journal article·2018-02

Synthesis and characterization of pectin/SiO2 hybrid materials

Nadezhda Rangelova, Lyubomir Aleksandrov, Sanchi Nenkova

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Abstract

Amorphous hybrid materials with participation of water soluble biopolymer (pectin from apple-AP) and silica derived from tetraethoxy silane (TEOS) were synthesized by sol–gel method. The influence of biopolymer content was determined. The principles of the hybrids formation were developed using structural data from Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), Differential thermal analysis (DTA/TG), and 13C-Nuclear magnetic resonance (13C-NMR) analysis. The most probable model of interaction between pectin and silica network in the hybrid materials were proposed. It has been found that the reaction between the organic and the inorganic components was performed by depolymerization of the intermolecular H-bonds. The formation of new H-bonds between silica and pectin was supposed.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Polysaccharides and Plant Cell Walls · Polysaccharides Composition and Applications · Mesoporous Materials and Catalysis

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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