Hydrothermal synthesis of titanosilicate type zeolitic layered PLS-1 and CDS-1 molecular sieve with CDO topology
Source abstract
Abstract
The titanosilicate type CDS-1 zeolite ([Ti]CDS-1) with CDO topology can be prepared from the corresponding zeolitic layered titanosilicate [Ti]PLS-1 via dehydrative condensation of interlayers’ Q 3 silanols. The precursor [Ti]PLS-1 is successfully synthesized from the mixture of an acidified kanemite, titanium tetraisopropoxide (Ti(O i Pr)4), a small amount of hydrogen peroxide (H2O2), tetramethylammonium hydroxide (TMAOH) and water (H2O) under hydrothermal synthesis. The obtained samples were characterized by powder-XRD, TG–DTA, N2 adsorption, solid state NMR and UV–Vis analyses. Further oxidation reaction of terminal alkenes was examined by using H2O2 as an oxidant.
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Research context
OpenAlex topics: Zeolite Catalysis and Synthesis · Mesoporous Materials and Catalysis · Chemical Synthesis and Characterization
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