journal article·2018-02Open access

Microstructural evolution and deformation behavior of Al-Cu alloys: A Transmission X-ray Microscopy (TXM) and micropillar compression study

C. Shashank Kaira, Christopher Kantzos, Jason J. Williams, Vincent De Andrade, Francesco De Carlo, Nikhilesh Chawla

Acta Materialia· Volume 144

Abstract

Abstract A unique approach to correlating an evolving 3D microstructure in an Al-Cu alloy and its micro-scale mechanical properties has been introduced. Using these nanoscale three-dimensional microstructures derived from Transmission X-ray Microscopy (TXM), individual contributions from different strengthening mechanisms were quantified. The spatial distribution and morphology of the individual θ′ and θ phases were seen to play an important role in influencing dislocation storage. Uniaxial micro-compression experiments were used to quantify the stress-strain response of the alloy at different aging times. Transmission electron microscopy (TEM) aided in discerning dislocation activity at these precipitates. A model is proposed to accurately predict the variation in yield stress by using appropriate morphological parameters from the 3D microstructure and its validity has been corroborated using experimental measurements. Distributions of 2D and 3D inter-precipitate spacing were seen to provide crucial insights on influencing deformation in such precipitation-strengthened alloys. Finally, the transition in deformation behavior and origin of numerous strain bursts were investigated using in situ micropillar compression testing.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Microstructure and mechanical properties · Aluminum Alloy Microstructure Properties · Aluminum Alloys Composites Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (54)

Show source-provided references
1. Structure and energetics of the coherent interface between the θ′ precipitate phase and aluminium in Al–Cu10.1016/j.actamat.2011.07.059 ↗
2. Mechanical properties enhanced by deformation-modified precipitation of θ′-phase approximants in an Al-Cu alloy10.1016/j.msea.2016.08.068 ↗
3. Small-volume aluminum alloys with native oxide shell deliver unprecedented strength and toughness10.1016/j.actamat.2016.12.055 ↗
4. Multiscale modeling of θ′ precipitation in Al-Cu binary alloys10.1016/j.actamat.2004.03.001 ↗
5. The effect of time and temperature on the precipitation behavior and hardness of Al-4 wt%Cu alloy using design of experiments10.1016/j.jmatprotec.2007.11.047 ↗
6. Interrupted aging and secondary precipitation in aluminium alloys10.1179/026708303225008112 ↗
7. The coarsening behaviour of θ″ and θ′ precipitates in two Al-Cu alloys10.1016/0001-6160(71)90076-9 ↗
8. Mechanisms of formation of [theta] and dissolution of [theta]’ precipitates in an Al-4% Cu alloy10.1016/0001-6160(66)90298-7 ↗
9. Precipitation in thin foils of Al-4 wt.% Cu alloy—II. Growth kinetics of θ precipitates10.1016/0001-6160(75)90067-X ↗
10. Coarsening of θ′ plates in al-cu alloys—I. experimental determination of mechanisms10.1016/0001-6160(81)90029-8 ↗
11. Yoshida · 2006
12. Structure of age-hardened aluminium-copper alloys10.1038/142569b0 ↗
13. Age-hardening of copper-aluminium alloys10.1088/0959-5309/52/1/310 ↗
14. Friedel · 1964 · vol. 70 · 15
15. Predicting slip behavior in alloys containing shearable and strong particles10.1016/0921-5093(93)90596-7 ↗
16. Distribution of plastic strain in alloys containing small particles10.1016/0026-0800(75)90038-5 ↗
17. Strengthening effect of unshearable particles of finite size: a computer experimental study10.1016/S1359-6454(99)00179-2 ↗
18. Computer experiment on superposition of strengthening effects of different particles10.1016/S1359-6454(99)00077-4 ↗
19. Precipitation hardening10.1007/BF02670416 ↗
20. Microstructural design of high-strength aluminum alloys10.1361/105497198770341734 ↗
21. Deformation and fracture in Al-CuAl2 eutectic composites10.1007/BF02913874 ↗
22. Orowan · 1948 · vol. 451
23. On the strengthening response of aluminum alloys containing shear-resistant plate-shaped precipitates10.1016/j.actamat.2008.08.023 ↗
24. On the form of the age-hardening response in high strength aluminium alloys10.1016/S0921-5093(01)01054-1 ↗
25. Strengthening of an Al–Cu–Sn alloy by deformation-resistant precipitate plates10.1016/j.actamat.2008.03.028 ↗
26. Probing novel microstructural evolution mechanisms in aluminum alloys using 4D nanoscale characterization10.1002/adma.201703482 ↗
27. High-efficiency fresnel zone plates for hard X-rays by 100 keV e-beam lithography and electroplating10.1107/S0909049511002366 ↗
28. Nanoscale 3D imaging at the advanced Photon source
29. Nanoscale three-dimensional microstructural characterization of an Sn-Rich solder alloy using high-resolution transmission x-ray microscopy (TXM)10.1017/S1431927616011429 ↗
30. Probing three-dimensional sodiation–desodiation equilibrium in sodium-ion batteries by in situ hard X-ray nanotomography10.1038/ncomms8496 ↗
31. Nanoscale X-ray imaging10.1038/nphoton.2010.267 ↗
32. Size dependence of mechanical properties of gold at the micron scale in the absence of strain gradients10.1016/j.actamat.2004.12.031 ↗
33. Correlation between critical temperature and strength of small-scale bcc pillars10.1103/PhysRevLett.103.105501 ↗
34. Microcompression of single-crystal magnesium10.1016/j.scriptamat.2009.12.017 ↗
35. Microscale deformation behavior of bicrystal boundaries in pure tin (Sn) using micropillar compression10.1016/j.actamat.2016.08.030 ↗
36. Effect of interfacial solute segregation on ductile fracture of Al–Cu–Sc alloys10.1016/j.actamat.2012.11.043 ↗
37. Cyclic stress—strain response of two-phase alloys Part II. Particles not penetrated by dislocations10.1016/0025-5416(74)90183-9 ↗
38. Slip in aluminum crystals containing strong, plate-like particles10.1016/0001-6160(70)90017-9 ↗
39. TomoPy: a framework for the analysis of synchrotron tomographic data10.1107/S1600577514013939 ↗
40. Scientific data exchange: a schema for HDF5-based storage of raw and analyzed data10.1107/S160057751401604X ↗
41. FIB damage of Cu and possible consequences for miniaturized mechanical tests10.1016/j.msea.2007.01.046 ↗
42. Effects of focused ion beam milling on the compressive behavior of directionally solidified micropillars and the nanoindentation response of an electropolished surface10.1016/j.actamat.2008.09.033 ↗
43. Investigation of the deformation behavior of aluminum micropillars produced by focused ion beam machining using Ga and Xe ions10.1016/j.scriptamat.2016.08.028 ↗
44. The effect of shear-resistant, plate-shaped precipitates on the work hardening of Al alloys: towards a prediction of the strength-elongation correlation10.1016/j.actamat.2009.08.034 ↗
45. The deformation and ageing of mild steel: III discussion of results10.1088/0370-1301/64/9/303 ↗
46. Grain boundary precipitation in Al-Cu
47. Microstructural evolution and age hardening in aluminium alloys10.1016/S1044-5803(99)00051-0 ↗
48. Nucleation-mediated structural refinement and aluminium alloy design10.4028/www.scientific.net/MSF.519-521.191 ↗
49. Multiscale microstructural characterization of Sn-rich alloys by three dimensional (3D) X-ray synchrotron tomography and focused ion beam (FIB) tomography10.1016/j.matchar.2012.05.004 ↗
50. Park · 1970
51. The effect of precipitate shape and orientation on dispersion strengthening in high strength aluminium alloys10.4028/www.scientific.net/MSF.217-222.1257 ↗
52. The deformation of plastically non-homogeneous materials10.1080/14786437008238426 ↗
53. The work-hardening of copper-silica10.1080/14786437108217406 ↗
54. Substitutional solutes in AlRu—I. Effects of solute on moduli, lattice parameters and vacancy production10.1016/0956-7151(93)90020-S ↗