journal article·2019-10

Effect of temperature on the transition in deformation modes in Mg single crystals

Gi-Dong Sim, Kelvin Y. Xie, Kevin J. Hemker, Jaafar A. El-Awady

Acta Materialia· Volume 178
Publisher page

Abstract

Abstract Here, an experimental study utilizing in-situ scanning electron microscopy (SEM) micro-compression testing and post-mortem transmission electron microscopy (TEM) imaging is presented to quantify the effect of temperature on the transition in deformation modes in twin-oriented Mg single crystals. Single crystal micropillars were fabricated using FIB milling, then tested by in-situ SEM micro-compression from 20 °C to 225 °C. It is observed that plasticity in the deformed Mg microcrystals at temperatures at and below 100 °C is governed by { 10 1 ¯ 2 } extension twinning. However, an anomalous increase of the flow stresses is observed at 100 °C, which is likely due to paucity of dislocation sources that are required to promote twin boundary migration. At 150 °C and above, extension twinning is suppressed and a continuous plastic flow and strain softening induced by prismatic dislocation mediated plasticity is observed. By comparing the current results with those from bulk scale studies for other hexagonal-closed-pack single crystals (e.g. titanium (Ti) and zirconium (Zr)), a general trend for the effect of temperature on the transition in deformation modes in HCP materials is proposed.
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Research context

OpenAlex topics: Magnesium Alloys: Properties and Applications · Metal and Thin Film Mechanics · MXene and MAX Phase Materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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