Microwave‐Induced Controlled Purification of Single‐Walled Carbon Nanotubes without Sidewall Functionalization
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Abstract
Abstract A microwave‐induced controlled method for the purification of single‐walled carbon nanotubes (SWCNTs) by removing residual metal catalysts and carbonaceous impurities is reported. Compared to conventional strong acid treatment, this one‐step method uses dilute acids and complexing agents and reduces the reaction times to the order of minutes. Furthermore, the SWCNTs retain their chemical and physical properties and are not functionalized. Electron microscopy, Raman spectroscopy, Fourier transform infrared (FTIR) spectroscopy, thermogravimetric analysis (TGA) and atomic absorption (AA) spectrometry studies were used to characterize the purified SWCNTs.
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Research context
OpenAlex topics: Carbon Nanotubes in Composites · Microwave-Assisted Synthesis and Applications · Graphene research and applications
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