Cracking mechanism in a laser powder bed fused cold-work tool steel: The role of residual stresses, microstructure and local elemental concentrations
Source abstract
Abstract
Laser powder bed fusion (LPBF) facilitates economic advantages by enhancing cutting speeds of tools through the implementation of complex internal cooling channels that could not be fabricated otherwise. However, tool steels are prone to cracking during the cyclic remelting process with extremely fast cooling rates due to their high carbon and alloying element contents and related stresses. In this work, a correlation between microscopic crack patterns in a tool steel processed via LPBF, residual stress gradients, local microstructure and near-crack elemental concentrations is studied using longitudinal/transverse sectional synchrotron X-ray micro-diffraction, electron microscopy techniques and atom probe tomography. A formation of horizontal micro-cracks correlates with longitudinal/transverse sectional residual stress drops, especially at geometrically notched positions and sample edges. Remarkably, the cracks propagate predominantly along the network of eutectic intergranular carbides of type M2C deposited at the grain boundaries of carbon martensite and retained austenite matrix. A comparison of representative carbide sizes at the crack surfaces and within the crack-free regions indicates that cracks propagate preferably through the carbides in a transcrystalline manner, whereas no correlation between the cracking and the martensite formation is observed. The observations link the crack propagation to the solidification microstructure and the prevailing eutectic network. Therefore, the stress-induced cracking of eutectic carbides, which formed during the solidification and fracture in the solid state due to tensile stress accumulations, was found as the predominant cracking mechanism of the tool steel during the LPBF process.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Additive Manufacturing Materials and Processes · High Entropy Alloys Studies · Advanced materials and composites
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (77)
Show source-provided references
1. Gibson · 2015
2. Additive manufacturing of metals10.1016/j.actamat.2016.07.019 ↗
3. Making sense of 3-D printing: creating a map of additive manufacturing products and services
4. Gebhardt · 2012
5. Microstructure and properties of FeCrMoVC tool steel produced by selective laser melting10.1016/j.matdes.2015.09.148 ↗
6. SLM additive manufacture of H13 tool steel with conformal cooling and structural lattices10.1108/RPJ-06-2014-0075 ↗
7. A criterion for cracking during solidification10.1016/j.actamat.2015.01.034 ↗
8. Campbell · 2003
9. Kou · 2013
10. A new hot-tearing criterion10.1007/s11661-999-0334-z ↗
11. Revealing hot tearing mechanism for an additively manufactured high-entropy alloy via selective laser melting10.1016/j.scriptamat.2019.04.036 ↗
12. Reducing hot tearing by grain boundary segregation engineering in additive manufacturing: example of an AlxCoCrFeNi high-entropy alloy10.1016/j.actamat.2020.116505 ↗
13. Cracking mechanism and mechanical properties of selective laser melted CoCrFeMnNi high entropy alloy using different scanning strategies10.1016/j.msea.2020.139672 ↗
14. Effect of minor alloying elements on crack-formation characteristics of Hastelloy-X manufactured by selective laser melting
15. Investigations on the microstructure and crack formation of IN738LC samples processed by selective laser melting using Gaussian and doughnut profiles10.1016/j.matdes.2015.10.027 ↗
16. Experimental investigation on selective laser melting of 17-4PH stainless steel10.1016/j.optlastec.2016.07.012 ↗
17. Effects of heat treatment on microstructure, mechanical and corrosion properties of 15-5 PH stainless steel parts built by selective laser melting process10.1016/j.jmapro.2019.12.048 ↗
18. Precipitation in 18 wt% Ni maraging steel of grade 35010.1016/S1359-6454(99)00370-5 ↗
19. Precipitation hardening in 350 grade maraging steel10.1007/BF02646522 ↗
20. Microstructural characterization and properties of selective laser melted maraging steel with different build directions10.1080/14686996.2018.1527645 ↗
21. Additive manufacturing of an Fe–Cr–Ni–Al maraging stainless steel: microstructure evolution, heat treatment, and strengthening mechanisms10.1016/j.msea.2020.139470 ↗
22. Microstructure and mechanical properties of maraging steel 300 after selective laser melting
23. Heat treatment and properties of a hot work tool steel fabricated by additive manufacturing10.1016/j.msea.2019.03.027 ↗
24. Densification behavior of gas and water atomized 316L stainless steel powder during selective laser melting10.1016/j.apsusc.2010.02.030 ↗
25. Fundamentals of selective laser melting of alloyed steel powders10.1016/S0007-8506(07)60395-3 ↗
26. Microstructure, mechanical, and tribological properties of M3:2 high-speed steel processed by selective laser melting, hot-isostatic pressing, and casting
27. Microstructure and mechanical properties of X65MoCrWV3-2 cold-work tool steel produced by selective laser melting
28. General investigations on processing tool steel X40CrMoV5-1 with selective laser melting10.1016/j.jmatprotec.2018.01.012 ↗
29. Defect-free laser powder bed fusion of Ti–48Al–2Cr–2Nb with a high temperature inductive preheating system10.1088/2515-7647/ab7080 ↗
30. Gottstein · 2007
31. Influence of powder bed preheating on microstructure and mechanical properties of H13 Tool steel SLM parts10.1016/j.phpro.2016.08.092 ↗
32. A critical review of powder-based additive manufacturing of ferrous alloys: process parameters, microstructure and mechanical properties10.1016/j.matdes.2018.02.018 ↗
33. Feasability Investigation for laser powder bed fusion of high-speed steel AISI M50 with base preheating system10.1007/s00501-019-0828-y ↗
34. Microstructure and properties of selective laser melted high hardness tool steel10.1016/j.phpro.2013.03.157 ↗
35. Rapid solidification microstructure and carbide precipitation behavior in electron beam melted high-speed steel10.1007/s11661-020-05661-z ↗
36. Study of laser-sinterability of ferro-based powders10.1108/13552540510623594 ↗
37. Defects in a laser powder bed fused tool steel
38. The high energy materials science beamline (HEMS) at PETRA III10.1063/1.3463221 ↗
39. PyFAI, a versatile library for azimuthal regrouping10.1088/1742-6596/425/20/202012 ↗
40. Noyan · 2013
41. Elastic constants and internal friction of martensitic steel, ferritic-pearlitic steel, and α-iron10.1016/j.msea.2006.11.147 ↗
42. Berechnung der elastischen konstanten des vielkristalls aus den konstanten des einkristalls10.1007/BF01337948 ↗
43. X-ray nanodiffraction reveals strain and microstructure evolution in nanocrystalline thin films10.1016/j.scriptamat.2012.07.034 ↗
44. X-ray analysis of residual stress gradients in TiN coatings by a Laplace space approach and cross-sectional nanodiffraction: a critical comparison10.1107/S0021889813019535 ↗
45. Inconel-steel multilayers by liquid dispersed metal powder bed fusion: microstructure, residual stress and property gradients
46. Correlative cross-sectional characterization of nitrided, carburized and shot-peened steels: synchrotron micro-X-ray diffraction analysis of stress, microstructure and phase gradients10.1016/j.jmrt.2021.01.099 ↗
47. Oxford Instruments Homepage. https://nano.oxinst.com/ultim-extreme, accessed in May 2021.
48. Field ion image formation10.1016/0039-6028(78)90410-7 ↗
49. Atom probe tomography of the oxide layer of an austenitic stainless CrMnN-steel10.1515/pm-2021-0019 ↗
50. Gault · 2012
51. Impact of laser pulsing on the reconstruction in an atom probe tomography10.1016/j.ultramic.2010.04.017 ↗
52. Field calibration using the energy distribution of field ionization10.1103/PhysRevLett.30.532 ↗
53. Field calibration using the energy distribution of a free-space field ionization10.1063/1.323985 ↗
54. Reconstructing atom probe data: a review10.1016/j.ultramic.2013.03.010 ↗
55. Larson · 2013
56. Selective laser melting of H13: microstructure and residual stress10.1007/s10853-017-1380-3 ↗
57. Residual stresses in selective laser sintering and selective laser melting10.1108/13552540610707013 ↗
58. Dilthey · 2002
59. Thermal conductivity of metal powders for powder bed additive manufacturing
60. Microstructure and composition homogeneity, tensile property, and underlying thermal physical mechanism of selective laser melting tool steel parts10.1016/j.msea.2016.11.047 ↗
61. Fractography of sintered iron and steels
62. Goldstein · 2017
63. Oxford Instruments Nanoanalysis Homepage. https://nano.oxinst.com/library/blog/extreme-tips-and-tricks, accessed in May 2021.
64. Ultra-low kV EDS – a new approach to improved spatial resolution, surface sensitivity, and light element compositional imaging and analysis in the SEM10.1017/S1551929517000013 ↗
65. Roberts · 1998
66. Solidification of austenitic stainless steel weldments: part III–the effect of solidification behavior on hot cracking susceptibility
67. Folkhard · 1984
68. Influence of the weld pool geometry on solidification crack formation
69. Selective laser sintering of gas atomized M2 high speed steel powder10.1023/A:1004720011671 ↗
70. Selective laser melting of prealloyed high alloy steel powder beds10.4028/www.scientific.net/MSF.514-516.516 ↗
71. Crystal structure analysis of M2 high speed steel parts produced by selective laser melting10.1016/j.matchar.2013.07.010 ↗
72. Selective laser melting of ultra-high-strength TRIP steel: processing, microstructure, and properties10.1007/s10853-016-0731-9 ↗
73. Hot work tool steel processed by laser powder bed fusion: a review on most relevant influencing factors
74. Determination of martensite start temperature of high-speed steels based on thermodynamic calculations10.1002/srin.202000063 ↗
75. A preliminary investigation on selective laser melting of M2 high speed steel
76. Determination of carbide and matrix compositions in high-speed steels by analytical electron microscopy10.1007/BF02670163 ↗
77. The decomposition of the M2C carbide in high speed steel