journal article·2025-03

Single-crystalline Ni-based superalloy builds using laser-directed energy deposition (L-DED): A multi-scale modeling and experimental approach

Swapnil Bhure, Divya Nalajala, Abhik Choudhury

Acta Materialia· Volume 286
Publisher page

Abstract

Additive manufacturing is rapidly becoming a viable alternative for producing complex geometries, making it a potential choice for manufacturing aerospace components. The high-pressure turbine blades in a jet engine not only have complex geometry but also require stringent microstructural specifications such as single-crystallinity. The combination of complexities in the topology and microstructure makes it challenging to identify the right process parameters for the additive manufacturing of these blades. In this paper, we describe an innovative workflow for identifying these parameters, involving physics-based modeling at the melt pool length scale and microstructure modeling at the grain and dendritic length scales. We introduce a novel diffuse-interface-inspired model to simulate the melt pool shape during multi-layer additive manufacturing. The thermal histories obtained from this model are used in a Potts-based microstructure model to determine the approximate texture during solidification. By combining the process and grain-scale model, we determine the parameter space for single-crystalline builds. Experimental analysis confirms that the identified parameters yield single-crystalline microstructures. Furthermore, the thermal histories are utilized in phase-field simulations that consider all the components of the CMSX-4 alloy to determine the primary dendrite arm spacing (PDAS), which, upon comparison with experimental measurements, serves as validation of the solidification conditions derived from the process model. Thus, the complementary use of modeling and experiments provides insights that allow the identification of appropriate additive parameters for epitaxial growth and aid in designing strategies for building complex shapes.
Source: expertdata · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · High Entropy Alloys Studies · Advanced Materials Characterization Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (52)

Show source-provided references
1. Reed · 2006
2. Nickel-Based Superalloys for Advanced Turbine Engines: Chemistry, Microstructure and Properties10.2514/1.18239 ↗
3. Research Progress in Nickel Base Single Crystal Superalloys10.4028/www.scientific.net/KEM.861.113 ↗
4. Investigation of solidification microstructure of single crystal CMSX-4 superalloy–experimental measurements and modelling predictions10.1179/1743133615Y.0000000021 ↗
5. Microstructure of the Nickel-base superalloy CMSX-4 fabricated by selective electron beam melting10.1007/s11661-015-3300-y ↗
6. Additive manufacturing of metallic components – Process, structure and properties10.1016/j.pmatsci.2017.10.001 ↗
7. Additive manufacturing of Nickel-based superalloys: A state-of-the-art review on process-structure-defect-property relationship10.1016/j.pmatsci.2023.101108 ↗
8. Epitaxial laser metal forming: Analysis of microstructure formation10.1016/S0921-5093(99)00202-6 ↗
9. Single-crystal laser deposition of superalloys: Processing-microstructure maps10.1016/S1359-6454(00)00367-0 ↗
10. Single-crystal height extension by laser metal deposition of CMSX-410.1016/j.procir.2020.09.057 ↗
11. Additive Manufacturing of Nickel-Base Superalloy René N5 through Scanning Laser Epitaxy (SLE) - Material Processing, Microstructures, and Microhardness Properties10.1002/adem.201600690 ↗
12. A coupled thermal, fluid flow, and solidification model for the processing of single-crystal alloy CMSX-4 through scanning laser epitaxy for turbine engine hot-section component repair (Part I)10.1007/s11663-014-0117-9 ↗
13. Additive Manufacturing of Single-Crystal Superalloy CMSX-4 Through Scanning Laser Epitaxy: Computational Modeling, Experimental Process Development, and Process Parameter Optimization10.1007/s11661-016-3571-y ↗
14. Microstructure and mechanical properties of CMSX-4 single crystals prepared by additive manufacturing10.1007/s11661-018-4762-5 ↗
15. A Single Crystal Process Window for Electron Beam Powder Bed Fusion Additive Manufacturing of a CMSX-4 Type Ni-Based Superalloy10.3390/ma14143785 ↗
16. Effects of processing parameters on crystal growth and microstructure formation in laser powder deposition of single-crystal superalloy10.1016/j.jmatprotec.2014.08.025 ↗
17. A review of the anomalies in directed energy deposition (DED) processes & potential solutions-part quality & defects10.1016/j.promfg.2021.06.093 ↗
18. Miedzinski · 2017
19. Nucleation ahead of the advancing interface in directional solidification10.1016/S0921-5093(97)80081-0 ↗
20. Columnar to equiaxed transition in solidification processing10.1016/S1468-6996(01)00047-X ↗
21. Stray grain formation in single crystal Ni-base superalloy welds10.1063/1.1602950 ↗
22. Analysis of stray grain formation in single-crystal Nickel-based superalloy welds
23. The effect of welding conditions on stray grain formation in single crystal welds – theoretical analysis10.1016/j.actamat.2004.08.039 ↗
24. Stray grain formation in welds of single-crystal Ni-base superalloy CMSX-410.1007/s11661-009-0078-9 ↗
25. Origin of stray grain formation in single-crystal superalloy weld pools from heat transfer and fluid flow modeling10.1016/j.actamat.2009.10.051 ↗
26. Welding of Nickel base superalloy single crystals10.1179/stw.1997.2.2.79 ↗
27. Toward DS/SX Ni-Based Superalloy Components Using L-DED: A Multi-scale Modeling and Experimental Approach
28. On the evolution of cast microstructures during processing of single crystal Ni-base superalloys using a Bridgman seed technique10.1016/j.matdes.2017.05.001 ↗
29. MicroSim: A high-performance phase-field solver based on CPU and GPU implementations10.1016/j.commatsci.2024.113438 ↗
30. Phase-field model for Hele–Shaw flows with arbitrary viscosity contrast. I. Theoretical approach10.1103/PhysRevE.60.1724 ↗
31. Sharp interface tracking using the phase-field equation10.1016/j.jcp.2006.05.025 ↗
32. Singh · 2019
33. Modeling of laser keyhole welding: Part I. Mathematical modeling, Numerical methodology, role of recoil pressure, multiple reflections, and free surface evolution10.1007/s11661-002-0190-6 ↗
34. Role of melt flow dynamics on track surface morphology in the L-PBF additive manufacturing process10.1016/j.ijheatmasstransfer.2021.121602 ↗
35. Extended smoothed boundary method for solving partial differential equations with general boundary conditions on complex boundaries10.1088/0965-0393/20/7/075008 ↗
36. Greenshields · 2020
37. Near Single-Crystalline CMSX-4 Superalloy Builds with Laser-Directed Energy Deposition (L-DED) Using Model-Informed Experiments
38. Kinetics of the Q-state Potts model in two dimensions10.1103/PhysRevLett.50.263 ↗
39. Janssens · 2010
40. A coupled finite element-cellular automaton model for the prediction of dendritic grain structures in solidification processes10.1016/0956-7151(94)90302-6 ↗
41. A three-dimensional cellular automation-finite element model for the prediction of solidification grain structures10.1007/s11661-999-0226-2 ↗
42. Thermophysical properties
43. Mills · 2002
44. A new hot-tearing criterion10.1007/s11661-999-0334-z ↗
45. Rappaz · 2009
46. Influence of solidification variables on the dendrite arm spacings of Ni-based superalloys10.1007/s11663-000-0162-4 ↗
47. Grand-potential formulation for multicomponent phase transformations combined with thin-interface asymptotics of the double-obstacle potential10.1103/PhysRevE.85.021602 ↗
48. A method for coupling the phase-field model based on a grand-potential formalism to thermodynamic databases10.1016/j.cossms.2015.03.003 ↗
49. Application of finite element, phase-field, and CALPHAD-based methods to Additive manufacturing of Ni-based superalloys10.1016/j.actamat.2017.05.003 ↗
50. On the primary spacing and microsegregation of cellular dendrites in laser deposited Ni–Nb alloys10.1088/1361-651X/aa7369 ↗
51. Phase-field simulations and microstructural analysis of epitaxial growth during rapid solidification of Additively manufactured AlSi10Mg alloy10.1016/j.matdes.2020.108985 ↗
52. Solidification of the Ni-based superalloy CMSX-4 simulated with full complexity in 3-dimensions10.1007/s40964-023-00513-9 ↗