journal article·2017-03

Effect of hot rolling and primary annealing on the microstructure and texture of a β-stabilised γ-TiAl based alloy

Petra Erdely, Peter Staron, Emad Maawad, Norbert Schell, Joachim Klose, Svea Mayer, Helmut Clemens

Acta Materialia· Volume 126
Publisher page

Abstract

Abstract Titanium aluminide alloys based on the ordered γ-TiAl phase are intermetallic materials well suited for lightweight high-temperature applications. The TNM alloys, a specific, β-solidifying group among them with a nominal composition of Ti-43.5Al-4Nb-1Mo-0.1B (at.-%), offer a homogeneous and fine-grained microstructure upon casting. This advantage has been exploited to develop a lab-scale hot rolling process in which a cost-effective ingot breakdown of the starting material is omitted. The present work establishes a fundamental understanding of the processes prevailing in the material during hot rolling and primary annealing. Microstructural analysis and texture measurements conducted at a synchrotron radiation source allow to study deformation, recovery, recrystallisation, as well as phase transformation mechanisms in detail. Different hot rolling procedures conducted within the (α+β) and (α+β/βo+γ) regions of the phase diagram are considered and investigated with regard to the prevalent mechanisms. Hot rolling in the (α+β) region entails an α2 phase texture novel in γ-TiAl based alloys. Hot rolling in the (α+β/βo+γ) region near the γ-solvus temperature particularly promotes the breakdown of the initial microstructure in TNM alloys. A specially designed hot rolling process prevents the accumulation of a modified cube texture component in the γ-TiAl phase that is typically linked to anisotropic mechanical properties.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Intermetallics and Advanced Alloy Properties · Titanium Alloys Microstructure and Properties · Advanced materials and composites

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (54)

Show source-provided references
1. Intermetallic γ-TiAl based alloy sheet materials - processing and mechanical properties
2. Processing of γ-TiAl based alloys on an industrial scale
3. Deformation behavior of differently processed γ-titanium aluminides10.1016/S0921-5093(01)01552-0 ↗
4. Development and evaluation of TiAl sheet structures for hypersonic applications10.1016/j.msea.2007.02.020 ↗
5. Manufacturing and properties of TiAl TNM sheet materials
6. Manufacturing and properties of high Nb-TiAl sheet materials
7. A novel hot pack rolling of high Nb–TiAl sheet from cast ingot10.1016/j.intermet.2015.07.009 ↗
8. Physical metallurgy for wrought gamma titanium aluminides: microstructure control through phase transformations10.1016/j.intermet.2004.12.014 ↗
9. Design of novel β-solidifying TiAl alloys with adjustable β/B2-phase fraction and excellent hot-workability10.1002/adem.200800164 ↗
10. Intermetallic titanium aluminides in aerospace applications - processing, microstructure and properties10.1080/09603409.2016.1163792 ↗
11. Design, processing, microstructure, properties, and applications of advanced intermetallic TiAl alloys10.1002/adem.201200231 ↗
12. Effect of carbon addition on solidification behavior, phase evolution and creep properties of an intermetallic β-stabilized γ-TiAl based alloy10.1016/j.intermet.2013.11.011 ↗
13. Microstructural design and mechanical properties of a cast and heat-treated intermetallic multi-phase γ-TiAl based alloy10.1016/j.intermet.2013.09.010 ↗
14. Change of microstructure in a TiAl intermetallic compound during high temperature deformation
15. Textures and plastic anisotropy in γ-TiAl10.1016/0956-7151(92)90175-E ↗
16. Texture and microstructure of Ti-49%Al after dynamic recrystallization and annealing10.2355/isijinternational.33.313 ↗
17. Micromechanical mechanism of texture formation in γ-TiAl10.1016/S0966-9795(01)00086-3 ↗
18. Texture evolution of the γ- and the α/α2-phase during hot rolling of γ-TiAl based alloys10.1016/j.intermet.2005.07.002 ↗
19. Stark · 2010 · 59
20. Synchrotron texture analysis with area detectors10.1107/S0021889803010136 ↗
21. High-energy X-rays: a tool for advanced bulk investigations in materials science and physics10.1080/07303300310001634952 ↗
22. Intermetallic titanium aluminides as innovative high temperature lightweight construction materials – how materialographic methods have contributed to their development10.3139/147.110366 ↗
23. Two-dimensional detector software: from real detector to idealised image or two-theta scan10.1080/08957959608201408 ↗
24. Yi · 2005 · 41
25. A novel pole figure inversion method: specification of the MTEX algorithm10.1107/S0021889808030112 ↗
26. A simple standard orientation density function: the hyperspherical de la Vallée Poussin kernel10.1002/1521-3951(199704)200:2<367::AID-PSSB367>3.0.CO;2-I ↗
27. Effect of microstructural instability on the creep resistance of an advanced intermetallic γ-TiAl based alloy10.1016/j.intermet.2016.09.007 ↗
28. Texture analysis in hexagonal materials10.1016/S0254-0584(03)00168-8 ↗
29. Modelling of texture development and deformation mechanisms in a Ti20V alloy using a self consistent polycrystal approach10.1155/TSM.25.45 ↗
30. Descriptive tools for the analysis of texture projects with large datasets using MTEX: strength, symmetry and components10.1144/SP409.8 ↗
31. Hot rolling deformation and recrystallization textures in fcc metals
32. Mechanism of deformation and development of rolling textures in polycrystalline f.c.c. metals - I. Description of rolling texture development in homogeneous CuZn alloys10.1016/0001-6160(88)90172-1 ↗
33. Randle · 2010
34. Texture formation in high niobium containing TiAl alloy
35. Measurement of uncertainty in orientation distribution function calculations10.1016/j.scriptamat.2013.10.017 ↗
36. Analysis of experimental and theoretical rolling textures of two-phase titanium alloys
37. On the process of transition of the cubic-body-centered modification into the hexagonal-close-packed modification of zirconium10.1016/S0031-8914(34)80244-3 ↗
38. Hot rolling textures in high-strength Ti alloys
39. Hot rolling textures in Ti
40. Evolution of hot rolling textures in a two-phase (α2+β) Ti3Al base alloy10.1016/S1359-6454(99)00327-4 ↗
41. Texture and anisotropy of mechanical properties in titanium and its alloys
42. Texture and microstructure evolution of commercially pure titanium during hot rolling: role of strain-paths10.1016/j.matdes.2015.11.073 ↗
43. Rolling and annealing textures of bcc metals
44. Microstructure and texture evolution in an intermetallic β-stabilized TiAl alloy during forging and subsequent isothermal annealing
45. An investigation on microstructural and mechanical properties of powder metallurgical TiAl alloy during hot pack-rolling10.1016/j.msea.2014.09.091 ↗
46. In situ observation of texture evolution during α → β and β → α phase transformations in titanium alloys investigated by neutron diffraction10.1016/j.actamat.2007.06.017 ↗
47. In situ observation of texture and microstructure evolution during rolling and globularization of Ti-6Al-4V10.1016/j.actamat.2012.11.037 ↗
48. In situ neutron diffraction study of texture evolution and variant selection during the α → β → α phase transformation in Ti-6Al-4V10.1016/j.actamat.2012.09.026 ↗
49. The influence of rolling temperature on texture evolution and variant selection during α → β → α phase transformation in Ti-6Al-4V10.1016/j.actamat.2012.07.025 ↗
50. Importance of the α → β transformation in the variant selection mechanisms of thermomechanically processed titanium alloys10.1016/j.scriptamat.2008.05.013 ↗
51. Some aspects of phase transformations in titanium alloys
52. Neutron diffraction study of texture development during hot working of different gamma-titanium aluminide alloys10.1007/s11661-004-0193-6 ↗
53. Appel · 2011
54. Stability of rolling texture during heat treatment in a two-phase Ti3Al base intermetallic alloy10.1016/S1359-6454(99)00328-6 ↗