Preparation of porous SiC-ceramics by sol–gel and spark plasma sintering
Source abstract
Abstract
A method for the production of porous SiC-ceramics from finely dispersed starting system SiO2–C by means of single-stage carbothermal process involving spark plasma sintering at moderate temperatures (≤1800 °C) is proposed. Synthesis of finely-dispersed SiO2–C system was performed by sol–gel as follows: tetraethoxysilane was hydrolyzed in the presence of polymeric source of carbon (phenolformaldehyde resin) with the subsequent drying and thermal treatment under inert atmosphere at 850 °C. The density of the obtained ceramic samples was found to vary within the range 1.43–1.84 g·cm−3 depending on the experimental conditions (the estimated porosity amounted to 42–55%). Ultimate compression strength was measured to be 94–279 MPa. Thermal behavior of materials in air flow up to 1400 °C, as well as microstructure and volumetric pore distribution (X-ray computerized microtomography), were studied.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · Recycling and utilization of industrial and municipal waste in materials production
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (55)
Show source-provided references
1. Bansal NP (2005) Handbook of ceramic composites. Kluwer Academic Publishers, Norwell10.1007/b104068 ↗
2. Katoh Y, Dong S, Kohyama A (2012) In: Kohyama A, Singh M, Lin H-T, Katoh Y (Ed) Advances in SiC/SiC ceramic composites: develeopments and applications in energy systems, ceramis transactions. Wiley, Hoboken, pp 77–8610.1002/9781118406014.ch6 ↗
3. Simonenko EP, Sevast’yanov DV, Simonenko NP, Sevast’yanov VG, Kuznetsov NT (2013) Promising ultra-high-temperature ceramic materials for aerospace applications. Russ J Inorg Chem 58:1669–169310.1134/S0036023613140039 ↗
4. Sevast’yanov VG, Simonenko EP, Gordeev AN, Simonenko NP, Kolesnikov AF, Papynov EK, Shichalin OO, Avramenko VA, Kuznesov NT (2013) Production of ultrahigh temperature composite materials HfB2-SiC and the study of their behavior under the action of a dissociated air flow. Russ J Inorg Chem 58:1269–127610.1134/S003602361311017X ↗
5. Kablov EN, Grashchenkov DV, Isaeva NV, Solntsev SS, Sevast’yanov VG (2012) Glass and ceramics based high-temperature composite materials for use in aviation technology. Glass Ceram 69:109–11210.1007/s10717-012-9425-1 ↗
6. Kablov EN, Grashchenkov DV, Isaeva NV, Solntsev SSt (2011) Perspective high-temperature ceramic composite materials. Russ J Gen Chem 81:986–99110.1134/S107036321105029X ↗
7. Wenbo H, Shanbao Z, Jihong Z (2014) Single-cycle thermal shock resistance of ZrB2–SiCnp ceramic composites. Ceram Int 40:16665–1666910.1016/j.ceramint.2014.08.028 ↗
8. Sevastyanov VG, Simonenko EP, Gordeev AN, Simonenko NP, Kolesnikov AF, Papynov EK, Shichalin OO, Avramenko VA, Kuznesov NT (2014) HfB2-SiC (45 vol %) ceramic material: manufacture and behavior under long-term exposure to dissociated air jet flow. Russ J Inorg Chem 59:1298–131110.1134/S0036023614110217 ↗
9. Wang L, Liang J, Fang G (2015) High temperature fracture behavior of ZrB2–SiC–graphite composite in vacuum and air. J Alloys Compd 619:145–15010.1016/j.jallcom.2014.08.255 ↗
10. Zhang X, Liu R, Xiong X, Chen Z (2015) Mechanical properties and ablation behavior of ZrB2–SiC ceramics fabricated by spark plasma sintering. Int J Refract Met Hard Mater 48:120–12510.1016/j.ijrmhm.2014.08.006 ↗
11. Sevastyanov VG, Simonenko EP, Gordeev AN, Simonenko NP, Kolesnikov AF, Papynov EK, Shichalin OO, Avramenko VA, Kuznesov NT (2014) HfB2-SiC (10–20 vol %) ceramic materials: manufacture and behavior under long-term exposure to dissociated air streams. Russ J Inorg Chem 59:1361–138210.1134/S0036023614120250 ↗
12. Carney C, Paul A, Venugopal S, Parthasarathy T, Binner J, Katz A, Brown P (2014) Qualitative analysis of hafnium diboride based ultra high temperature ceramics under oxyacetylene torch testing at temperatures above 2100°C. J Eur Ceram Soc 34:1045–105110.1016/j.jeurceramsoc.2013.11.018 ↗
13. Musa C, Orrù R, Sciti D, Silvestroni L, Cao G (2013) Synthesis, consolidation and characterization of monolithic and SiC whiskers reinforced HfB2 ceramics. J Eur Ceram Soc 33:603–61410.1016/j.jeurceramsoc.2012.10.004 ↗
14. Wäsche R, Klaffke D, Wötting G (2009) Tribological behaviour of structural Si-based ceramics in fretting tests at room temperature. Tribol Lett 33:211–21910.1007/s11249-009-9413-y ↗
15. Krenkel W, Heidenreich B, Renz R (2002) C/C-SiC composites for advanced friction systems. Adv Eng Mater 4:427–43610.1002/1527-2648(20020717)4:7<427::AID-ADEM427>3.0.CO;2-C ↗
16. Amanov A, Pyun Y, Kim J, Sasaki S (2014) Enhancement in wear resistance of sintered silicon carbide at various temperatures. Tribol Int 74:28–3710.1016/j.triboint.2014.01.027 ↗
17. Mukherjee M (2011) Silicon carbide - materials, processing and applications in electronic devices. InTech, Rijeka10.5772/852 ↗
18. Marsi N, Majlis BY, Hamzah AA, Mohd-Yasin F (2014) The mechanical and electrical effects of MEMS capacitive pressure sensor based 3C-SiC for extreme temperature. J Eng 2014:1–810.1155/2014/715167 ↗
19. Schroder DK (2013) Progress in SiC materials/devices and their competition. Selected topics in electronics and systems, In: Cristoloveanu S, Shur MS (Ed) Frontiers in Electronics, vol 53. World Scientific Publishing Co. Pte. Ltd., Singapore-New Jersey-London, pp 69–9210.1142/9789814541862_0005 ↗
20. Ropagnol X, Bouvier M, Reid M, Ozaki T (2014) Improvement in thermal barriers to intense terahertz generation from photoconductive antennas. J Appl Phys 116:043107/1–043107/710.1063/1.4891451 ↗
21. Schnabel M, Weiss C, Löper P, Canino M, Summonte C, Wilshaw PR, Janz S (2014) Nanocrystalline SiC formed by annealing of a-SiC:H on Si substrates: a study of dopant interdiffusion. J Appl Phys 116:024315/1–024315/1010.1063/1.4890030 ↗
22. Chen LY, Johnson RW, Neudeck PG, Beheim GM, Spry DJ, Meredith RD, Hunter GW (2012) Packaging technologies for 500°C SiC electronics and sensors. Mater Sci Forum 717-720:1033–103610.4028/www.scientific.net/MSF.717-720.1033 ↗
23. Scace RI, Slack GA (1960) Silicon carbide – a high temperature semiconductor. Pergamon Press, Oxford, London, New York, Paris
24. Karandikar P, Evans G, Klier E, Aghajanian M (2013) In: Halbig Michael MS, Narayan R, Colombo P (eds) Advances in bioceramics and porous ceramics V, vol 33(6). Wiley, Hoboken, NJ, USA, pp 153–161
25. Ledoux MJ, Pham-Huu C (2001) A novel catalyst support for heterogeneous catalysis. Cattech 5:226–24610.1023/A:1014092930183 ↗
26. Dhiman R, Johnson E, Skou EM, Morgen P, Andersen SM (2013) SiC nanocrystals as Pt catalyst supports for fuel cell applications. J Mater Chem A 1:6030–603610.1039/C3TA10238F ↗
27. Leroi P, Madani B, Pham-Huu C, Ledoux M-J, Savin-Poncet S, Bousquet JL (2004) Ni/SiC: a stable and active catalyst for catalytic partial oxidation of methane. Catal Today 91-92:53–5810.1016/j.cattod.2004.03.009 ↗
28. Keller N, Vieira R, Nhut J-M, Pham-Huu C, Ledoux MJ (2005) New catalysts based on silicon carbide support for improvements in the sulfur recovery: new silicon carbide nanotubes as catalyst support for the trickle-bed H2S oxidation. J Braz Chem Soc 16:514–51910.1590/S0103-50532005000400003 ↗
29. Marín P, Ordóñez S, Díez FV (2012) Performance of silicon-carbide foams as supports for Pd-based methane combustion catalysts. J Chem Technol Biotechnol 87:360–36710.1002/jctb.2726 ↗
30. Schaafhausen S, Yazhenskikh E, Heidenreich S, Müller M (2014) Corrosion of silicon carbide hot gas filter candles in gasification environment. J Eur Ceram Soc 34:575–58810.1016/j.jeurceramsoc.2013.10.011 ↗
31. Bläsing M, Schaafhausen S, Müller M (2014) Investigation of alkali induced corrosion of SiC filter candles at high temperature, in gasification environment. J Eur Ceram Soc 34:1041–104410.1016/j.jeurceramsoc.2013.10.035 ↗
32. Zhu S, Ding S, Xi H, Wang R (2005) Low-temperature fabrication of porous SiC ceramics by preceramic polymer reaction bonding. Mater Lett 59:595–59710.1016/j.matlet.2004.11.003 ↗
33. Fukushima M, Zhou Y, Yoshizawa Y (2009) Fabrication and microstructural characterization of porous SiC membrane supports with Al2O3–Y2O3 additives. J Membr Sci 339:78–8410.1016/j.memsci.2009.04.033 ↗
34. Suwanmethanond V, Goo E, Liu PKT, Johnston G, Sahimi M, Tsotsis TT (2000) Porous silicon carbide sintered substrates for high-temperature membranes. Ind Eng Chem Res 39:3264–327110.1021/ie0000156 ↗
35. Lin P-K, Tsai D-S (2005) Preparation and analysis of a silicon carbide composite membrane. J Am Ceram Soc 80:365–37210.1111/j.1151-2916.1997.tb02839.x ↗
36. Fukushima M, Zhou Y, Miyazaki H, Yoshizawa Y, Hirao K, Iwamoto Y, Yamazaki S, Nagano T (2006) Microstructural characterization of porous silicon carbide membrane support with and without alumina additive. J Am Ceram Soc 89:1523–152910.1111/j.1551-2916.2006.00931.x ↗
37. Iwamoto Y (2007) Precursors-derived ceramic membranes for high-temperature separation of hydrogen. J Ceram Soc Japan 115:947–95410.2109/jcersj2.115.947 ↗
38. Simonenko EP, Simonenko NP, Zharkov MA, Shembel NL, Simonov-Emel’yanov ID, Sevastyanov VG, Kuznetsov NT (2015) Preparation of high-porous SiC ceramics from polymeric composites based on diatomite powder. J Mater Sci 50:733–74410.1007/s10853-014-8633-1 ↗
39. Simonenko EP, Simonenko NP, Derbenev AV, Nikolaev NA, Grashchenkov DV, Kuznetsov NT (2013) Synthesis of nanocrystalline silicon carbide using the sol-gel technique. Russ J Inorg Chem 58:1143–115110.1134/S0036023613100215 ↗
40. Sevast’yanov VG, Simonenko EP, Ignatov NA, Ezhov YS, Kuznetsov NT (2010) Low-temperature synthesis of TaC through transparent tantalum-carbon containing gel. Inorg Mater 46:495–50010.1134/S0020168510050109 ↗
41. Simonenko EP, Ignatov NA, Simonenko NP, Ezhov YS, Sevastyanov VG, Kuznetsov NT (2011) Synthesis of highly dispersed super-refractory tantalum-zirconium carbide Ta4ZrC5 and tantalum-hafnium carbide Ta4HfC5 via sol-gel technology. Russ J Inorg Chem 56:1681–168710.1134/S0036023611110258 ↗
42. Sevastyanov VG, Simonenko EP, Ignatov NA, Ezhov YS, Simonenko NP, Kuznetsov NT (2011) Low-temperature synthesis of nanodispersed titanium, zirconium, and hafnium carbides. Russ J Inorg Chem 56:661–67210.1134/S0036023611050214 ↗
43. Ciudad E, Sánchez-González E, Borrero-López O, Guiberteau F, Nygren M, Ortiz AL (2013) Sliding-wear resistance of ultrafine-grained SiC densified by spark plasma sintering with 3Y2O3+5Al2O3 or Y3Al5O12 additives. Scr Mater 69:598–60110.1016/j.scriptamat.2013.07.007 ↗
44. Hotta M (2012) Microstructural control for ultrafine-grained non-oxide structural ceramics. J Ceram Soc Japan 120:123–13010.2109/jcersj2.120.123 ↗
45. He ZH, Katsui H, Tu R, Goto T (2014) Consolidation of SiC powder coated with SiO2 nanolayer by spark plasma sintering. Key Eng Mater 616:32–3610.4028/www.scientific.net/KEM.616.32 ↗
46. Rahman A, Singh A, Harimkar SP, Singh RP (2014) Mechanical characterization of fine grained silicon carbide consolidated using polymer pyrolysis and spark plasma sintering. Ceram Int 40:12081–1209110.1016/j.ceramint.2014.04.048 ↗
47. Suzuki TS, Uchikoshi T, Sakka Y (2014) Densification of SiC by colloidal processing and SPS without sintering additives. Adv Appl Ceram 113:85–8810.1179/1743676113Y.0000000133 ↗
48. Sahin FC, Apak B, Akin I, Kanbur HE, Genckan DH, Turan A, Goller G, Yucel O (2012) Spark plasma sintering of B4C–SiC composites. Solid State Sci 14:1660–166310.1016/j.solidstatesciences.2012.05.037 ↗
49. Fujisawa M, Hata T, Bronsveld P, Castro V, Tanaka F, Kikuchi H, Furuno T, Imamura Y (2004) SiC/C composites prepared from wood-based carbons by pulse current sintering with SiO2: electrical and thermal properties. J Eur Ceram Soc 24:3575–358010.1016/j.jeurceramsoc.2003.12.021 ↗
50. Zhou M, Rodrigo PDD, Wang X, Hu J, Dong S, Cheng Y-B (2014) A novel approach for preparation of dense TiC–SiC nanocomposites by sol–gel infiltration and spark plasma sintering. J Eur Ceram Soc 34:1949–195410.1016/j.jeurceramsoc.2014.01.028 ↗
51. Sevastyanov VG, Simonenko EP, Simonenko NP, Grashchenkov DV, Kablov EN, Kuznetsov NT (2013) Synthesis of SiC-whiskers via sol-gel technique in the bulk of SiC composite. In: The 19th international conference on composite materials, e-Proceedings, Montreal, 4695–4702
52. Kuznetsov NT, Sevast’janov VG, Simonenko EP, Ignatov NA, Simonenko NP, Ezhov YS (2008) Method for obtaining highly-dispersible refractory carbides for coating and composites based thereon. Patent RU No. 2333888, 20 Sept 2008
53. Kuznetsov NT, Sevast’yanov VG, Simonenko EP (2010) Finely dispersed refractory compounds for high-temperature ceramic matrix composite applications. Russ J Gen Chem 80:658–66510.1134/S107036321003045X ↗
54. Simonenko EP, Simonenko NP, Sevastyanov VG, Grashchenkov DV, Kuznetsov NT, Kablov EN (2011) Functionally graded composite material SiC/(ZrO2-HfO2-Y2O3) prepared via sol-gel technology. Composit Nanostr [Komposity i nanostructuri] 3:52–64
55. Sevastyanov VG, Ezhov YS, Simonenko EP, Kuznetsov NT (2004) Thermodynamic analysis of the production of silicon carbide via silicon dioxide and carbon. Mater Sci Forum 457-460:59–6210.4028/www.scientific.net/MSF.457-460.59 ↗