journal article·2004-07

Sintering of nanophase WC–15vol.%Co hard metals by rapid sintering process

Hwan-Cheol Kim, Dong-Young Oh, In-Jin Shon

Publisher page

Abstract

Abstract A sintering method for the rapid sintering of a nanostructured hard metals in short time is introduced with a focus on the manufacturing potential of this novel high-frequency induction heated sintering (HFIHS) process. The advantage of this process allows very quick densification to near theoretical density and prohibition of grain growth in nanostructured materials. In this work, we developed a new process of sintering for nanostructured WC–15vol.%Co hard metals. A highly dense WC–15vol.%Co with a relative density of up to 99.4% was produced with simultaneous application of 60 MPa pressure and induced current within 1 min. The average grain size was about 258 nm and mean free path was about 11.6 nm. The fracture toughness and hardness values obtained were 11.9 MPa m1/2 and 1992 HV30, respectively. Also, we produced dense WC–Co hard metals with a relative density of 97% without applying pressure.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (32)

Show source-provided references
1. Observation of Co nanoparticle dispersions in WC nanograins in WC–Co cermets consolidated from chemically synthesized powders10.1016/0965-9773(96)00028-1 ↗
2. Sintering and microstructure of nanophase WC/Co hardmetals10.1016/S0924-0136(96)02748-3 ↗
3. Nanostructured WC/Co composite powder prepared by high energy ball milling10.1016/j.scriptamat.2003.08.009 ↗
4. Experimental and simulation studies on grain growth in TiC and WC-based cermets during liquid phase sintering10.1007/BF03028212 ↗
5. Compared activities of platinum and high-surface-area Mo2C and WC catalysts for reforming reactions10.1016/0021-9517(92)90329-G ↗
6. Strength degradation of a tungsten carbide–cobalt composite at elevated temperature10.1016/S1044-5803(98)00056-4 ↗
7. Particle size, size distribution, and dislocations in nanocrystalline tungsten carbide10.1016/S0965-9773(99)00023-9 ↗
8. Adhesion properties of CVD diamond film on binderless sintered tungsten carbide prepared by the spark sintering method10.1016/S0925-9635(98)00242-8 ↗
9. An investigation of the influence of powder particle size on microstructure and hardness of bulk samples of tungsten carbide10.1016/S0032-5910(01)00391-6 ↗
10. Synthesis of tungsten carbide by dynamic shock compression of a tungsten–acetylene black powder mixture10.1016/S0925-8388(00)00700-3 ↗
11. Structure and properties of nanocrystalline TiC full-density bulk alloy consolidated from mechanically reacted powders10.1016/S0925-8388(00)00692-7 ↗
12. Two-step synthesis of nanostructured tungsten carbide–cobalt powders10.1016/S1359-6462(01)00668-6 ↗
13. Niihara · 1990
14. Nanocrystalline materials: A study of WC-based hard metals10.1016/S0079-6425(97)00021-2 ↗
15. Study of nanostructured WC–Co composites10.1016/0263-4368(95)92675-A ↗
16. On the formation of very large WC crystals during sintering of ultrafine WC–Co alloys10.1016/S0263-4368(01)00069-5 ↗
17. Spark plasma sintering behavior of nanocrystalline WC–10Co cemented carbide powders10.1016/S0921-5093(02)00605-6 ↗
18. Microstructure and mechanical properties of nanocrystalline WC–10Co cemented carbides10.1016/S1359-6462(01)00835-1 ↗
19. Hardness, and toughness of nanostructured and conventional WC–Co composites10.1016/S0965-9773(98)00123-8 ↗
20. Determination of three-dimensional grain size distribution by linear intercept measurement10.1016/S1359-6454(97)00442-4 ↗
21. Consolidation of nanocrystalline materials by compaction and sintering
22. Consolidation of powders under high pressure-cold sintering
23. Gutmanas EY, Lawley A. Processing of specialty alloys, composites and intermetallics from fine elemental powders. In: Andreotti ER, McGeehan PJ, editors. Advances in powder metallurgy, vol. 2. Princeton, NJ: 1990. p. 1–14
24. Plasma activated sintering of additive-free AlN powders to near-theoretical density in 5 minutes10.1557/JMR.1992.2643 ↗
25. Bazanov VN, Balankin SA, Grigoriev JeG, Gunichev VV, Novikov SV, Yartsev VA. in PM’90, PM into the 1990’s International Conference on Powder Metallurgy, London 1990. The Institute of Metals, London 1990. p. 270
26. Microstructure and mechanical properties of resistance sintered titanium10.1016/0956-716X(90)90079-V ↗
27. Effect of carbon content on the shape of WC grains during liquid phase sintering of WC–Co hard metals
28. A critical evaluation of indentation techniques for measuring fracture toughness: I. Direct crack measurements10.1111/j.1151-2916.1981.tb10320.x ↗
29. On the fracture toughness of cemented carbides10.1016/0001-6160(88)90143-5 ↗
30. On the toughness of brittle materials reinforced with a ductile phase10.1016/0001-6160(88)90149-6 ↗
31. One step synthesis and consolidation of WC–10vol.%Co hard material10.1007/BF03186093 ↗
32. Low and high temperature hardness of WC–6 wt.%Co alloys10.1016/S0263-4368(97)81231-0 ↗