journal article·2020-09Open access

Correlative Nano‐Computed Tomography and Focused Ion‐Beam Sectioning: A Case Study on a Co‐Base Superalloy Oxide Scale

Malte Lenz, Janis Wirth, Silvan Englisch, Jan Rosiwal, Nadine Buchinger, Martin Weiser, Sannakaisa Virtanen, Benjamin Apeleo Zubiri, Erdmann Spiecker

Advanced Engineering Materials· Volume 22· Issue 9

Abstract

Herein, the capabilities of a correlative tomography approach combining laboratory nano X‐ray computed tomography, focused ion‐beam sectioning, and energy‐dispersive X‐ray spectroscopy are utilized for the characterization of multilayered oxide scales of Co‐base superalloys regarding their 3D morphology and chemical composition. The combination of complementary 3D imaging techniques allows for a precise and reliable segmentation of the pore space, oxide precipitates, and different phases of the initial material. Such information is instrumental to a microscopic understanding of oxidation in this new class of superalloys and key to improvement of oxidation resistance in the next‐generation high‐temperature materials.
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Research context

OpenAlex topics: High Temperature Alloys and Creep · Nuclear Materials and Properties · Advanced Materials Characterization Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Institute of Micro- and Nanostructure Research (IMN) & Center for Nanoanalysis and Electron Microscopy (CENEM) Interdisciplinary Center for Nanostructured Films (IZNF) Friedrich-Alexander-Universität Erlangen-Nürnberg Cauerstraße 3 Erlangen 91058 Germany

Institute for Surface Science and Corrosion Friedrich-Alexander-Universität Erlangen-Nürnberg Martensstraße 7 Erlangen 91058 Germany

Funding

Deutsche Forschungsgemeinschaft

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