journal article·2020-01-02

Synthesis of Magnetic Ordered Mesoporous Carbons (OMC) as an Electrochemical Platform for Ultrasensitive and Simultaneous Detection of Thebaine and Papaverine

Motahare Vakili Fathabadi, Hasan Hashemipour Rafsanjani, Mohammad Mehdi Foroughi, Shohreh Jahani, Nasrin Arefi Nia

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Abstract

Coal particles (<44 micron) in solid phase were used to successful synthesis of the magnetic ordered mesoporous carbons (MnFe 2 O 4 -OMC) in the present research. A tubular reactor was used to do reaction. Transmission and scanning electron microscopy (TEM and SEM) and X-ray diffraction (XRD) were applied to characterize the as-synthesized samples. Consequently, synthesis of mesoporous carbon was observed in tubular form. In order to prove its utilization, the as-prepared MnFe 2 O 4 -OMC has been applied as a modifier for simultaneous electro-chemical detection of thebaine and papaverine. It has been demonstrated that the electrode response has been linear from 0.01 and 500.0 μ M with a limit of detection of 0.0036 and 0.01 μ M (3 s m −1 ) through DPV for thebaine and papaverine. Moreover, modified electrode has been employed for determining thebaine and papaverine in urine specimens.
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Research context

OpenAlex topics: Electrochemical sensors and biosensors · Electrochemical Analysis and Applications · Advanced Chemical Sensor Technologies

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References (46)

Show source-provided references
1. Thebaine in hair as a marker for chronic use of illegal opium poppy substances10.1016/j.forsciint.2010.05.013 ↗
2. A rapid and reliable solid phase extraction method for high-performance liquid chromatographic analysis of opium alkaloids from papaver plants10.1248/cpb.53.1446 ↗
3. Determination of opiate alkaloids in process liquors using capillary electrophoresis10.1016/j.jpba.2006.09.040 ↗
4. Liquid chromatography of alkaloids, drugs, and nitrogen heterocycles on a porous polymer10.1021/ac50062a044 ↗
5. A novel highly sensitive thebaine sensor based on MWCNT and dandelion-like Co3O4 nanoflowers fabricated via solvothermal synthesis10.1016/j.microc.2019.103980 ↗
6. GC-MS detection and characterization of thebaine as a urinary marker of opium use10.1007/s11419-007-0028-4 ↗
7. Automated multiple development thin-layer chromatography for separation of opiate alkaloids and derivatives10.1016/j.chroma.2005.05.023 ↗
8. Development of an indirect competitive ELISA for the determination of papaverine10.1016/j.talanta.2005.01.001 ↗
9. Estimated world requirements of narcotic drugs for 1957
10. Facile fabrication of 3D dandelion-like cobalt oxide nanoflowers and its functionalization in the first electrochemical sensing of oxymorphone: evaluation of kinetic parameters at the surface electrode10.1149/2.0511914jes ↗
11. Macro- and microstructural tracking of ageing-related changes of papaverine hydrochloride-loaded electrospun nanofibrous buccal sheets10.1016/j.jpba.2017.05.035 ↗
12. Papaverine improves sublingual blood flow in patients with septic shock10.1016/j.jss.2015.01.016 ↗
13. Electromembrane extraction followed by high performance liquid chromatography: an efficient method for extraction and determination of morphine, oxymorphone, and methylmorphine from urine samples10.1039/C4AY00480A ↗
14. Lanthanum doped fern-like CuO nanoleaves/MWCNTs modified glassy carbon electrode for simultaneous determination of tramadol and acetaminophen10.1016/j.snb.2019.01.069 ↗
15. Preparation and characterization of PbO2–CeO2 nanocomposite electrode with high cerium content and its appplication in the electrocatalytic degradation of malachite green physical and analytical electrochemistry, electrocatalysis, and photoelectrochemistry10.1149/2.0961509jes ↗
16. The effect of ultrasonic irradiation on the morphology of NiO/Co3O4 nanocomposite and its application to the simultaneous electrochemical determination of droxidopa and carbidopa10.1016/j.ultsonch.2019.04.002 ↗
17. Inkjet-printed carbon nanotube electrodes with low sheet resistance for electrochemical sensor applications10.1149/2.008402jes ↗
18. Voltammetric determination of droxidopa in the presence of tryptophan using a nanostructured base electrochemical sensor10.33961/JECST.2018.9.2.109 ↗
19. Sensitive detection of morphine in the presence of dopamine with La3+ doped fern-like CuO nanoleaves/MWCNTs modified carbon paste electrode10.1016/j.molliq.2019.03.135 ↗
20. MnCo2O4-rGO hybrid magnetic nanocomposite modified glassy carbon electrode for sensitive detection of L-tryptophan10.1149/2.1251910jes ↗
21. Fabrication of a new electrochemical sensor for simultaneous determination of codeine and diclofenac using synergic effect of feather-type La3+–ZnO nano-flower10.1149/2.1051906jes ↗
22. A label-free electrochemical DNA aptasensor for the detection of dopamine10.1149/2.0501603jes ↗
23. Electroanalysis of imidacloprid insecticide in river waters using functionalized multi-walled carbon nanotubes modified glassy carbon electrode10.1149/2.1541809jes ↗
24. Direct growth of ternary copper nickel cobalt oxide nanowires as binder-free electrode on carbon cloth for nonenzymatic glucose sensing10.1016/j.microc.2018.07.014 ↗
25. Evaluation of the usefulness of an electrochemical sensor in detecting ascorbic acid using a graphite screen-printed electrode modified with NiFe2O4 nanoparticles
26. A review on metal-organic frameworks: synthesis and applications10.1016/j.trac.2019.06.007 ↗
27. Effect of electronic coupling on the electrocatalytic performance of Ag–MFe2O4 (M=Co, Mn) nanocomposites10.1149/2.1781713jes ↗
28. Fabrication of hierarchical graphene@Fe3O4@SiO2@polyaniline quaternary composite and its improved electrochemical performance10.1016/j.jallcom.2015.02.062 ↗
29. Fe3O4-CNTs nanocomposites: inorganic dispersant assisted hydrothermal synthesis and application in lithium ion batteries10.1016/j.jssc.2014.02.016 ↗
30. Selective photodegradation of 1-methylimidazole-2-thiol by the magnetic and dual conductive imprinted photocatalysts based on TiO2/Fe3O4/MWCNTs10.1016/j.cej.2013.11.088 ↗
31. Enhanced electrochemical performance for EDLC using ordered mesoporous carbons (CMK-3 and CMK-8): role of mesopores and mesopore structures10.1016/j.jallcom.2018.11.348 ↗
32. Excellent performance of highly conductive porous Na-embedded carbon nanowalls for electric double-layer capacitors with a wide operating temperature range10.1039/C7TA01085K ↗
33. Preparation of hierarchical porous carbon from waste printed circuit boards for high performance electric double-layer capacitors10.1016/j.jpowsour.2016.05.054 ↗
34. Synthesis of carbon nanostructures from coal by chemical solid synthesis method10.1049/mnl.2016.0089 ↗
35. Synthesis and structural analysis of nanocrystalline MnFe2O410.1016/j.phpro.2014.10.053 ↗
36. Preparation and characterization of nano-sized magnetic particles LaCoO3 by ultrasonic-assisted coprecipitation method10.1080/15533174.2015.1031010 ↗
37. Bard · 2001
38. Development of a capillary electrophoresis method for the screening of human urine for multiple drugs of abuse10.1016/j.jchromb.2007.05.038 ↗
39. Determination of thebaine in water samples, biological fluids, poppy capsule, and narcotic drugs, using electromembrane extraction followed by high-performance liquid chromatography analysis10.1016/j.aca.2011.05.042 ↗
40. Simultaneous analysis of Thebaine, 6-MAM and six abused opiates in postmortem fluids and tissues using Zymark® automated solid-phase extraction and gas chromatography–mass spectrometry10.1016/j.jchromb.2005.05.031 ↗
41. Simultaneous chemiluminescence determination of thebaine and noscapine using support vector machine regression10.1016/j.saa.2009.12.021 ↗
42. Development of a voltammetric procedure for assay of thebaine at a multi-walled carbon nanotubes electrode: quantification and electrochemical studies10.1007/s10008-009-0921-3 ↗
43. Electrochemical determination of papaverine on Mg–Al layered double hydroxide/graphene oxide and CNT modified carbon paste electrode10.1109/JSEN.2016.2533429 ↗
44. Development of a new hplc method for determination of papaverine in presence of its photooxidation products
45. Determination of papaverine and cocaine by use of a precipitation system coupled on-line to an atomic absorption spectrometer10.1016/0731-7085(94)90028-0 ↗
46. Detection of papaverine for the possible identification of illicit opium cultivation10.1021/acs.analchem.6b03797 ↗