Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles
Source abstract
Abstract
Wet chemical synthesis (WCS), especially under high temperatures, is one of the most frequently used strategies for nanostructured material construction, which has been used extensively in medical-, energy-, and environment-related applications. Although knowledge about the WCS process has been accumulated in the past two decades, the high temperature used in the process and multiphase nature of intermediates and products are key factors preventing the processes from rationalization. In this paper, by using multilevel in situ cells, we developed a strategy to monitor the reaction details of WCS processed in the solid, liquid, and gas phase simultaneously. This protocol has proven successful to reconstruct the WCS process of Fe 5 C 2 nanoparticles (NPs) and unravel the complicated chemistry in the synthesis process.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Catalytic Processes in Materials Science · Nanomaterials for catalytic reactions · Electrocatalysts for Energy Conversion
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
Shanghai Institute of Applied Physics, Chinese Academy of Science, Shanghai Synchrotron Radiation Facility (SSRF), Shanghai 201204, China
Department of Chemical Physics, University of Science and Technology of China, Hefei 230026, China
State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China
Israel Chemicals Limited, Shanghai 200021, China
Funding
Ministry of Science and Technology of the People's Republic of China · China Postdoctoral Science Foundation · National Natural Science Foundation of China
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