journal article·2021-02Open access

Crystallographic orientation-dependent strain hardening in a precipitation-strengthened Al-Cu alloy

Brian Milligan, Dong Ma, Lawrence Allard, Amy Clarke, Amit Shyam

Acta Materialia· Volume 205

Abstract

Abstract While the strengthening of Al-Cu alloys due to precipitation has been extensively studied, the effect of crystallographic orientation of the matrix and precipitates, as well as precipitate morphology, on the strain hardening behavior is not well understood. Here we investigate this effect with in situ neutron diffraction during deformation of an Al-Cu alloy (206) after multiple aging treatments. Precipitate-dislocation interactions were found to change from precipitate shearing for microstructures predominantly containing GPI and θ′′ precipitates to Orowan looping for microstructures with primarily θ′ and θ precipitates. Notably, significant anisotropy in strain hardening behavior was observed when θ′ precipitates were present, which was attributed to crystallographic orientation dependent load transfer from the Al matrix to the θ′ precipitates. The anisotropic load transfer is hypothesized to be caused by the extent of rotation of high aspect-ratio θ′ precipitates, owing to dislocations looping around them during plastic deformation of the matrix. Predictions from an analytical model describing the anisotropic magnitude of load transfer from precipitate rotation agree well with experimental results, successfully validating the precipitate rotation hypothesis and explaining the anisotropic strain hardening behavior. This model allows for the prediction of stresses separately in the precipitate and matrix phases as a function of crystallographic orientation, only given the bulk mechanical properties.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Aluminum Alloy Microstructure Properties · Microstructure and mechanical properties · Metal Forming Simulation Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (63)

Show source-provided references
1. The effect of shear-resistant, plate-shaped precipitates on the work hardening of Al alloys: Towards a prediction of the strength–elongation correlation10.1016/j.actamat.2009.08.034 ↗
2. A theoretical investigation of the effect of precipitate habit plane on plastic anisotropy in age hardenable aluminium alloys10.1088/1361-651X/aac51a ↗
3. Physical Metallurgy of Light Alloys
4. P. Shower, J.R. Morris, D. Shin, B. Radhakrishnan, L.F. Allard, A. Shyam, Temperature-dependent stability of θ′-Al2Cu precipitates investigated with phase field simulations and experiments, Materialia. 5 (2019) 100185. doi: 10.1016/j.mtla.2018.100185.10.1016/j.mtla.2018.100185 ↗
5. Multiscale modeling of θ′ precipitation in Al–Cu binary alloys10.1016/j.actamat.2004.03.001 ↗
6. Excess vacancies and the mechanism of the slow reaction in aluminum-4% copper alloy10.1016/0025-5416(69)90037-8 ↗
7. In-situ STEM imaging of growth and phase change of individual CuAlX precipitates in Al alloy
8. Dislocation dynamics in aluminum containing θ’ phase: Atomistic simulation and continuum modeling10.1016/j.ijplas.2019.02.010 ↗
9. Microstructural evolution and deformation behavior of Al-Cu alloys: A Transmission X-ray Microscopy (TXM) and micropillar compression study10.1016/j.actamat.2017.11.009 ↗
10. Phase-Field Simulation of Orowan Strengthening by Coherent Precipitate Plates in an Aluminum Alloy10.1007/s11661-015-2895-3 ↗
11. The interaction of dislocations and precipitates10.1016/0001-6160(60)90125-5 ↗
12. THE STRENGTH OF AN ALLOY CONTAINING ZONES10.1016/0001-6160(57)90003-2 ↗
13. Effect of copper content on the tensile elongation of Al–Cu–Mn–Zr alloys: Experiments and finite element simulations
14. H. Sehitoglu, T. Foglesong, H.J. Maier, Precipitate Effects on the Mechanical Behavior of Aluminum Copper Alloy: Part I. Experiments, METALLURGICAL AND MATERIALS TRANSACTIONS A. (n.d.) 13.
15. H. Sehitoglu, T. Foglesong, H.J. Maier, Precipitate Effects on the Mechanical Behavior of Aluminum Copper Alloys: Part II. Modeling, METALLURGICAL AND MATERIALS TRANSACTIONS A. (n.d.) 8.
16. On the form of the age-hardening response in high strength aluminium alloys10.1016/S0921-5093(01)01054-1 ↗
17. Discrete dislocation dynamics simulations of dislocation-θ′ precipitate interaction in Al-Cu alloys10.1016/j.jmps.2018.05.015 ↗
18. Precipitation during high temperature aging of Al−Cu alloys: A multiscale analysis based on first principles calculations10.1016/j.actamat.2019.01.024 ↗
19. Multiscale modelling of the morphology and spatial distribution of θ′ precipitates in Al-Cu alloys10.1016/j.actamat.2017.04.042 ↗
20. Elevated temperature microstructural stability in cast AlCuMnZr alloys through solute segregation
21. Solute segregation at the Al/θ′-Al2Cu interface in Al-Cu alloys10.1016/j.actamat.2017.09.020 ↗
22. Mechanisms for stabilizing θ′(Al2Cu) precipitates at elevated temperatures investigated with phase field modeling10.1016/j.mtla.2019.100335 ↗
23. The aluminium-copper system10.1179/imtr.1985.30.1.211 ↗
24. J. M. Silcock, The θ’ structure in aluminum copper alloys., 9 (1956) 680.10.1107/S0365110X56001820 ↗
25. Crystal Structures of Al2Cu Revisited: Understanding Existing Phases and Exploring Other Potential Phases10.3390/met9101037 ↗
26. Coherency Stresses, Composition and Dislocation Interactions for 0" Precipitates in Age-Hardened AI-Cu
27. An analysis of the influence of the precipitate type on the mechanical behavior of Al - Cu alloys by means of micropillar compression tests10.1016/j.actamat.2020.05.040 ↗
28. Precipitation Hardening
29. Direct Observaion for the Interaction of Dislocations with θ′ Precipitates in an Aluminum-3.8 Wt.-% Copper Alloy
30. Probing Novel Microstructural Evolution Mechanisms in Aluminum Alloys Using 4D Nanoscale Characterization10.1002/adma.201703482 ↗
31. A simple model for dislocation behavior, strain and strain rate hardening evolution in deforming aluminum alloys10.1016/S0749-6419(01)00015-8 ↗
32. Microstructural design of high-strength aluminum alloys10.1361/105497198770341734 ↗
33. Strengthening of an Al–Cu–Sn alloy by deformation-resistant precipitate plates10.1016/j.actamat.2008.03.028 ↗
34. Multiscale modelling of precipitation hardening in Al–Cu alloys: Dislocation dynamics simulations and experimental validation10.1016/j.actamat.2020.02.019 ↗
35. The anisotropy of age-hardened Al-4 pct Cu single crystals during plane-strain compression10.1007/BF02680590 ↗
36. G.D. Moan, J.D. Embury, A STUDY OF THE BAUSCHINGER EFFECT IN Al-01 ALLOYS, (n.d.) 12.
37. Studies on the Work-Hardening Behavior of AA2219 under Different Aging Treatments10.1007/s11661-009-0062-4 ↗
38. Microstress evolution during in situ loading of a superalloy containing high volume fraction of c0 phase
39. Lattice parameter misfit evolution during creep of a cobalt-based superalloy single crystal with cuboidal and rafted gamma-prime microstructures10.1016/j.actamat.2017.06.025 ↗
40. Comparative Evaluation of Cast Aluminum Alloys for Automotive Cylinder Heads: Part I—Microstructure Evolution10.1007/s11661-017-3985-1 ↗
41. Dieter · 1988
42. Temperature-dependent elastic anisotropy and mesoscale deformation in a nanostructured ferritic alloy10.1038/ncomms6178 ↗
43. Orientation-dependent evolution of the dislocation density in grain populations with different crystallographic orientations relative to the tensile axis in a polycrystalline aggregate of stainless steel10.1016/j.actamat.2013.11.012 ↗
44. First In Situ Lattice Strains Measurements Under Load at VULCAN10.1007/s11661-010-0495-9 ↗
45. Preparation of high quality Al TEM specimens via a double-jet electropolishing technique10.1016/j.matchar.2007.04.003 ↗
46. 25 years of image analysis10.1038/nmeth.2089 ↗
47. Fiji: an open-source platform for biological-image analysis10.1038/nmeth.2019 ↗
48. Comparative Evaluation of Cast Aluminum Alloys for Automotive Cylinder Heads: Part II—Mechanical and Thermal Properties10.1007/s11661-017-3986-0 ↗
49. CRSS of γ/γ′ phases from in situ neutron diffraction of a directionally solidified superalloy tension tested at 900°C10.1016/j.actamat.2008.04.057 ↗
50. Guinier-Preston zones in Al-rich Al-Cu and Al-Ag single crystals10.1016/S0921-4526(96)01232-X ↗
51. Dynamics and kinetics of dislocations in Al and Al–Cu alloy under dynamic loading10.1016/j.ijplas.2013.09.008 ↗
52. H. Mecking, U.F. Kocks, C. Hartig, TA.YLOR FACTORS IN MATERIALS WITH MANY DEFORMATION MODES, 35 (1996) 7.10.1016/1359-6462(96)00137-6 ↗
53. Fracture of brittle particles in a ductile matrix10.1007/BF00018353 ↗
54. On the strengthening response of aluminum alloys containing shear-resistant plate-shaped precipitates10.1016/j.actamat.2008.08.023 ↗
55. Atomistic study of fundamental character and motion of dislocations in intermetallic Al2Cu10.1016/j.ijplas.2016.09.005 ↗
56. Precipitation hardening in Al–Cu–Mg alloys revisited10.1016/j.scriptamat.2005.09.010 ↗
57. Neutron diffraction measurement of the residual stress in the cementite and ferrite phases of cold-drawn steel wires10.1016/S1359-6454(96)00051-1 ↗
58. Anisotropy in creep ageing behavior of textured Al-Cu alloy under different stress states10.1016/j.matchar.2020.110539 ↗
59. A screw dislocation interacting with a bimaterial interface incorporating surface strain gradient elasticity10.1016/j.euromechsol.2015.05.010 ↗
60. The effects of microstructural stability on the compressive response of two cast aluminum alloys up to 300°C10.1016/j.msea.2017.06.024 ↗
61. Nye · 1986
62. A first-principles study of the structural, mechanical and electronic properties of precipitates of Al 2 Cu in Al–Cu alloys10.1039/C7CP06757G ↗
63. Growth behavior of γ ’ / γ ’ ’ coprecipitates in Ni-Base superalloys10.1016/j.actamat.2018.10.028 ↗