Use of quasi-static nanoindentation data to obtain stress–strain characteristics for metallic materials

This paper concerns optimization of procedures and algorithms for extraction of stress–strain relationships from quasi-static nanoindentation experiments, using finite element method modelling. Several issues are highlighted, including the usefulness of incorporating residual indent shape in the comparisons, as well as load–displacement–time data, and the significance of creep and interfacial friction. The study is focused on extruded copper bar, using a spherical indenter and assuming transverse isotropy throughout. It is shown that, using the methodology presented here, experimental nanoindentation data could be used to estimate the yield stress and work-hardening rate, with good accuracy, i.e. the yield stress could have been obtained to a precision of about ±10%, and the work-hardening rate to about ±25%. Such inferred constitutive relations are more likely to be reliable if the comparisons are made in regimes within which creep does not significantly influence the behaviour, and in general the timescale of measurement is important. 2010 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.