journal article·2023-09Open access

The microstructural origin of a hardness double-peak in an age-hardened EN-AW 6082

Christoph M. Hell, Bjørn Holmedal, Ruben Bjørge, Calin D. Marioara, Randi Holmestad

Acta Materialia· Volume 256

Abstract

In this study, the origin of a double-peak during artificial aging of an EN-AW 6082 is analyzed with (S)TEM. The acquired TEM data is used as an input into a strength model (Holmedal, 2015) to explore the origin of the double-peak, thus, a broader strength plateau. It is concluded that the first peak arises after about 160 min at 175 °C from a population of relatively wide β′′-type precipitates with a high number density and a narrow length spread. The second peak occurs after 10 h artificial aging and can be traced to a broader size distribution of precipitate lengths of roughly the same type of precipitates as found for the first peak. The longest precipitates, however, act more efficiently as obstacles for gliding dislocations and maintain therefore the high strength. Those long precipitates are of a hybrid type of different, but mainly overaged phases. It is found that this broad strength plateau with a double-peak can arise after a rapid heat-up to the artificial aging temperature. Due to the rapid heat-up, structures of overaged phases are already found within the β′′ precipitates of the first peak making them wider. Ultimately, however, this leads to the evolution of few but very large overaged hybrid-type precipitates co-existing with β′′-type precipitates at the second peak. The mixed morphology counteracts the loss of strength from Ostwald ripening and leads to the second peak. A slower heating rate results in fewer precipitate nucleation sites and in the formation of longer and purer but slimmer βperfect′′ phases.
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Research context

OpenAlex topics: Microstructure and mechanical properties · Aluminum Alloy Microstructure Properties · Aluminum Alloys Composites Properties

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References (33)

Show source-provided references
1. Strength contributions from precipitates10.1080/09500839.2015.1125029 ↗
2. T. Saito, E.A. Mørtsell, S. Wenner, C.D. Marioara, S.J. Andersen, J. Friis, K. Matsuda, R. Holmestad, Atomic structures of precipitates in Al–Mg–Si alloys with small additions of other elements, (ISSN: 15272648) 20 (7) (2018) 1800125. http://dx.doi.org/10.1002/adem.201800125.10.1002/adem.201800125 ↗
3. The effects of quench rate and pre-deformation on precipitation hardening in Al-Mg-Si alloys with different cu amounts10.1016/j.msea.2014.04.094 ↗
4. Mechanisms controlling the artificial aging of Al-Mg-Si alloys10.1016/j.actamat.2011.02.010 ↗
5. The effect of cu on precipitation in Al-Mg-Si alloys10.1080/14786430701287377 ↗
6. Gottstein · 200410.1007/978-3-662-09291-0 ↗
7. The shearable–non-shearable transition in Al–Mg–Si–Cu precipitation hardening alloys: implications on the distribution of slip, work hardening and fracture10.1080/14786430500154935 ↗
8. Porter · 2009
9. Ageing behaviour of an Fe-20Ni-1.8Mn-1.6Ti-0.59Al (wt%) maraging alloy: Clustering, precipitation and hardening10.1016/j.actamat.2004.08.018 ↗
10. Double-peak age strengthening of cold-worked 2024 aluminum alloy10.1016/j.actamat.2012.11.039 ↗
11. The influence of alloy composition on precipitates of the Al-Mg-Si system10.1007/s11661-005-1001-7 ↗
12. Experiments and modeling of double-peak precipitation hardening and strengthening mechanisms in Al-Zn-Mg alloy10.1016/S1003-6326(14)63324-0 ↗
13. Age-hardening behavior of cast Al-Si base alloy10.1016/j.matlet.2003.12.027 ↗
14. Influence of natural aging and ramping before artificial aging on the microstructure of two different 6xxx alloys10.1016/j.jmrt.2022.10.139 ↗
15. Smart align—a new tool for robust non-rigid registration of scanning microscope data10.1186/s40679-015-0008-4 ↗
16. Hell · 2022
17. Modelling of the age hardening behaviour of Al-Mg-Si alloys10.1016/S1359-6454(00)00301-3 ↗
18. Kocks · 1975
19. An improved modelling framework for strength and work hardening of precipitate strengthened Al–Mg–Si alloys
20. Precipitation of non-spherical particles in aluminum alloys part II: numerical simulation and experimental characterization during aging treatment of an Al-Mg-Si alloy10.1007/s11661-015-3196-6 ↗
21. A yield strength model for the Al-Mg-Si-Cu alloy AA611110.1016/S1359-6454(03)00028-4 ↗
22. The influence of precipitation on the work-hardening behavior of the aluminum alloys AA6111 and AA703010.1007/s11661-003-0007-2 ↗
23. The effect of obstacle strength distribution on the critical resolved shear stress of engineering alloys10.4028/www.scientific.net/MSF.794-796.449 ↗
24. Boyer · 1985
25. Callister · 2007
26. Nano-sized twins induce high rate sensitivity of flow stress in pure copper10.1016/j.actamat.2005.01.031 ↗
27. Synthesis and characterization of electrodeposited nanocrystalline nickel–iron alloys10.1016/S0921-5093(02)00586-5 ↗
28. The strength of nanocrystalline metals with and without flaws10.1016/S0921-5093(97)00185-8 ↗
29. Assessment of advanced taylor models, the taylor factor and yield-surface exponent for FCC metals10.1016/j.ijplas.2018.10.015 ↗
30. Anderson · 2017
31. Modeling of precipitate strengthening with near-chemical accuracy: case study of Al-6xxx alloys10.1016/j.actamat.2022.118144 ↗
32. Precipitation in an A356 foundry alloy with Cu additions - A transmission electron microscopy study10.1016/j.jallcom.2019.01.229 ↗
33. Origin of double-peak precipitation hardening in metallic alloys10.1016/j.ijplas.2018.07.016 ↗