journal article·2021-12Open access

Synthesis and characterization of ultra-fine titania powders for wastewater treatment

Mineral Processing Research Centre, Pakistan Council of Scientific and Industrial Research, Ferozepur Road, Lahore, Pakistan, S. Zahra, F. Deeba, Centre for Enviromental Protection, Pakistan Council of Scientific and Industrial Research, Ferozepur Road, Lahore, Pakistan, M. Irshad, Department of Chemistry, DSNT, University of Education, College Road, Township, Lahore, Pakistan, A. Sheikh, Mineral Processing Research Centre, Pakistan Council of Scientific and Industrial Research, Ferozepur Road, Lahore, Pakistan, S. Zahra, Department of Physics, DSNT, University of Education, College Road, Township, Lahore, Pakistan, A. M. Khan, Department of Chemistry, DSNT, University of Education, College Road, Township, Lahore, Pakistan

Abstract

Ultra-fine titania powders were synthesized through sol-gel method. A surfactant-free nonaqueous approach was followed as a quite suitable alternative to surfactants using titanium tetrachloride and 2-ethyl hexanol as precursors. The prepared samples were calcined at different temperatures ranging from 500 ºC to 800 ºC. The crystal structure and thermal stability of metal oxide particles were studied using X-ray diffraction technique (XRD) and differential scanning calorimetry (DSC-TGA) respectively. The purity of powders was checked by infrared spectroscopy (IR) whereas the surface morphology was studied by field emission scanning electron microscopy (FESEM). The prepared titania samples were employed for the reduction of cyanide, BOD, COD, TDS, color and pH of industrial wastewater.
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Research context

OpenAlex topics: TiO2 Photocatalysis and Solar Cells · Advanced Photocatalysis Techniques · Gas Sensing Nanomaterials and Sensors

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