journal article·2012-04

Channel size distribution of complex three-dimensional microstructures calculated from the topological characterization of isodistance structures

V.W.L. Chan, K. Thornton

Acta Materialia· Volume 60· Issue 6-7
Publisher page

Abstract

Abstract We present a novel approach for quantifying the channel size distribution (CSD) of complex three-dimensional microstructures. The CSD, which characterizes the probability of finding a channel bottleneck with a given size, is difficult to measure for materials with complex microstructures that are extensively interconnected. More importantly, insights about the physical properties of these materials, such as transport properties, may be provided by their CSD. The CSD is measured by topological characterization of a distance function, which is calculated from complex microstructural data using the level set method. The newly developed method for calculating CSD is shown to be robust such that it is applicable to both smooth and discontinuous (bi-level) data. The method is demonstrated by calculating the CSDs for three-dimensional microstructures formed through conserved (Cahn–Hilliard) and nonconserved (Allen–Cahn) dynamics. We found significant differences between the two structures in their characteristic channel size and the width of their distributions, even though their genera, a measure of connectivity, are almost identical. The CSD, which was not previously available for complex microstructures, will provide a new means to correlate properties of composite materials with their performance.
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Research context

OpenAlex topics: Theoretical and Computational Physics · Advanced Materials Characterization Techniques · Nanoporous metals and alloys

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References (40)

Show source-provided references
1. ScienceDirect – scripta materialia: three-dimensional materials science10.1016/j.scriptamat.2005.11.048 ↗
2. Foreword: scripta materialia viewpoint set on 3D characterization and analysis of materials10.1016/j.scriptamat.2006.02.038 ↗
3. 3-D microstructural characterization: methods, analysis, and applications10.1007/BF02748490 ↗
4. Three-dimensional materials science: an intersection of three-dimensional reconstructions and simulations10.1557/mrs2008.123 ↗
5. Quantitative serial sectioning analysis10.1046/j.1365-2818.2001.00832.x ↗
6. Automated serial sectioning for 3-D analysis of microstructures10.1016/j.scriptamat.2006.01.019 ↗
7. Measurement of three-dimensional microstructure in a LiCoO2 positive electrode10.1016/j.jpowsour.2010.04.066 ↗
8. Three-dimensional reconstruction of a solid-oxide fuel-cell anode10.1038/nmat1668 ↗
9. 3D reconstruction and characterization of polycrystalline microstructures using a FIB-SEM system10.1016/j.matchar.2006.01.019 ↗
10. Morphological and topological analysis of coarsened nanoporous gold by x-ray nanotomography10.1063/1.3285175 ↗
11. First direct 3D visualisation of microstructural evolutions during sintering through X-ray computed microtomography10.1016/j.actamat.2004.09.027 ↗
12. On the application of Xray microtomography in the field of materials science10.1002/1527-2648(200108)3:8<539::AID-ADEM539>3.0.CO;2-6 ↗
13. A new femtosecond laser-based tomography technique for multiphase materials10.1002/adma.201003600 ↗
14. Design of a femtosecond laser assisted tomographic atom probe10.1063/1.2194089 ↗
15. Confocal laser scanning microscopy: applications in material science and technology10.1007/BF02744951 ↗
16. Phase field modeling of polycrystalline freezing10.1016/j.msea.2005.09.057 ↗
17. Phase-field approach to polycrystalline solidification including heterogeneous and homogeneous nucleation
18. Large-scale three-dimensional phase field simulation of gamma’-rafting and creep deformation10.1080/14786430903081990 ↗
19. Coarsening of bicontinuous structures via nonconserved and conserved dynamics10.1103/PhysRevE.75.021120 ↗
20. 3D reconstruction of microstructure in a commercial purity aluminum10.1016/j.scriptamat.2006.02.017 ↗
21. Topological complexity and the dynamics of coarsening10.1038/nmat1138 ↗
22. The morphological evolution of dendritic microstructures during coarsening10.1007/s11661-003-0084-2 ↗
23. Three-dimensional characterization of dendritic microstructures10.1016/S1359-6454(00)00355-4 ↗
24. The morphology of topologically complex interfaces10.1016/j.scriptamat.2008.10.032 ↗
25. Spatial correlations in symmetric and asymmetric bicontinuous structures10.1016/j.actamat.2009.08.049 ↗
26. On the use of 2-D moment invariants for the automated classification of particle shapes10.1016/j.actamat.2007.09.039 ↗
27. On the use of moment invariants for the automated analysis of 3D particle shapes10.1088/0965-0393/16/4/045008 ↗
28. The evolution of interfacial topology during coarsening10.1016/j.actamat.2005.10.010 ↗
29. Connectivity and topology of a phase-separating bicontinuous structure in a polymer mixture: direct measurements of coordination number, inter-junction distances and Euler characteristic10.1063/1.1607912 ↗
30. Topological similarity of sponge-like bicontinuous morphologies differing in length scale10.1002/1521-4095(20021118)14:22<1615::AID-ADMA1615>3.0.CO;2-S ↗
31. Interfacial and topological measurements of bicontinuous polymer morphologies10.1103/PhysRevE.64.010803 ↗
32. Multifunctionality of three-dimensional self-assembled composite structure10.1016/j.scriptamat.2009.03.006 ↗
33. On spinodal decomposition10.1016/0001-6160(61)90182-1 ↗
34. Mechanisms of phase transformations within the miscibility gap of Fe-rich Fe-Al alloys10.1016/0001-6160(76)90063-8 ↗
35. New algorithms for euclidean distance transformation of an n-dimensional digitized picture with applications10.1016/0031-3203(94)90133-3 ↗
36. A level set approach for computing solutions to incompressible two-phase flow10.1006/jcph.1994.1155 ↗
37. A PDE-based fast local level set method10.1006/jcph.1999.6345 ↗
38. A level-set method for the evolution of faceted crystals10.1137/S1064827599351921 ↗
39. Hyde · 1997
40. Marching cubes: a high resolution 3D surface construction algorithm10.1145/37402.37422 ↗