journal article·2025-01

Effect of process parameters on microstructure and properties of W-Ti-Zr-Nb tungsten alloy fabricated by LPBF

Yuchen Mu, Chunjie Shen, Zhuo Li, Shujing Shi, Lin Xiong

Publisher page

Abstract

A novel tungsten alloy with the composition 73W-9Ti-9Zr-9Nb was successfully fabricated by Laser Powder Bed Fusion (LPBF). This study investigates the relationship between process parameters and the microstructure, defects, phases and mechanical properties of the alloy. The results revealed that with an increase in the laser power ( P) from 50 to 100 W, the number of unmelted W particles decreased, transitioning the microstructure of the as-fabricated samples from W particles embedded in the Ti-Zr-Nb matrix to W dendrites within the Ti-Zr-Nb-W matrix. Simultaneously, the porosity decreased from 20.1 % to 0.1 % as the P increased. There was no W 2Zr brittle phase in W-Ti-Zr-Nb, and the interface between the W particles, W dendrites, and the matrix was well-bonded. the interfaces between the W particles, W dendrites, and the matrix were well-bonded. As a result of these optimized processing conditions, the sample processed at a P of 100 W exhibited optimal overall performance, achieving a microhardness of 612.8 HV and an ultimate compressive strength of 2410 MPa. Increasing the laser power improved the overall performance of the material by reducing defects, increasing the proportion of dendrites, and enhancing solution strengthening.
Source: expertdata · Quality: candidate unverified · Source record ↗

Research context

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (31)

Show source-provided references
1. Additive manufacturing of tungsten, tungsten-based alloys, and tungsten matrix composites10.1007/s42864-022-00153-6 ↗
2. Microstructure and mechanical properties of W-Zr reactive materials10.1016/j.msea.2016.02.009 ↗
3. Impact-initiated behavior and reaction mechanism of W/Zr composites with SHPB setup10.1063/1.4967340 ↗
4. Effect of Zr additions on crystal structures and mechanical properties of binary W–Zr alloys: A first-principles study10.1557/jmr.2018.426 ↗
5. Experimental study on impact-initiated characters of W/Zr energetic fragments10.1016/j.matdes.2015.06.107 ↗
6. Atomic interaction mechanism for designing the interface of W/Zr-based bulk metallic glass composites
7. Improving the damage potential of W-Zr reactive structure material under extreme loading condition10.1016/j.dt.2020.03.001 ↗
8. Effect of W powders characteristics on the Ti-rich phase and properties of W-10 wt.% Ti alloy10.1016/j.ijrmhm.2015.02.003 ↗
9. Quantitative strengthening evaluation of powder metallurgy Ti-Zr binary alloys with high strength and ductility10.1016/j.jallcom.2020.156954 ↗
10. Effect of increasing Ti content on the phase, interface, dynamic mechanical properties and ballistic performance of W-Ti-Zr alloys
11. Selective laser melting additive manufacturing of tungsten with niobium alloying: microstructure and suppression mechanism of microcracks10.1016/j.jallcom.2021.159879 ↗
12. Composition-dependent shuffle-shear coupling and shuffle-regulated strain glass transition in compositionally modulated Ti-Nb alloys10.1016/j.actamat.2023.118697 ↗
13. Structural transformations of ceramics forming during high-temperature Nitridation of Zr-Nb alloys10.1134/S0020168522050065 ↗
14. The relation between wetting and interfacial chemistry in the Zr-based BMGs/W system10.1016/j.jallcom.2016.08.181 ↗
15. Impact of mechanical activation on sintering kinetics and mechanical properties of ultrafine-grained 95W-Ni-Fe tungsten heavy alloys10.1016/j.jallcom.2018.09.176 ↗
16. Dynamic and quasi-static torsional behavior of tungsten heavy alloy specimens fabricated through sintering, heat-treatment, swaging and aging10.1016/S0921-5093(97)00547-9 ↗
17. A review on additive manufacturing of refractory tungsten and tungsten alloys
18. Microstructure and mechanical properties of additive manufactured W-Ni-Fe-co composite produced by selective laser melting10.1016/j.ijrmhm.2019.105111 ↗
19. Effect of processing parameters on microstructure and properties of tungsten heavy alloys fabricated by SLM10.1016/j.ijrmhm.2019.03.020 ↗
20. Towards selective laser melting of high-density tungsten10.3390/met13081431 ↗
21. Densification during sintering in the presence of a liquid phase. I. Theory10.1063/1.1735155 ↗
22. Binding mechanisms in selective laser sintering and selective laser melting10.1108/13552540510573365 ↗
23. High-density tungsten fabricated by selective laser melting: densification, microstructure, mechanical and thermal performance10.1016/j.optlastec.2019.03.018 ↗
24. Microstructure and mechanical properties of novel tungsten heavy alloys prepared using FeNiCoCrCu HEA as binder
25. New low-temperature sintering tungsten-nickel-antimony alloy: microstructure evolution and mechanical properties10.1016/j.ijrmhm.2022.105952 ↗
26. Effect of Fe addition in W-Ni-cu heavy alloy processed through powder metallurgy on microstructure and mechanical properties10.1016/j.jallcom.2023.172578 ↗
27. Sutrisna, development of ODS tungsten heavy alloys reinforced with Co9Al8W superalloy binder by mechanical alloying10.1016/j.jallcom.2022.163762 ↗
28. W-cu composites with excellent comprehensive properties10.1016/j.compositesb.2022.109664 ↗
29. The influence of pre-sintering temperature on the microstructure and properties of infiltrated ultrafine-grained tungsten-copper composites10.1016/j.jallcom.2020.153761 ↗
30. Microstructure and mechanical properties of hot isostatic pressed tungsten heavy alloy with FeNiCoCrMn high entropy alloy binder10.1016/j.jmrt.2022.12.078 ↗
31. Effect of sintering temperatures on grain coarsening behaviors and mechanical properties of W-NiTi heavy tungsten alloys10.3390/ma15228035 ↗