journal article·2021-08Open access

Evaluating the grain-scale deformation behavior of a single-phase FCC high entropy alloy using synchrotron high energy diffraction microscopy

J.V. Gordon, R.E. Lim, M.J. Wilkin, D.C. Pagan, R.A. Lebensohn, A.D. Rollett

Acta Materialia· Volume 215

Abstract

Abstract Although the deformation behavior of high-entropy alloys (HEAs) has been extensively studied at the macroscale, many important properties have yet to be explored for these alloys at the microscale, thus hampering accurate prediction of damage and failure processes. Synchrotron high-energy diffraction microscopy (HEDM) and fast-Fourier transform-based crystal plasticity modeling was conducted to investigate the three-dimensional (3D) grain-resolved micromechanical response for approximately 1,900 constituent grains within a single-phase FCC HEA up to 1% applied strain. The evolution of grain-resolved elastic strains, lattice reorientations, and maximum resolved shear stresses (mRSS) were evaluated to quantify elastic, yield, and fully plastic behavior. Overall, the initial critical resolved shear stress (CRSS), determined via in situ HEDM and companion modeling, was found to be > 20% higher than estimated using the classical polycrystalline Taylor factor (M = 3.06). However, a descriptive parameter based on the average grain-resolved Taylor factor ( M ¯ ) was found to show excellent agreement with plastic yielding behavior observed within HEDM datasets. Noticeable deviations in HEDM lattice reorientations compared to both EVP-FFT simulations and classical predictions for FCC polycrystals were discovered, highlighting the complexity in correlating local lattice reorientations, Taylor, and Schmid factors with plastic response for this material at the grain-scale. Therefore, it is anticipated that the overall trends and parameter identification of 3D grain-resolved properties in this study can serve as an important foundation for continued mesoscale investigation on both well-established and newly developed Cantor-like HEAs.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: High Entropy Alloys Studies · Additive Manufacturing Materials and Processes · Advanced Materials Characterization Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (65)

Show source-provided references
1. Reasons for the superior mechanical properties of medium-entropy CrCoNi compared to high-entropy CrMnFeCoNi10.1016/j.actamat.2017.02.036 ↗
2. Temperature dependent stacking fault energy of FeCrCoNiMn high entropy alloy10.1016/j.scriptamat.2015.05.041 ↗
3. Cooperative deformation in high-entropy alloys at ultralow temperatures10.1126/sciadv.aax4002 ↗
4. Vanadium is an optimal element for strengthening in both fcc and bcc high-entropy alloys10.1016/j.actamat.2020.01.062 ↗
5. Irradiation behavior in high entropy alloys10.1016/S1006-706X(15)30084-4 ↗
6. Microstructural development in equiatomic multicomponent alloys10.1016/j.msea.2003.10.257 ↗
7. A fracture-resistant high-entropy alloy for cryogenic applications10.1126/science.1254581 ↗
8. Strong and ductile non-equiatomic high-entropy alloys: design, processing, microstructure, and mechanical properties10.1007/s11837-017-2540-2 ↗
9. Microstructure and mechanical properties of high-entropy alloy Co20Cr26Fe20Mn20Ni14 processed by high-pressure torsion at 77 K and 300 K10.1038/s41598-018-29446-y ↗
10. Plastic strain partitioning in dual phase Al13CoCrFeNi high entropy alloy10.1016/j.msea.2018.02.044 ↗
11. High entropy alloys: a focused review of mechanical properties and deformation mechanisms10.1016/j.actamat.2019.12.015 ↗
12. X-ray characterization of the micromechanical response ahead of a propagating small fatigue crack in a Ni-based superalloy10.1016/j.actamat.2019.08.005 ↗
13. Fatigue crack initiation, slip localization and twin boundaries in a nickel-based superalloy10.1016/j.cossms.2014.06.001 ↗
14. Modeling slip system strength evolution in Ti-7Al informed by in-situ grain stress measurements10.1016/j.actamat.2017.02.042 ↗
15. Study of grain-level deformation and residual stresses in Ti-7Al under combined bending and tension using high energy diffraction microscopy (HEDM)10.1016/j.ijsolstr.2016.05.010 ↗
16. Strong grain neighbour effects in polycrystals10.1038/s41467-017-02213-9 ↗
17. Using synchrotron radiation to improve understanding of deformation of polycrystalline metals by measuring, modelling and publishing 4D information
18. Quantification of cyclic twinning-detwinning behavior during low-cycle fatigue of pure magnesium using high energy X-ray diffraction10.1016/j.ijfatigue.2019.04.011 ↗
19. Measured resolved shear stresses and Bishop-Hill stress states in individual grains of austenitic stainless steel10.1016/j.actamat.2017.09.021 ↗
20. In situ tensile study of PM-HIP and wrought 316 L stainless steel and Inconel 625 alloys with high energy diffraction microscopy10.1016/j.msea.2018.09.083 ↗
21. In-situ study of planar slip in a commercial aluminum-lithium alloy using high energy X-ray diffraction microscopy10.1016/j.actamat.2019.04.030 ↗
22. Simulation domain size requirements for elastic response of 3D polycrystalline materials
23. Critical resolved shear stress for slip and twin nucleation in single crystalline FeNiCoCrMn high entropy alloy10.1016/j.matchar.2017.05.014 ↗
24. Slip nucleation in single crystal FeNiCoCrMn high entropy alloy10.1016/j.scriptamat.2015.09.009 ↗
25. Orientation dependence of twinning in single crystalline CoCrFeMnNi high-entropy alloy10.1016/j.msea.2017.08.065 ↗
26. Twinning in [001]-oriented single crystals of CoCrFeMnNi high-entropy alloy at tensile deformation10.1016/j.msea.2017.12.059 ↗
27. Size effect, critical resolved shear stress, stacking fault energy, and solid solution strengthening in the CrMnFeCoNi high-entropy alloy10.1038/srep35863 ↗
28. The influences of temperature and microstructure on the tensile properties of a CoCrFeMnNi high-entropy alloy10.1016/j.actamat.2013.06.018 ↗
29. Assessment of surface and bulk-dominated methodologies to measure critical resolved shear stresses in hexagonal materials10.1016/j.actamat.2019.11.023 ↗
30. Plastic deformation of single crystals of the equiatomic Cr−Mn−Fe−Co−Ni high-entropy alloy in tension and compression from 10 K to 1273 K
31. Low-cycle fatigue properties of CoCrFeMnNi high-entropy alloy compared with its conventional counterparts10.1016/j.msea.2020.139661 ↗
32. Microstructure evolution and critical stress for twinning in the CrMnFeCoNi high-entropy alloy10.1016/j.actamat.2016.07.038 ↗
33. Influence of deformation induced nanoscale twinning and FCC-HCP transformation on hardening and texture development in medium-entropy CrCoNi alloy10.1016/j.actamat.2018.07.028 ↗
34. Exploring new links between crystal plasticity models and high-energy X-ray diffraction microscopy10.1016/j.cossms.2019.07.002 ↗
35. Texture analysis with MTEX-free and open source software toolbox. In Solid State Phenomena10.4028/www.scientific.net/SSP.160.63 ↗
36. Tensile properties of high-and medium-entropy alloys10.1016/j.intermet.2013.03.018 ↗
37. Far-field high-energy diffraction microscopy: a tool for intergranular orientation and strain analysis10.1177/0309324711405761 ↗
38. An elasto-viscoplastic formulation based on fast Fourier transforms for the prediction of micromechanical fields in polycrystalline materials10.1016/j.ijplas.2011.12.005 ↗
39. Validation of micro-mechanical FFT-based simulations using high energy diffraction microscopy on Ti-7Al10.1016/j.actamat.2018.05.036 ↗
40. Quantification of location-dependence in a large-scale additively manufactured build through experiments and micromechanical modeling10.1016/j.mtla.2019.100397 ↗
41. A multi-scale, multi-physics modeling framework to predict spatial variation of properties in additive-manufactured metals
42. Effect of microstructure on the elasto-viscoplastic deformation of dual phase titanium structures10.1007/s00466-017-1467-3 ↗
43. Characterization of metal additive manufacturing surfaces using synchrotron X-ray CT and micromechanical modeling10.1007/s00466-017-1531-z ↗
44. A FFT-based numerical implementation of mesoscale field dislocation mechanics: application to two-phase laminates10.1016/j.ijsolstr.2018.12.027 ↗
45. Processing, microstructure and mechanical properties of the CrMnFeCoNi high-entropy alloy10.1007/s11837-015-1589-z ↗
46. Theory of strengthening in fcc high entropy alloys10.1016/j.actamat.2016.07.040 ↗
47. DREAM.3D: a digital representation environment for the analysis of microstructure in 3D10.1186/2193-9772-3-5 ↗
48. Modeling the effect of neighboring grains on twin growth in HCP polycrystals10.1088/1361-651X/aa7bbb ↗
49. Direct measurement of critical resolved shear stress of prismatic and basal slip in polycrystalline Ti using high energy X-ray diffraction microscopy10.1016/j.actamat.2017.05.015 ↗
50. Temperature dependencies of the elastic moduli and thermal expansion coefficient of an equiatomic, single-phase CoCrFeMnNi high-entropy alloy10.1016/j.jallcom.2014.11.061 ↗
51. Determining grain resolved stresses in polycrystalline materials using three-dimensional X-ray diffraction10.1107/S0021889810012963 ↗
52. Statistical aspects of grain-level strain evolution and reorientation during the heating and elastic-plastic loading of a Ni-base superalloy at elevated temperature10.1016/j.mtla.2021.101063 ↗
53. Yield strength prediction of titanium alloys10.1007/s11837-015-1436-2 ↗
54. Enhancement in fatigue performance of metastable austenitic stainless steel through directed energy deposition additive manufacturing10.1016/j.matdes.2019.107630 ↗
55. In-situ high energy X-ray diffraction study of the elastic response of a metastable β-titanium alloy10.1016/j.actamat.2020.07.050 ↗
56. In-situ observation of bulk 3D grain evolution during plastic deformation in polycrystalline Cu10.1016/j.ijplas.2014.10.013 ↗
57. Polycrystal plasticity: comparison between grain-scale observations of deformation and simulations10.1146/annurev-conmatphys-031113-133846 ↗
58. Average intragranular misorientation trends in polycrystalline materials predicted by a viscoplastic self-consistent approach10.1016/j.actamat.2015.10.035 ↗
59. Investigation of porosity, texture, and deformation behavior using high energy X-rays during in-situ tensile loading in additively manufactured 316 L stainless steel10.1016/j.msea.2021.141034 ↗
60. Hosford · 1993
61. Influence of directional strength-to-stiffness on the elastic-plastic transition of fcc polycrystals under uniaxial tensile loading10.1016/j.actamat.2009.11.009 ↗
62. A statistical study of the relationship between plastic strain and lattice misorientation on the surface of a deformed Ni-based superalloy10.1016/j.actamat.2020.05.029 ↗
63. Microstructural effects on damage evolution in shocked copper polycrystals10.1016/j.actamat.2016.06.054 ↗
64. Lattice rotations of individual bulk grains Part II: correlation with initial orientation and model comparison10.1016/j.actamat.2004.02.045 ↗
65. Micromechanical and macromechanical effects in grain scale polycrystal plasticity experimentation and simulation10.1016/S1359-6454(01)00242-7 ↗