journal article·2024-11Open access

Precipitation kinetics of ferritic / martensitic oxide dispersion strengthened steels: Influence of the matrix phase transformation

Gabriel Spartacus, Joël Malaplate, Frédéric De Geuser, Isabelle Mouton, Denis Sornin, Raphaëlle Guillou, Alexis Deschamps

Acta Materialia· Volume 280

Abstract

ODS steels are candidate materials for the future generation of nuclear power plants. Ferritic / Martensitic (F/M) ODS steels display better formability thanks to high temperature austenitic transformation. The precipitation kinetics of a F/M Fe-9Cr ODS steel had been characterized by in-situ Small Angle X-ray Scattering (SAXS). The influence of the matrix phase transformation has been established, with an increase of the growth rate of the nano-oxides in austenite, leading to nano-oxides ~ 2x larger than in Fe-14Cr ferritic ODS grades at the end of the thermal treatment. Moreover, the APT volume after a heating ramp up to 1100 °C displayed three grains, two likely corresponding to non-transformed ferrite and one to martensite (transformed from austenite), identified thanks to their C content. In the untransformed ferrite domain, the nano-oxides number density was found to be very similar to the Fe-14Cr grade, and significantly higher than the martensitic grain. Anomalous SAXS as well as comparison between Atom Probe Tomography (APT) and SAXS provided evidences that the nano-oxides stabilize with a Y2Ti2O7 or Y2TiO5 stoichiometry around 1100 °C.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Fusion materials and technologies · Hydrogen embrittlement and corrosion behaviors in metals · Nuclear Materials and Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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