Improved understanding of the growth of blocky alpha in welded Zircaloy-4
Source abstract
Abstract
Zirconium alloys are widely used in nuclear reactors as fuel cladding materials. Fuel cladding is used to contain the nuclear fuel and cladding tubes are typically sealed using welds. Welding of zirconium alloys can result in changes in the local microstructure, with the potential to grow so called ‘blocky α’ grains in the welded region during subsequent thermal processing and these blocky α grains have the potential to be detrimental to the integrity of the component. In this work, complimentary heating experiments with ex situ and in situ electron backscatter diffraction (EBSD) analysis are used to aid understanding of the blocky α grain growth within the weld region. These experiments reveal that blocky α grain growth is related to the prior-β (high temperature) microstructure, as grains grow adjacent to a prior-β grain boundary and the orientation of the growing α grain can be explained using neighbourhood orientations from this prior-β grain. This growth mechanism is explained via a simple mechanism which is related to the α grain orientations, grain boundary structures and local stored energy. Ultimately, our findings indicate that the likely grain growth (size and morphology) across the weld region can now be predicted from the initial as-welded microstructure.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Nuclear Materials and Properties · Microstructure and mechanical properties · Titanium Alloys Microstructure and Properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (24)
Show source-provided references
1. Blocky Alpha Transformation in Zircaloy-4 Weldments10.1007/s11837-019-03604-7 ↗
2. D.D. Amick, “Method of quenching zirconium and alloys thereof,” no. US patent 3847684. 1974. [Online]. Available: https://www.google.co.uk/patents/US3847684.
3. Formation of very large ‘blocky alpha’ grains in Zircaloy-410.1016/j.actamat.2017.03.002 ↗
4. D.F. Washburn, “The formation of large grains in alpha zircaloy-4 during heat treatment after small plastic deformations,” 1964. [Online]. Available: https://www.osti.gov/biblio/4675033.
5. Temperature and time effects of post-weld heat treatments on tensile properties and microstructure of Zircaloy-410.1016/j.jnucmat.2021.152952 ↗
6. Microstructural evolution of β-quenched Zircaloy-4 during agings between 100 and 750°C10.1016/0022-3115(94)90226-7 ↗
7. “Zirconium, Zr, ” MatWeb Material property data. https://www.matweb.com/search/DataSheet.aspx?MatGUID=6e8936b3ad994f13bfb29923cc1506a9 (accessed Jun. 29, 2022).
8. On the process of transition of the cubic-body-centered modification into the hexagonal-close-packed modification of zirconium10.1016/S0031-8914(34)80244-3 ↗
9. Determination of the Orientation of a Parent β Grain from the Orientations of the Inherited α Plates in the Phase Transformation from Body-Centred Cubic to Hexagonal Close Packed10.1107/S0021889895004067 ↗
10. The calculation of a parent grain orientation from inherited variants for approximate (b.c.c.-h.c.p.) orientation relations10.1107/S0021889802005824 ↗
11. Back calculation of parent austenite orientation using a clustering approach10.1107/S002188981204914X ↗
12. Specific analysis of EBSD data to study the texture inheritance due to the β → α phase transformation10.1023/A:1022842712172 ↗
13. An advanced approach to reconstructing parent orientation maps in the case of approximate orientation relations: Application to steels10.1016/j.actamat.2012.04.034 ↗
14. ARPGE: A computer program to automatically reconstruct the parent grains from electron backscatter diffraction data10.1107/S0021889807048777 ↗
15. Reconstruction of deformed parent grains from microstructure inherited by phase transformations10.1016/j.scriptamat.2018.08.042 ↗
16. An automated method to determine the orientation of the high-temperature beta phase from measured EBSD data for the low-temperature alpha-phase in Ti-6Al-4V10.1016/S0921-5093(02)00844-4 ↗
17. A new method for automated reconstruction of pre-transformation microstructures10.1080/09500839.2016.1180436 ↗
18. Iterative determination of the orientation relationship between austenite and martensite from a large amount of grain pair misorientations10.1007/s11661-016-3462-2 ↗
19. Reconstruction of parent grains from EBSD data10.1016/j.matchar.2006.03.008 ↗
20. Effective structural unit analysis in hexagonal close-packed alloys – reconstruction of parent β microstructures and crystal orientation post-processing analysis10.1107/S1600576721011584 ↗
21. The development and applications of zirconium alloys10.1016/0261-3069(85)90165-7 ↗
22. Optimizing broad ion beam polishing of zircaloy-4 for electron backscatter diffraction analysis10.1016/j.micron.2022.103268 ↗
23. K.G. Lusby, “Investigation into Blocky Alpha Microstructures in Zircaloy-4 Welds,” 2017.
24. The beta to alpha phase transformation in zircaloy-410.1016/0022-3115(70)90216-3 ↗