journal article·2020-08-11Open access

Kinetics of Capability Aging in Ti-13Nb-13Zr Alloy

Myoungjae Lee, In-Su Kim, Young Hoon Moon, Hyun Sik Yoon, Chan Hee Park, Taekyung Lee

Crystals· Volume 10· Issue 8

Abstract

Metals for biomedical implant applications require a simultaneous achievement of high strength and low Young’s modulus from the viewpoints of mechanical properties. The American Society for Testing and Materials (ASTM) standards suggest two types of processing methods to confer such a mechanical performance to Ti-13Nb-13Zr alloy: solution treatment (ST) and capability aging (CA). This study elucidated the kinetics of CA process in Ti-13Nb-13Zr alloy. Microstructural evolution and mechanical change were investigated depending on the CA duration from 10 min to 6 h. The initial ST alloy possessed the full α′-martensitic structure, leading to a low strength, low Young’s modulus, and high ductility. Increasing CA duration increased mechanical strength and Young’s modulus in exchange for the reduction of ductility. Such a tendency is attributed to the decomposition of α′ martensite into (α+β) structure, particularly hard α precipitates. Mechanical compatibility (i.e., Young’s modulus compensated with a mechanical strength) of Ti-13Nb-13Zr alloy rarely increased by changing CA duration, suggestive of the intrinsic limit of static heat treatment.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Titanium Alloys Microstructure and Properties · Intermetallics and Advanced Alloy Properties · Orthopaedic implants and arthroplasty

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

School of Mechanical Engineering, Pusan National University, Busan 46241, Korea

Advanced Metals Division, Korea Institute of Materials Science, Changwon 51508, Korea

Department of Naval Architecture and Ocean Engineering, Pusan National University, Busan 46241, Korea

Funding

National Research Foundation of Korea

References (27)

Show source-provided references
1. Incorporation of Ca ions into anodic oxide coatings on the Ti-13Nb-13Zr alloy by plasma electrolytic oxidation10.1016/j.msec.2019.109957 ↗
2. Kolli, R., and Devaraj, A. (2018). A Review of Metastable Beta Titanium Alloys. Metals, 8.10.3390/met8070506 ↗
3. ASTM F1713-08(2013) (2013). Standard Specification for Wrought Titanium-13Niobium-13Zirconium Alloy for Surgical Implant Applications (UNS R58130), ASTM International.
4. Mechanical biocompatibilities of titanium alloys for biomedical applications10.1016/j.jmbbm.2007.07.001 ↗
5. Corrosion wear fracture of new β type biomedical titanium alloys10.1016/S0921-5093(98)01167-8 ↗
6. Breaking the limit of Young’s modulus in low-cost Ti-Nb-Zr alloy for biomedical implant applications10.1016/j.jallcom.2020.154401 ↗
7. Enhanced mechanical compatibility of submicrocrystalline Ti-13Nb-13Zr alloy10.1016/j.msea.2010.04.057 ↗
8. Effect of thermomechanical processing on microstructure of a Ti-13Nb-13Zr alloy10.1016/S0925-8388(01)01604-8 ↗
9. The role of heat treatment on microstructure and mechanical properties of Ti-13Zr-13Nb alloy for biomedical load bearing applications10.1016/j.jmbbm.2011.03.023 ↗
10. Influence of microstructure and alloying elements on corrosion behavior of Ti-13Nb-13Zr alloy10.1016/S0010-938X(03)00186-0 ↗
11. Elastic modulus of biomedical titanium alloys by nano-indentation and ultrasonic techniques-A comparative study10.1016/j.msea.2007.12.029 ↗
12. Microstructure tailoring to enhance strength and ductility in Ti-13Nb-13Zr for biomedical applications10.1016/j.scriptamat.2013.08.028 ↗
13. On the grain size refinement of TiAl alloys by cyclic heat treatment10.1016/S0921-5093(01)01543-X ↗
14. Electrochemical corrosion behaviour of nanotubular Ti-13Nb-13Zr alloy in Ringer’s solution10.1016/j.corsci.2009.04.013 ↗
15. Microstructure and mechanical performance tailoring of Ti-13Nb-13Zr alloy fabricated by selective laser melting after post heat treatment10.1016/j.jallcom.2018.10.030 ↗
16. Microstructural evolution and strain-hardening behavior of multi-pass caliber-rolled Ti-13Nb-13Zr10.1016/j.msea.2015.09.062 ↗
17. Lowering of elastic modulus in the near-beta Ti-13Nb-13Zr alloy through heat treatment10.1080/02670836.2020.1732608 ↗
18. New surface-hardened, low-modulus, corrosion-resistant Ti13Nb13Zr alloy for total hip arthroplasty
19. Phase Decomposition in a Ti-13Nb-13Zr Alloy during Aging at 600 °C10.2320/matertrans.43.2956 ↗
20. The competition between martensite and omega in quenched Ti-Nb alloys10.1007/BF02645135 ↗
21. Influence of Thermal Treatment on the Microstructure, Mechanical Properties, and Corrosion Resistance of Newly Developed Ti20Nb13Zr Biomedical Alloy in a Simulated Body Environment10.1007/s11665-019-03908-4 ↗
22. Influence of tempering temperature and time on the α′-Ti-6Al-4V martensite10.1016/0925-8388(95)02057-8 ↗
23. Young’s modulus and mechanical properties of Ti-29Nb-13Ta-4.6Zr in relation to α″ martensite10.1007/s11661-002-0299-7 ↗
24. Effects of Ta content on Young’s modulus and tensile properties of binary Ti-Ta alloys for biomedical applications10.1016/j.msea.2003.12.011 ↗
25. Microstructures and mechanical properties of metastable [beta] TiNbSn alloys cold rolled and heat treated10.1016/j.jallcom.2006.08.267 ↗
26. Fatigue behavior of arc melted Ti–13Nb–13Zr alloy10.1016/j.ijfatigue.2004.01.011 ↗
27. Influence of martensitic transformation on mechanical compatibility of biomedical β type titanium alloy TLM10.1016/j.msea.2005.12.079 ↗