensile strength and modulus, Coventry: Courtaulds Limited (1980)
30. ASTM: Standard D3379–75: Standard test method for tensile strength and Young’s modulus for high-modulus single-filament materials (withdrawn 1998) (1975)
31. Virk, A.S., Hall, W., Summerscales, J.: Failure strain as the key design criterion for fracture of natural fibre composites. Compos Sci Technol 70(6), 995–999 (2010)10.1016/j.compscitech.2010.02.018 ↗
32. Marques de Sá, J.P.: Applied Statistics Using SPSS, STATISTICA, MATLAB and R, Springer-Verlag Berlin Heidelberg, 2007, ISBN 978-3-540-71971-7 (2007)10.1007/978-3-540-71972-4 ↗
33. Åström, B.T.: Manufacturing of polymer composites. Chapman & Hall, London (1997). ISBN 0748770763
34. Williams, C., Summerscales, J., Grove, S.: Resin Infusion under Flexible Tooling (RIFT): a review. Compos A Appl Sci Manuf 27A(7), 517–524 (1996)10.1016/1359-835X(96)00008-5 ↗
35. Cripps, D., Searle, T.J., Summerscales, J.: Chapter 21: Open mould techniques for thermoset composites. In: Talreja, R., Månson, J.-A. (eds.) Comprehensive composite materials encyclopaedia—polymer matrix composites, vol. 2, pp. 737–761. Elsevier Science, Oxford (2000)10.1016/B0-08-042993-9/00188-1 ↗
36. Feiler, M., Dudenhausen, W., Chatzigeorgiou, L.: Manufacturing of primary aircraft structures with vacuum assisted resin infusion, Society of Manufacturing Engineers (ICCM-14) (2003)
37. Summerscales, J., Searle, T.J.: Review: low pressure (vacuum infusion) techniques for moulding large composite structures. Proc IMechE L J Mater Des Appl L219(1), 45–58 (2005)10.1243/146442005X10238 ↗
38. Summerscales, J.: Resin Infusion Under Flexible Tooling (RIFT), Encyclopedia of Composites—second edition, John Wiley & Sons, 2648-2658, DOI: 10.1002/9781118097298.weoc216 (2012)10.1002/9781118097298.weoc216 ↗
39. Adams, D.F., Carlsson, L.A., Pipes, R.B.: Experimental characterization of advanced composite materials. CRC Press, Boca Raton (2002). ISBN 1587161001
40. ASTM Standard D3039–00: Standard test method for tensile properties of polymer matrix composite materials (2000)
41. BS EN ISO 527–1:1996: Plastics—determination of tensile properties (1996)
42. BS EN ISO 527–4:1996: Plastics—determination of tensile properties (1996)
43. Gonzalez, R.C., Woods, R.E.: Digital image processing, Prentice Hall, ISBN 013168728X (2007)
44. Gonzalez, R.C., Woods, R.E., Eddins, S.L.: Digital image processing using matlab, Prentice Hall, ISBN 0130085197 (2003)
45. Matlab Image Processing Toolbox, http://www.mathworks.com/access/helpdesk/help/toolbox/images/adapthisteq.html (2008)
46. Zuiderveld, K.: Contrast limited adaptive histogram equalization. In: Heckbert, P.S., (ed), Graphic Gems IV, Academic Press Inc., 474–485 (1994)10.1016/B978-0-12-336156-1.50061-6 ↗
47. Elsayed, E.A.: ‘Reliability Engineering’, Addison Wesley Longman, ISBN 0201634813 (1996)
48. Reliasoft, Life data analysis reference, ReliaSoft Publishing, http://reliawiki.com/index.php/Life_Data_Analysis_Reference , accessed on 25 June 2013 (2013)
49. Folkes, M.J.: Short fibre reinforced thermoplastics, Chichester: Research Studies Press, ISBN 0471102091 (1982)
50. Krenchel, H.: Fibre reinforcement. Akademisk Forlag, Copenhagen (1964)
51. Press, W.H., Teukolsky, S.A., Vetterling, W.T., Flannery, B.P.: Numerical Recipes, Cambridge: Cambridge University Press, ISBN 0521880688 (2007)
52. Harris, J., Bond, I.P., Weaver, P., Wisnom, M.: Improving fibre reinforced plastics’ through-thickness properties using novel shaped fibres. Proc IMechE L J Mater Des Appl 218(L1), 29–35 (2004)10.1177/146442070421800104 ↗
53. Hucker, M., Bond, I., Bleay, S., Haq, S.: Experimental evaluation of unidirectional hollow glass fibre/epoxy composites under compressive loading. Compos A Appl Sci Manuf 34(10), 927–932 (2003)10.1016/S1359-835X(03)00236-7 ↗
54. Lamy, B., Baley, C.: Stiffness prediction of flax fibers-epoxy composite materials. J Mater Sci Lett 19(11), 979–980 (2000)10.1023/A:1006776423764 ↗
55. Bodros, E., Baley, C.: Study of the tensile properties of stinging nettle fibres (Urtica dioica). Mater Lett 62(14), 2143–2145 (2008)10.1016/j.matlet.2007.11.034 ↗
56. Cox, H.L.: The elasticity and strength of paper and other fibrous materials. Br J Appl Phys 3, 72–79 (1952)10.1088/0508-3443/3/3/302 ↗
57. Kelly, A., Tyson, W.R.: Tensile properties of fibre-reinforced metals: copper/tungsten and copper/molybdenum. J Mech Phys Solids 13, 329–350 (1965)10.1016/0022-5096(65)90035-9 ↗
58. Potter, R.T.: Strength of composites. In: Kelly, A. (ed.) Concise encyclopedia of composite materials. Pergamon, Oxford (1989). ISBN 0-08-034718-5