journal article·2019-07-26Open access

Assessment of characteristics and cytotoxic effects of 316L stainless steel coated with a new titanium oxide nano-structure coating method

Xiaoxi HE, Alireza VALANEZHAD, Ikuya WATANABE, Noriaki YOSHIDA

Dental Materials Journal· Volume 38· Issue 4

Abstract

In order to fabricate the TiO2 nano-structure coating on the Ti-free stainless steel with good adhesion, commercially obtained 316L stainless steel (316L SS) plates were chemically treated by KOH aqueous solution including TiH2 powder at 60C for 3 days in an oil bath shaker, and subsequently heated up to 550-800C under the air atmosphere. The crystal structure, color, adhesive strength and cytotoxic effects of coating were investigated. Fiber-like hydrogen titanate nano-structures were formed on the 316L SS surface and made a fine network. X-ray diffraction (XRD) patterns showed that hydrogen titanate phase converted to anatase and rutile after heat treatment above 550C. The heat treated sample at 800C for 1 h showed the highest adhesive strength and the lowest cytotoxicity. The alkali treatment method in this study is expected to be used on the other Ti-free metals with further research.
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Research context

OpenAlex topics: Bone Tissue Engineering Materials · TiO2 Photocatalysis and Solar Cells · Nanoparticles: synthesis and applications

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Orthodontics and Dentofacial Orthopedics, Graduate School of Biomedical Sciences, Nagasaki University

Department of Dental and Biomedical Materials Science, Graduate School of Biomedical Sciences, Nagasaki University

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