Hg2+ determination by DPASV by using poly (methylene disulfide)/Au nanoparticle/MWCNT modified glassy carbon electrode by differential pulse anodic stripping voltammetry (DPASV) technique
Source abstract
Abstract
In the present work, a glassy carbon electrode (GCE) was surface modified by a poly (methylene disulfide)/Au–nanoparticles/multiwall carbon nanotubes (PMDS/AuNPs/MWCNT) to improve its ability to detect of trace mercury cations in polluted water. The produced electrode was characterized with FE-SEM, HR-TEM, AFM, XRD, and FT-IR techniques. The obtained results proved the success of the modification process and revealed that the process had a significant effect on the morphology of the electrode and its surface roughness. EIS analysis demonstrated the improvement of the electrochemical properties of the surface-modified sample. Accordingly, the obtained charge transfer resistance (Rct) decreased from 477.1 Ohm cm2 for the unmodified GCE to 83.4 Ohm cm2 for the modified-GCE. The designed modified electrode was used as an ultra-sensitive electrode for determining the concentration of Hg2+ cation using the differential pulse anodic stripping voltammetry (DPASV) technique.
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Research context
OpenAlex topics: Electrochemical Analysis and Applications · Electrochemical sensors and biosensors · Conducting polymers and applications
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References (98)
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