Effect of hot rolling and primary annealing on the microstructure and texture of a β-stabilised γ-TiAl based alloy
Source abstract
Abstract
Abstract Titanium aluminide alloys based on the ordered γ-TiAl phase are intermetallic materials well suited for lightweight high-temperature applications. The TNM alloys, a specific, β-solidifying group among them with a nominal composition of Ti-43.5Al-4Nb-1Mo-0.1B (at.-%), offer a homogeneous and fine-grained microstructure upon casting. This advantage has been exploited to develop a lab-scale hot rolling process in which a cost-effective ingot breakdown of the starting material is omitted. The present work establishes a fundamental understanding of the processes prevailing in the material during hot rolling and primary annealing. Microstructural analysis and texture measurements conducted at a synchrotron radiation source allow to study deformation, recovery, recrystallisation, as well as phase transformation mechanisms in detail. Different hot rolling procedures conducted within the (α+β) and (α+β/βo+γ) regions of the phase diagram are considered and investigated with regard to the prevalent mechanisms. Hot rolling in the (α+β) region entails an α2 phase texture novel in γ-TiAl based alloys. Hot rolling in the (α+β/βo+γ) region near the γ-solvus temperature particularly promotes the breakdown of the initial microstructure in TNM alloys. A specially designed hot rolling process prevents the accumulation of a modified cube texture component in the γ-TiAl phase that is typically linked to anisotropic mechanical properties.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Intermetallics and Advanced Alloy Properties · Titanium Alloys Microstructure and Properties · Advanced materials and composites
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (54)
Show source-provided references
1. Intermetallic γ-TiAl based alloy sheet materials - processing and mechanical properties
2. Processing of γ-TiAl based alloys on an industrial scale
3. Deformation behavior of differently processed γ-titanium aluminides10.1016/S0921-5093(01)01552-0 ↗
4. Development and evaluation of TiAl sheet structures for hypersonic applications10.1016/j.msea.2007.02.020 ↗
5. Manufacturing and properties of TiAl TNM sheet materials
6. Manufacturing and properties of high Nb-TiAl sheet materials
7. A novel hot pack rolling of high Nb–TiAl sheet from cast ingot10.1016/j.intermet.2015.07.009 ↗
8. Physical metallurgy for wrought gamma titanium aluminides: microstructure control through phase transformations10.1016/j.intermet.2004.12.014 ↗
9. Design of novel β-solidifying TiAl alloys with adjustable β/B2-phase fraction and excellent hot-workability10.1002/adem.200800164 ↗
10. Intermetallic titanium aluminides in aerospace applications - processing, microstructure and properties10.1080/09603409.2016.1163792 ↗
11. Design, processing, microstructure, properties, and applications of advanced intermetallic TiAl alloys10.1002/adem.201200231 ↗
12. Effect of carbon addition on solidification behavior, phase evolution and creep properties of an intermetallic β-stabilized γ-TiAl based alloy10.1016/j.intermet.2013.11.011 ↗
13. Microstructural design and mechanical properties of a cast and heat-treated intermetallic multi-phase γ-TiAl based alloy10.1016/j.intermet.2013.09.010 ↗
14. Change of microstructure in a TiAl intermetallic compound during high temperature deformation
15. Textures and plastic anisotropy in γ-TiAl10.1016/0956-7151(92)90175-E ↗
16. Texture and microstructure of Ti-49%Al after dynamic recrystallization and annealing10.2355/isijinternational.33.313 ↗
17. Micromechanical mechanism of texture formation in γ-TiAl10.1016/S0966-9795(01)00086-3 ↗
18. Texture evolution of the γ- and the α/α2-phase during hot rolling of γ-TiAl based alloys10.1016/j.intermet.2005.07.002 ↗
19. Stark · 2010 · 59
20. Synchrotron texture analysis with area detectors10.1107/S0021889803010136 ↗
21. High-energy X-rays: a tool for advanced bulk investigations in materials science and physics10.1080/07303300310001634952 ↗
22. Intermetallic titanium aluminides as innovative high temperature lightweight construction materials – how materialographic methods have contributed to their development10.3139/147.110366 ↗
23. Two-dimensional detector software: from real detector to idealised image or two-theta scan10.1080/08957959608201408 ↗
24. Yi · 2005 · 41
25. A novel pole figure inversion method: specification of the MTEX algorithm10.1107/S0021889808030112 ↗
26. A simple standard orientation density function: the hyperspherical de la Vallée Poussin kernel10.1002/1521-3951(199704)200:2<367::AID-PSSB367>3.0.CO;2-I ↗
27. Effect of microstructural instability on the creep resistance of an advanced intermetallic γ-TiAl based alloy10.1016/j.intermet.2016.09.007 ↗
28. Texture analysis in hexagonal materials10.1016/S0254-0584(03)00168-8 ↗
29. Modelling of texture development and deformation mechanisms in a Ti20V alloy using a self consistent polycrystal approach10.1155/TSM.25.45 ↗
30. Descriptive tools for the analysis of texture projects with large datasets using MTEX: strength, symmetry and components10.1144/SP409.8 ↗
31. Hot rolling deformation and recrystallization textures in fcc metals
32. Mechanism of deformation and development of rolling textures in polycrystalline f.c.c. metals - I. Description of rolling texture development in homogeneous CuZn alloys10.1016/0001-6160(88)90172-1 ↗
33. Randle · 2010
34. Texture formation in high niobium containing TiAl alloy
35. Measurement of uncertainty in orientation distribution function calculations10.1016/j.scriptamat.2013.10.017 ↗
36. Analysis of experimental and theoretical rolling textures of two-phase titanium alloys
37. On the process of transition of the cubic-body-centered modification into the hexagonal-close-packed modification of zirconium10.1016/S0031-8914(34)80244-3 ↗
38. Hot rolling textures in high-strength Ti alloys
39. Hot rolling textures in Ti
40. Evolution of hot rolling textures in a two-phase (α2+β) Ti3Al base alloy10.1016/S1359-6454(99)00327-4 ↗
41. Texture and anisotropy of mechanical properties in titanium and its alloys
42. Texture and microstructure evolution of commercially pure titanium during hot rolling: role of strain-paths10.1016/j.matdes.2015.11.073 ↗
43. Rolling and annealing textures of bcc metals
44. Microstructure and texture evolution in an intermetallic β-stabilized TiAl alloy during forging and subsequent isothermal annealing
45. An investigation on microstructural and mechanical properties of powder metallurgical TiAl alloy during hot pack-rolling10.1016/j.msea.2014.09.091 ↗
46. In situ observation of texture evolution during α → β and β → α phase transformations in titanium alloys investigated by neutron diffraction10.1016/j.actamat.2007.06.017 ↗
47. In situ observation of texture and microstructure evolution during rolling and globularization of Ti-6Al-4V10.1016/j.actamat.2012.11.037 ↗
48. In situ neutron diffraction study of texture evolution and variant selection during the α → β → α phase transformation in Ti-6Al-4V10.1016/j.actamat.2012.09.026 ↗
49. The influence of rolling temperature on texture evolution and variant selection during α → β → α phase transformation in Ti-6Al-4V10.1016/j.actamat.2012.07.025 ↗
50. Importance of the α → β transformation in the variant selection mechanisms of thermomechanically processed titanium alloys10.1016/j.scriptamat.2008.05.013 ↗
51. Some aspects of phase transformations in titanium alloys
52. Neutron diffraction study of texture development during hot working of different gamma-titanium aluminide alloys10.1007/s11661-004-0193-6 ↗
53. Appel · 2011
54. Stability of rolling texture during heat treatment in a two-phase Ti3Al base intermetallic alloy10.1016/S1359-6454(99)00328-6 ↗