journal article·2025-06Open access

Production of Parallel Aligned Nanofiber Rovings From Continuous Bundles

Behzat Yıldırım, Ali Kılıç, Halil İbrahim İçoğlu, Mehmet Topalbekiroğlu

Advanced Materials Technologies· Volume 10· Issue 12

Abstract

Abstract This study presents a novel approach to converting electrospun polyacrylonitrile (PAN) nanofiber bundles into rovings, essential for nanofiber yarn spinning, through the implementation of false twisting and drawing processes. The false twisting process is optimized by varying the input bundle angle (40° to 60°), twister type (A, B, C), and rotation speed (20, 50, and 80 rpm). A bundle input angle of 55°, twister type B, and a twister rotation speed of 80 rpm show the best results in terms of longer twisted length, lower average thickness, and thickness variation values. The morphological, physical, and mechanical properties of the resulting nanofiber rovings for drawing process implementation are also evaluated. Scanning electron microscope (SEM) analysis further reveals significant improvements in nanofiber alignment and uniformity. The drawing process reduces the average nanofiber diameter from 297 to 200 nm and decreases the standard deviation of alignment angles from 14.2° to 8.1°, indicating a substantial enhancement in parallel nanofiber alignment. These morphological changes contribute to a marked increase in tensile strength from 2.2 to 3.3 cN tex−1. Integrating false twisting and drawing processes in electrospun nanofiber production can significantly enhance the mechanical properties and alignment of nanofibers, making them more suitable for advanced textile applications.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Electrospun Nanofibers in Biomedical Applications · Advanced Sensor and Energy Harvesting Materials · Additive Manufacturing and 3D Printing Technologies

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Textile Engineering Gaziantep University Gaziantep TR27310 Turkey

Uluğ Bey High Technology Application and Research Center (ULUTEM) Gaziantep University Gaziantep TR27310 Turkey

Department of Mechanical Engineering Gaziantep University Gaziantep TR27310 Turkey

Funding

Türkiye Bilimsel ve Teknolojik Araştirma Kurumu

References (79)

Show source-provided references
1. 10.1002/app.2148110.1002/app.21481 ↗
2. 10.1021/acs.chemrev.8b0059310.1021/acs.chemrev.8b00593 ↗
3. 10.1002/app.5558010.1002/app.55580 ↗
4. 10.1016/B978-0-08-100550-7.00011-510.1016/B978-0-08-100550-7.00011-5 ↗
5. 10.1080/00405000.2017.129320410.1080/00405000.2017.1293204 ↗
6. 10.1080/00405000.2011.55225410.1080/00405000.2011.552254 ↗
7. 10.1038/s41598-021-99890-w10.1038/s41598-021-99890-w ↗
8. Nguyen T. · Micromachines · 2023 · 14
9. 10.1016/j.msec.2008.10.03710.1016/j.msec.2008.10.037 ↗
10. 10.1080/0040500070146397910.1080/00405000701463979 ↗
11. 10.1016/j.polymer.2004.04.00110.1016/j.polymer.2004.04.001 ↗
12. 10.1016/j.polymer.2006.05.01210.1016/j.polymer.2006.05.012 ↗
13. 10.3390/nano710029310.3390/nano7100293 ↗
14. 10.1016/j.carbon.2018.06.02210.1016/j.carbon.2018.06.022 ↗
15. 10.1016/j.ensm.2019.04.04310.1016/j.ensm.2019.04.043 ↗
16. 10.1016/j.apmt.2019.06.01510.1016/j.apmt.2019.06.015 ↗
17. 10.1021/nl034425610.1021/nl0344256 ↗
18. 10.1002/polb.2081410.1002/polb.20814 ↗
19. 10.1002/app.2429010.1002/app.24290 ↗
20. 10.1063/1.264437910.1063/1.2644379 ↗
21. 10.1002/mame.20090040610.1002/mame.200900406 ↗
22. 10.1088/0957-4484/12/3/32910.1088/0957-4484/12/3/329 ↗
23. 10.1088/0957-4484/24/25/25570810.1088/0957-4484/24/25/255708 ↗
24. 10.1016/j.polymer.2005.02.00210.1016/j.polymer.2005.02.002 ↗
25. 10.1016/j.polymer.2007.04.04410.1016/j.polymer.2007.04.044 ↗
26. 10.1039/C9NR00446G10.1039/C9NR00446G ↗
27. 10.1080/00405000.2020.178927410.1080/00405000.2020.1789274 ↗
28. 10.1002/marc.20070087310.1002/marc.200700873 ↗
29. 10.1002/app.3080710.1002/app.30807 ↗
30. 10.1016/j.matlet.2017.10.05510.1016/j.matlet.2017.10.055 ↗
31. 10.1007/s12221-018-8011-810.1007/s12221-018-8011-8 ↗
32. 10.1002/polb.2200310.1002/polb.22003 ↗
33. 10.1016/j.polymer.2008.04.01510.1016/j.polymer.2008.04.015 ↗
34. 10.1002/pen.2370510.1002/pen.23705 ↗
35. 10.1002/jbm.b.3012210.1002/jbm.b.30122 ↗
36. Chvojka J. · Fibres Text. East. Eur. · 2013 · 98 · 21
37. 10.1002/app.2752410.1002/app.27524 ↗
38. 10.2147/IJN.S14399010.2147/IJN.S143990 ↗
39. B.Barua PhD Thesis University of Oklahoma Norman OH USA2015.
40. 10.1002/app.2867310.1002/app.28673 ↗
41. 10.1021/am508812a10.1021/am508812a ↗
42. 10.1016/j.biomaterials.2008.03.03110.1016/j.biomaterials.2008.03.031 ↗
43. 10.1021/acsnano.5b0364410.1021/acsnano.5b03644 ↗
44. 10.1021/acsami.1c0098310.1021/acsami.1c00983 ↗
45. 10.1016/j.polymer.2004.11.07510.1016/j.polymer.2004.11.075 ↗
46. L.Javazmi S. A.Hosseini Ravandi M. E.Sharifkhani inProc. of the 2018 Int. Conf. on Nanoscience and Nanotechnology Wollongong Australia Jan‐Feb2018.
47. 10.1002/marc.20100046310.1002/marc.201000463 ↗
48. 10.1016/j.matlet.2021.13022910.1016/j.matlet.2021.130229 ↗
49. 10.1063/1.275310910.1063/1.2753109 ↗
50. 10.1021/acs.iecr.6b0068610.1021/acs.iecr.6b00686 ↗
51. J. R.Lee S. Y.Jee H. J.Kim Y. T.Hong S.Kim S. J.Park WIPO WO2006123879A12006.
52. A. F.Lotus PhD Thesis The University of Akron Akron OH USA2009.
53. 10.1533/978185573765510.1533/9781855737655 ↗
54. R. Z.Naar PhD Thesis Massachusetts Institute of Technology Cambridge MA USA1975.
55. 10.1080/0040500770863138310.1080/00405007708631383 ↗
56. Demir A. · Chem Fibers Int. · 1996 · 46 · 361
57. 10.1080/0040500750863050710.1080/00405007508630507 ↗
58. 10.1080/0040500750863050810.1080/00405007508630508 ↗
59. 10.1080/0040500750863053710.1080/00405007508630537 ↗
60. 10.1088/0022-3727/10/5/00110.1088/0022-3727/10/5/001 ↗
61. 10.1016/j.matlet.2012.04.00510.1016/j.matlet.2012.04.005 ↗
62. B.Kim J.Bykova L.Plata Y.Yang M. D.Lima US Patent U.S. Patent No. 11913142 2024.
63. C.Kim S.Lee J.Seok J.Ryu D. H.Kim US Patent U.S. Patent US10648105 2020.
64. H. Y.Kim U.S. Patent Application No. US20090324950 2009.
65. 10.1016/j.polymer.2010.11.04410.1016/j.polymer.2010.11.044 ↗
66. 10.1088/1758-5090/7/2/02500610.1088/1758-5090/7/2/025006 ↗
67. 10.1177/152808371774074110.1177/1528083717740741 ↗
68. 10.1016/j.matdes.2019.10762010.1016/j.matdes.2019.107620 ↗
69. 10.1016/j.mtcomm.2022.10496610.1016/j.mtcomm.2022.104966 ↗
70. 10.1016/j.mtcomm.2024.10902510.1016/j.mtcomm.2024.109025 ↗
71. 10.1002/adem.20240098910.1002/adem.202400989 ↗
72. 10.1002/app.2694910.1002/app.26949 ↗
73. 10.1016/j.actbio.2018.02.00910.1016/j.actbio.2018.02.009 ↗
74. 10.1080/00405000.2014.92224510.1080/00405000.2014.922245 ↗
75. Das A. · Indian J.Fibre Text Res. · 2002 · 27 · 135
76. 10.1177/004051751982992610.1177/0040517519829926 ↗
77. 10.1177/00405175040740050610.1177/004051750407400506 ↗
78. 10.1016/S0079-6425(02)00003-810.1016/S0079-6425(02)00003-8 ↗
79. 10.1002/ppap.20140001810.1002/ppap.201400018 ↗