journal article·2000-07

Residual Compression Stress Profile in High-Modulus Carbon Fiber Embedded in Isotactic Polypropylene by Micro-Raman Spectroscopy

H. D. Wagner, M. S. Amer, L. S. Schadler

Applied Composite Materials· Volume 7· Issue 4
Publisher page

Abstract

Raman spectroscopy was used to investigate the compressive fragmentation process and the interface behavior in ultra high modulus (UHM) (750 GPa Modulus) pitch-based graphite/polypropylene composites upon cooling from processing temperature to room temperature. It is found that bulging is the primary mechanism of failure in these fibers, and Raman peak position measurements show that not all visually detected features represent real fiber failure. However, at real break locations, the fiber strain is found to drop to zero.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Fiber-reinforced polymer composites · Graphite, nuclear technology, radiation studies · Graphene research and applications

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (24)

Show source-provided references
1. Ha, Jong-Bae and Nairn, J. S., 'Compression Failure Mechanisms of Single-ply Unidirectional Carbon-fiber Composites', SAMPE Quarterly 23 (3), 1992, 29–36.
2. Madhukar, M. S. and Drzal, L. T., 'Fiber-Matrix Adhesion and Its Effect on Composite Mechanical Properties. III. Longitudinal Compressive Properties of Graphite/Epoxy Composites', J. Composite Materials 26 (3), 1992, 310–333.10.1177/002199839202600301 ↗
3. Langford, J., Jr., 'Characterization of Compressive Damage Mechanisms in Advanced Fiber Reinforced Composites', J. Materials Science, in press.
4. Melanitis, N. and Galiotis, C., 'A New Technique for Assessing the Compressive Behavior of Single Filaments', J. Materials Science 25, 1990, 5081.10.1007/BF00580133 ↗
5. Melanitis, N., Tetlow, P., Galiotis, C., and Smith, S., 'Compressional Behavior of Carbon Fibers', J. Materials Science 29, 1994, 786–799.10.1007/BF00445995 ↗
6. Wood, J. R., Wagner, H. D., and Marom, G., 'The Compressive Fragmentation Phenomenon: Using Microcomposites to Evaluate Thermal Stresses, Single Fiber Compressive Strengths, Weibull Parameters and the Interfacial Shear Strengths', Proc. Roy. Soc., London A452, 1996, 235–252.
7. Wood, J. R., Wagner, H. D., and Marom, G., 'A Model for Compressive Fragmentation', Advanced Composites Lett. 3 (4), 1994, 133–138.
8. Cox, H. L., 'The Elasticity and Strength of Paper and Other Fibrous Materials', Brit. J. Appl. Phys. 3, 1952, 72–79.10.1088/0508-3443/3/3/302 ↗
9. Schadler, L. S., Melanitis, N., Galiotis, C., Figueroa, J. C., and Laird, C., 'Interphase Behavior in Carbon / Thermoplastic Model Composites Using Laser Raman Spectroscopy', J. Materials Science 27, 1992, 1663–1670.10.1007/BF00542931 ↗
10. Wagner, H. D., 'Interfaces in Microcomposites and Macrocomposites: The Issue of Thermal Residual Stresses', Composite Interfaces (1994) 2 (5), 1995, 321–336._See also H. D. Wagner, 'Solution of the Thermal Residual Stress Problem in Composites with Anisotropic Interphases', Physical Review B 53 (9) (1 March 1996-I), 5055–5058.10.1163/156855494X00166 ↗
11. Incardona, S. Migliaresi, C., Wagner, H. D., Gilbert, A. H., and Marom, G., 'The Mechanical Role of the Fiber-Matrix Transcrystalline Interphase in Carbon Fiber Reinforced J-Polymer Microcomposites', Composites Science and Technology 47, 1993, 43–50.10.1016/0266-3538(93)90094-W ↗
12. Wagner, H. D., Wood, J. R., and Marom, G., 'Claryfying the Application of Weibull Statistics for Determining the Stress State of a Fiber from Fragmentation Tests', Advanced Composites Lett. 2 (5), 1993, 172–176.
13. Wagner, H. D. and Nairn, J. A., 'Thermal Residual Stresses in Three Concentric Transversely Isotropic Cylinders: Application to Thermoplastic Matrix Composites Containing a Transcrystalline Interphase', Composites Science and Technology 57 (9–10), 1997, 1289–1302.10.1016/S0266-3538(97)00058-4 ↗
14. Robinson, I. M., Jahankhani, M., Day, R. J., Young, R. J., and Galiotis, C., 'TITLE', J. Materials Science Lett. 6, 1987, 1212.10.1007/BF01729187 ↗
15. Amer, M. S., Koczak, M. J., Galiotis, C., and Schadler, L. S., 'Environmental Degradation Studies of the Interface in Single-Filament Graphite/Epoxy Composites Using Laser Raman Spectroscopy', Advanced Composites Lett. 3 (1), 1994, 17.
16. Melanitis, N., Tetlow, P., Galiotis, C., and Davies, C., 'Monitoring the Micromechanics of Reinforcement in Carbon Fiber/Epoxy Resin Systems', J. Materials Science 28, 1993, 1648.10.1007/BF00363362 ↗
17. Piggott, M. R., 'Interface Properties and Their Influence on Fiber reinforced Polymers', in T. Vigo and B. Kunzig (eds.), Composite Application: The Role of Matrix, Fiber, and Interface, Part III, Chapter 9, 1992, p. 232.
18. Amer, M. S., and Schadler, L. S., 'Stress Concentration Phenomenon in Graphite/Epoxy Composites; Tension / Compression Effects', Composites Science and Technology 57, 1997, 1129–1137.10.1016/S0266-3538(96)00181-9 ↗
19. Nairn, J. A., 'Thermoelastic Analysis of Residual Stresses in Unidirectional High-Performance Composites', Polymer Composites 6 (2), 1985, 123–130.10.1002/pc.750060211 ↗
20. Wood, J. R., Huang, Y., Young, R. J., and Marom, G., 'Measurement of the Thermal Strains During Compressive Fragmentation in Single-Fibre Composites by Raman Spectroscopy', Composites Science and Technology 55, 1995, 223–229.10.1016/0266-3538(95)00082-8 ↗
21. Saado, Y., Wood, J. R., and Marom, G., 'Thermal Shrinkage Induced Compressive Fragmentation in Composite Materials', Composite Interfaces 5 (1997), 117–124.10.1163/156855497X00091 ↗
22. Paiva, M. C., Nardin, M. Bernardo, C. A., and Schultz, J., 'Influence of Thermal History on the Results of Fragmentation Tests on High Modulus Carbon-Fiber/Polycarbonate Model Composites', Composites Science and Technology 57, 1997, 839–844.10.1016/S0266-3538(96)00173-X ↗
23. Nardin, M., Personal communication, 1994.
24. Narayanan, S. and Schadler, L. S., 'Assessment of Strains Along Fiber Surface Features in Graphite Epoxy Composites Loaded in Compression', Composites Science and Technology, in press.